A Reversible Phase Transition of 2D Coordination Layers by B–H∙∙∙Cu(II) Interactions in a Coordination Polymer Article Swipe
Lei Gan
,
Pol Gimeno‐Fonquernie
,
Mark E. Light
,
Gantulga Norjmaa
,
Gregori Ujaque
,
Duane Choquesillo‐Lazarte
,
Julio Fraile
,
Francesç Teixidor
,
Clara Viñas
,
José Giner Planas
·
YOU?
·
· 2019
· Open Access
·
· DOI: https://doi.org/10.3390/molecules24173204
YOU?
·
· 2019
· Open Access
·
· DOI: https://doi.org/10.3390/molecules24173204
Materials that combine flexibility and open metal sites are crucial for myriad applications. In this article, we report a 2D coordination polymer (CP) assembled from CuII ions and a flexible meta-carborane-based linker [Cu2(L1)2(Solv)2]•xSolv (1-DMA, 1-DMF, and 1-MeOH; L1: 1,7-di(4-carboxyphenyl)-1,7-dicarba-closo-dodecaborane). 1-DMF undergoes an unusual example of reversible phase transition on solvent treatment (i.e., MeOH and CH2Cl2). Solvent exchange, followed by thermal activation provided a new porous phase that exhibits an estimated Brunauer-Emmett-Teller (BET) surface area of 301 m2 g−1 and is capable of a CO2 uptake of 41 cm3 g−1. The transformation is reversible and 1-DMF is reformed on addition of DMF to the porous phase. We provide evidence for the reversible process being the result of the formation/cleavage of weak but attractive B–H∙∙∙Cu interactions by a combination of single-crystal (SCXRD), powder (PXRD) X-ray diffraction, Raman spectroscopy, and DFT calculations.
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- Type
- article
- Language
- en
- Landing Page
- https://doi.org/10.3390/molecules24173204
- https://www.mdpi.com/1420-3049/24/17/3204/pdf?version=1567515705
- OA Status
- gold
- Cited By
- 11
- References
- 90
- Related Works
- 10
- OpenAlex ID
- https://openalex.org/W2971667757
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Raw OpenAlex JSON
- OpenAlex ID
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https://openalex.org/W2971667757Canonical identifier for this work in OpenAlex
- DOI
-
https://doi.org/10.3390/molecules24173204Digital Object Identifier
- Title
-
A Reversible Phase Transition of 2D Coordination Layers by B–H∙∙∙Cu(II) Interactions in a Coordination PolymerWork title
- Type
-
articleOpenAlex work type
- Language
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enPrimary language
- Publication year
-
2019Year of publication
- Publication date
-
2019-09-03Full publication date if available
- Authors
-
Lei Gan, Pol Gimeno‐Fonquernie, Mark E. Light, Gantulga Norjmaa, Gregori Ujaque, Duane Choquesillo‐Lazarte, Julio Fraile, Francesç Teixidor, Clara Viñas, José Giner PlanasList of authors in order
- Landing page
-
https://doi.org/10.3390/molecules24173204Publisher landing page
- PDF URL
-
https://www.mdpi.com/1420-3049/24/17/3204/pdf?version=1567515705Direct link to full text PDF
- Open access
-
YesWhether a free full text is available
- OA status
-
goldOpen access status per OpenAlex
- OA URL
-
https://www.mdpi.com/1420-3049/24/17/3204/pdf?version=1567515705Direct OA link when available
- Concepts
-
Coordination polymer, Coordination complex, Polymer, Phase transition, Chemistry, Transition metal, Crystallography, Coordination number, Phase (matter), Materials science, Chemical physics, Catalysis, Ion, Organic chemistry, Physics, Thermodynamics, MetalTop concepts (fields/topics) attached by OpenAlex
- Cited by
-
11Total citation count in OpenAlex
- Citations by year (recent)
-
2024: 4, 2023: 1, 2022: 1, 2021: 2, 2020: 2Per-year citation counts (last 5 years)
- References (count)
-
90Number of works referenced by this work
- Related works (count)
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10Other works algorithmically related by OpenAlex
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| referenced_works | https://openalex.org/W1979681627, https://openalex.org/W1999937609, https://openalex.org/W2891670902, https://openalex.org/W1677747913, https://openalex.org/W2618127528, https://openalex.org/W2792288416, https://openalex.org/W2883042906, https://openalex.org/W2572045154, https://openalex.org/W2599379284, https://openalex.org/W2091161882, https://openalex.org/W2141939342, https://openalex.org/W2607412255, https://openalex.org/W1988515201, https://openalex.org/W2588265396, https://openalex.org/W2558046062, https://openalex.org/W2744528294, https://openalex.org/W2158962087, https://openalex.org/W2086917649, https://openalex.org/W2051853320, https://openalex.org/W2019481980, https://openalex.org/W2522564267, https://openalex.org/W1974335314, https://openalex.org/W2802762250, https://openalex.org/W2802260133, https://openalex.org/W966261395, https://openalex.org/W2728167338, https://openalex.org/W2756103189, https://openalex.org/W2040402142, https://openalex.org/W3023823680, https://openalex.org/W4248548734, https://openalex.org/W2049350055, https://openalex.org/W2124952091, https://openalex.org/W1995082042, https://openalex.org/W2005230726, https://openalex.org/W2095838412, https://openalex.org/W2030915403, https://openalex.org/W2011460312, https://openalex.org/W2090264815, https://openalex.org/W2069094014, https://openalex.org/W1972677469, https://openalex.org/W2021834633, https://openalex.org/W1979274575, https://openalex.org/W1981907332, https://openalex.org/W2275579934, https://openalex.org/W2562781547, https://openalex.org/W2559216790, https://openalex.org/W2805844430, https://openalex.org/W2091606578, https://openalex.org/W2095256453, https://openalex.org/W2072776117, https://openalex.org/W2894887975, https://openalex.org/W2289202918, https://openalex.org/W2106584729, https://openalex.org/W2801874581, https://openalex.org/W2204898354, https://openalex.org/W2318731154, https://openalex.org/W2950557880, https://openalex.org/W2067752356, https://openalex.org/W1999112652, https://openalex.org/W2046974590, https://openalex.org/W2107332779, https://openalex.org/W2903520083, https://openalex.org/W2142054017, https://openalex.org/W2056726952, https://openalex.org/W2003865154, https://openalex.org/W2936086346, https://openalex.org/W2766163942, https://openalex.org/W2469771790, https://openalex.org/W2039198778, https://openalex.org/W2035124676, https://openalex.org/W2023694170, https://openalex.org/W1976849598, https://openalex.org/W2602791658, https://openalex.org/W2138885168, https://openalex.org/W2038123723, https://openalex.org/W6600255608, https://openalex.org/W2131350133, https://openalex.org/W2145538332, https://openalex.org/W2092157292, https://openalex.org/W2143981217, https://openalex.org/W2023271753, https://openalex.org/W2148284063, https://openalex.org/W2015723183, https://openalex.org/W1964837435, https://openalex.org/W2033990154, https://openalex.org/W2017218551, https://openalex.org/W2027324312, https://openalex.org/W2021677344, https://openalex.org/W1972266093, https://openalex.org/W2464559437 |
| referenced_works_count | 90 |
| abstract_inverted_index.a | 18, 28, 62, 82, 125 |
| abstract_inverted_index.2D | 19 |
| abstract_inverted_index.41 | 86 |
| abstract_inverted_index.In | 13 |
| abstract_inverted_index.We | 105 |
| abstract_inverted_index.an | 41, 68 |
| abstract_inverted_index.by | 58, 124 |
| abstract_inverted_index.is | 79, 91, 95 |
| abstract_inverted_index.m2 | 76 |
| abstract_inverted_index.of | 44, 74, 81, 85, 99, 115, 118, 127 |
| abstract_inverted_index.on | 48, 97 |
| abstract_inverted_index.to | 101 |
| abstract_inverted_index.we | 16 |
| abstract_inverted_index.301 | 75 |
| abstract_inverted_index.CO2 | 83 |
| abstract_inverted_index.DFT | 137 |
| abstract_inverted_index.DMF | 100 |
| abstract_inverted_index.L1: | 37 |
| abstract_inverted_index.The | 89 |
| abstract_inverted_index.and | 4, 27, 35, 53, 78, 93, 136 |
| abstract_inverted_index.are | 8 |
| abstract_inverted_index.but | 120 |
| abstract_inverted_index.cm3 | 87 |
| abstract_inverted_index.for | 10, 108 |
| abstract_inverted_index.new | 63 |
| abstract_inverted_index.the | 102, 109, 113, 116 |
| abstract_inverted_index.(CP) | 22 |
| abstract_inverted_index.CuII | 25 |
| abstract_inverted_index.MeOH | 52 |
| abstract_inverted_index.area | 73 |
| abstract_inverted_index.from | 24 |
| abstract_inverted_index.ions | 26 |
| abstract_inverted_index.open | 5 |
| abstract_inverted_index.that | 1, 66 |
| abstract_inverted_index.this | 14 |
| abstract_inverted_index.weak | 119 |
| abstract_inverted_index.(BET) | 71 |
| abstract_inverted_index.1-DMF | 39, 94 |
| abstract_inverted_index.Raman | 134 |
| abstract_inverted_index.X-ray | 132 |
| abstract_inverted_index.being | 112 |
| abstract_inverted_index.g−1 | 77 |
| abstract_inverted_index.metal | 6 |
| abstract_inverted_index.phase | 46, 65 |
| abstract_inverted_index.sites | 7 |
| abstract_inverted_index.(PXRD) | 131 |
| abstract_inverted_index.(i.e., | 51 |
| abstract_inverted_index.1-DMF, | 34 |
| abstract_inverted_index.g−1. | 88 |
| abstract_inverted_index.linker | 31 |
| abstract_inverted_index.myriad | 11 |
| abstract_inverted_index.phase. | 104 |
| abstract_inverted_index.porous | 64, 103 |
| abstract_inverted_index.powder | 130 |
| abstract_inverted_index.report | 17 |
| abstract_inverted_index.result | 114 |
| abstract_inverted_index.uptake | 84 |
| abstract_inverted_index.(1-DMA, | 33 |
| abstract_inverted_index.1-MeOH; | 36 |
| abstract_inverted_index.Solvent | 55 |
| abstract_inverted_index.capable | 80 |
| abstract_inverted_index.combine | 2 |
| abstract_inverted_index.crucial | 9 |
| abstract_inverted_index.example | 43 |
| abstract_inverted_index.polymer | 21 |
| abstract_inverted_index.process | 111 |
| abstract_inverted_index.provide | 106 |
| abstract_inverted_index.solvent | 49 |
| abstract_inverted_index.surface | 72 |
| abstract_inverted_index.thermal | 59 |
| abstract_inverted_index.unusual | 42 |
| abstract_inverted_index.(SCXRD), | 129 |
| abstract_inverted_index.CH2Cl2). | 54 |
| abstract_inverted_index.addition | 98 |
| abstract_inverted_index.article, | 15 |
| abstract_inverted_index.evidence | 107 |
| abstract_inverted_index.exhibits | 67 |
| abstract_inverted_index.flexible | 29 |
| abstract_inverted_index.followed | 57 |
| abstract_inverted_index.provided | 61 |
| abstract_inverted_index.reformed | 96 |
| abstract_inverted_index.Materials | 0 |
| abstract_inverted_index.assembled | 23 |
| abstract_inverted_index.estimated | 69 |
| abstract_inverted_index.exchange, | 56 |
| abstract_inverted_index.treatment | 50 |
| abstract_inverted_index.undergoes | 40 |
| abstract_inverted_index.activation | 60 |
| abstract_inverted_index.attractive | 121 |
| abstract_inverted_index.reversible | 45, 92, 110 |
| abstract_inverted_index.transition | 47 |
| abstract_inverted_index.combination | 126 |
| abstract_inverted_index.flexibility | 3 |
| abstract_inverted_index.coordination | 20 |
| abstract_inverted_index.diffraction, | 133 |
| abstract_inverted_index.interactions | 123 |
| abstract_inverted_index.applications. | 12 |
| abstract_inverted_index.calculations. | 138 |
| abstract_inverted_index.spectroscopy, | 135 |
| abstract_inverted_index.single-crystal | 128 |
| abstract_inverted_index.transformation | 90 |
| abstract_inverted_index.B–H∙∙∙Cu | 122 |
| abstract_inverted_index.formation/cleavage | 117 |
| abstract_inverted_index.meta-carborane-based | 30 |
| abstract_inverted_index.Brunauer-Emmett-Teller | 70 |
| abstract_inverted_index.[Cu2(L1)2(Solv)2]•xSolv | 32 |
| abstract_inverted_index.1,7-di(4-carboxyphenyl)-1,7-dicarba-closo-dodecaborane). | 38 |
| cited_by_percentile_year.max | 98 |
| cited_by_percentile_year.min | 89 |
| corresponding_author_ids | https://openalex.org/A5013308183 |
| countries_distinct_count | 2 |
| institutions_distinct_count | 10 |
| corresponding_institution_ids | https://openalex.org/I4210134458 |
| citation_normalized_percentile.value | 0.60748571 |
| citation_normalized_percentile.is_in_top_1_percent | False |
| citation_normalized_percentile.is_in_top_10_percent | False |