Ammonia-Assisted Quadrupled-Yield ZIF-67 Derivation Enables Single Oxygen-Dominated Nonradical Oxidation for Enhanced Ciprofloxacin Degradation Article Swipe
Xiaoxian Hu
,
Di Zhang
,
Xinyu Li
,
Junfeng Wu
,
Xiang Guo
,
Hongbin Gao
,
Minghui Hao
,
Yingchun Wang
,
Bang Li
,
Xinhai Zhang
·
YOU?
·
· 2025
· Open Access
·
· DOI: https://doi.org/10.3390/ma18184337
YOU?
·
· 2025
· Open Access
·
· DOI: https://doi.org/10.3390/ma18184337
The widespread contamination of aquatic systems by ciprofloxacin (CIP)—a persistent fluoroquinolone antibiotic—poses severe ecological risks due to its antibacterial resistance induction. Conventional sulfate radical-based advanced oxidation processes (SR-AOPs) suffer from inefficient catalyst synthesis, exemplified by low-yield ZIF-67 precursors (typically <25%). To address this, a nitrogen-doped carbon composite Co3O4/N@C was synthesized via ammonia-assisted ligand exchange followed by pyrolysis, using N-doped ZIF-67 as a self-sacrificial template. The ammonia incorporation quadrupled precursor yield compared to ammonia-free methods. This catalyst activated peroxydisulfate (PDS) to degrade 95% CIP within 90 min under the optimized conditions (0.5 g/L catalyst, 2 mmol/L PDS, pH 5), representing a 30% enhancement over non-ammonia analogs. Mechanistic studies identified singlet oxygen (1O2) as the dominant reactive species, facilitated by N-doped carbon-mediated electron transfer. This strategy overcomes the scalability barrier of MOF-derived catalysts for practical antibiotic wastewater remediation.
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- article
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- en
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- https://doi.org/10.3390/ma18184337
- https://www.mdpi.com/1996-1944/18/18/4337/pdf?version=1758075181
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- References
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https://doi.org/10.3390/ma18184337Digital Object Identifier
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Ammonia-Assisted Quadrupled-Yield ZIF-67 Derivation Enables Single Oxygen-Dominated Nonradical Oxidation for Enhanced Ciprofloxacin DegradationWork title
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2025Year of publication
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2025-09-16Full publication date if available
- Authors
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Xiaoxian Hu, Di Zhang, Xinyu Li, Junfeng Wu, Xiang Guo, Hongbin Gao, Minghui Hao, Yingchun Wang, Bang Li, Xinhai ZhangList of authors in order
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https://doi.org/10.3390/ma18184337Publisher landing page
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https://www.mdpi.com/1996-1944/18/18/4337/pdf?version=1758075181Direct link to full text PDF
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goldOpen access status per OpenAlex
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https://www.mdpi.com/1996-1944/18/18/4337/pdf?version=1758075181Direct OA link when available
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