An efficient p-n type based (NiO/CeO2) hybrid composite photocatalyst and its performance for cationic dye degradation: Probable degradation pathways, optimization activities, and depth mechanism insights Article Swipe
M Suresh Kumar
,
Atikur Rahman
,
Vijay Pratap Singh
·
YOU?
·
· 2024
· Open Access
·
· DOI: https://doi.org/10.1016/j.nxener.2024.100228
YOU?
·
· 2024
· Open Access
·
· DOI: https://doi.org/10.1016/j.nxener.2024.100228
In this work, NiO, CeO2, and NiO/CeO2 nanoparticles were prepared by stepwise a simple co-precipitation method and subsequently hybridized with various ratios (1:1, 1:2, and 1:3) a facile mixing method. The prepared NiO/CeO2 composite samples at diverse ratios were analyzed using various analytical techniques, including X-ray diffraction (XRD), Fourier-transform infrared spectroscopy (FT-IR), UV–visible diffuse reflectance spectroscopy (UV-DRS), Field emission scanning electron microscopy (FE-SEM), X-ray photoelectron spectroscopy (XPS), photoluminescence (PL), and Raman spectroscopy. These methods were employed to investigate the chemical composition, morphological features, and optical characteristics of the composites, providing a comprehensive understanding of their properties and potential characteristics. The photocatalytic degradation of methylene blue (MB) was investigated by the prepared NiO/CeO2 composite samples with changing parameters, such as pH, catalyst dose, initial dye concentration, and agitation time under UV and solar light irradiation. Kinetic investigations revealed that the photodegradation of MB followed a pseudo-first-order kinetic model. Amongst the tested catalysts NiO/CeO2 (1:2) exhibited the highest photo-degradation of MB dye (97%) at pH around 10 in 60 min compared to 45% for neat NiO and 67% for pure CeO2 respectively. Similarly, under natural solar conditions, it takes time but degrades 94% Of MB at 210 min. The radical detection test was carried out with trapping agents ethylene diamine tetra acetic acid (EDTA), isopropyl alcohol (IPA), and benzoquinone (BQ) to establish the vital role of hydroxyl radicals (OH•) in the photodegradation of dyes. Eventually, the high stability and recyclability of the NiO/CeO2 (1:2) photocatalyst was confirmed after five consecutive runs. The mechanistic pathway of the dye degradation was explained by the scheme model based on p-n hetero-junction. Overall the study demonstrates the effectiveness of NiO/CeO2 (1:2) heterojunctions in photocatalytic applications, for the removal of dye contaminants from wastewater using UV and visible light conditions.
Related Topics
Concepts
Degradation (telecommunications)
Cationic polymerization
Non-blocking I/O
Mechanism (biology)
Composite number
Photocatalysis
Chemistry
Chemical engineering
Materials science
Computer science
Catalysis
Engineering
Composite material
Biochemistry
Physics
Telecommunications
Polymer chemistry
Quantum mechanics
Metadata
- Type
- article
- Language
- en
- Landing Page
- https://doi.org/10.1016/j.nxener.2024.100228
- OA Status
- diamond
- Cited By
- 10
- References
- 96
- Related Works
- 10
- OpenAlex ID
- https://openalex.org/W4405531260
All OpenAlex metadata
Raw OpenAlex JSON
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https://openalex.org/W4405531260Canonical identifier for this work in OpenAlex
- DOI
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https://doi.org/10.1016/j.nxener.2024.100228Digital Object Identifier
- Title
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An efficient p-n type based (NiO/CeO2) hybrid composite photocatalyst and its performance for cationic dye degradation: Probable degradation pathways, optimization activities, and depth mechanism insightsWork title
- Type
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articleOpenAlex work type
- Language
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enPrimary language
- Publication year
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2024Year of publication
- Publication date
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2024-12-18Full publication date if available
- Authors
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M Suresh Kumar, Atikur Rahman, Vijay Pratap SinghList of authors in order
- Landing page
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https://doi.org/10.1016/j.nxener.2024.100228Publisher landing page
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YesWhether a free full text is available
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diamondOpen access status per OpenAlex
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https://doi.org/10.1016/j.nxener.2024.100228Direct OA link when available
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Degradation (telecommunications), Cationic polymerization, Non-blocking I/O, Mechanism (biology), Composite number, Photocatalysis, Chemistry, Chemical engineering, Materials science, Computer science, Catalysis, Engineering, Composite material, Biochemistry, Physics, Telecommunications, Polymer chemistry, Quantum mechanicsTop concepts (fields/topics) attached by OpenAlex
- Cited by
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10Total citation count in OpenAlex
- Citations by year (recent)
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2025: 10Per-year citation counts (last 5 years)
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96Number of works referenced by this work
- Related works (count)
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10Other works algorithmically related by OpenAlex
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| referenced_works_count | 96 |
| abstract_inverted_index.a | 12, 26, 90, 143 |
| abstract_inverted_index.10 | 164 |
| abstract_inverted_index.60 | 166 |
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| abstract_inverted_index.Of | 191 |
| abstract_inverted_index.UV | 129, 288 |
| abstract_inverted_index.as | 118 |
| abstract_inverted_index.at | 35, 161, 193 |
| abstract_inverted_index.by | 10, 108, 258 |
| abstract_inverted_index.in | 165, 227, 276 |
| abstract_inverted_index.it | 185 |
| abstract_inverted_index.of | 86, 93, 102, 140, 157, 223, 230, 238, 252, 272, 282 |
| abstract_inverted_index.on | 263 |
| abstract_inverted_index.pH | 162 |
| abstract_inverted_index.to | 76, 169, 218 |
| abstract_inverted_index.210 | 194 |
| abstract_inverted_index.45% | 170 |
| abstract_inverted_index.67% | 175 |
| abstract_inverted_index.94% | 190 |
| abstract_inverted_index.NiO | 173 |
| abstract_inverted_index.The | 30, 99, 196, 249 |
| abstract_inverted_index.and | 5, 16, 24, 69, 83, 96, 125, 130, 174, 215, 236, 289 |
| abstract_inverted_index.but | 188 |
| abstract_inverted_index.dye | 123, 159, 254, 283 |
| abstract_inverted_index.for | 171, 176, 279 |
| abstract_inverted_index.min | 167 |
| abstract_inverted_index.out | 202 |
| abstract_inverted_index.p-n | 264 |
| abstract_inverted_index.pH, | 119 |
| abstract_inverted_index.the | 78, 87, 109, 138, 148, 154, 220, 228, 233, 239, 253, 259, 267, 270, 280 |
| abstract_inverted_index.was | 106, 200, 243, 256 |
| abstract_inverted_index.(BQ) | 217 |
| abstract_inverted_index.(MB) | 105 |
| abstract_inverted_index.1:2, | 23 |
| abstract_inverted_index.1:3) | 25 |
| abstract_inverted_index.CeO2 | 178 |
| abstract_inverted_index.NiO, | 3 |
| abstract_inverted_index.acid | 210 |
| abstract_inverted_index.blue | 104 |
| abstract_inverted_index.five | 246 |
| abstract_inverted_index.from | 285 |
| abstract_inverted_index.high | 234 |
| abstract_inverted_index.min. | 195 |
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| abstract_inverted_index.pure | 177 |
| abstract_inverted_index.role | 222 |
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| abstract_inverted_index.test | 199 |
| abstract_inverted_index.that | 137 |
| abstract_inverted_index.this | 1 |
| abstract_inverted_index.time | 127, 187 |
| abstract_inverted_index.were | 8, 38, 74 |
| abstract_inverted_index.with | 19, 114, 203 |
| abstract_inverted_index.(1:1, | 22 |
| abstract_inverted_index.(1:2) | 152, 241, 274 |
| abstract_inverted_index.(97%) | 160 |
| abstract_inverted_index.(PL), | 68 |
| abstract_inverted_index.CeO2, | 4 |
| abstract_inverted_index.Field | 57 |
| abstract_inverted_index.Raman | 70 |
| abstract_inverted_index.These | 72 |
| abstract_inverted_index.X-ray | 45, 63 |
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| abstract_inverted_index.based | 262 |
| abstract_inverted_index.dose, | 121 |
| abstract_inverted_index.dyes. | 231 |
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| abstract_inverted_index.their | 94 |
| abstract_inverted_index.under | 128, 181 |
| abstract_inverted_index.using | 40, 287 |
| abstract_inverted_index.vital | 221 |
| abstract_inverted_index.work, | 2 |
| abstract_inverted_index.(IPA), | 214 |
| abstract_inverted_index.(XPS), | 66 |
| abstract_inverted_index.(XRD), | 47 |
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| abstract_inverted_index.agents | 205 |
| abstract_inverted_index.around | 163 |
| abstract_inverted_index.facile | 27 |
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| abstract_inverted_index.Overall | 266 |
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| abstract_inverted_index.various | 20, 41 |
| abstract_inverted_index.visible | 290 |
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| abstract_inverted_index.analyzed | 39 |
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| abstract_inverted_index.infrared | 49 |
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| abstract_inverted_index.scanning | 59 |
| abstract_inverted_index.stepwise | 11 |
| abstract_inverted_index.trapping | 204 |
| abstract_inverted_index.(FE-SEM), | 62 |
| abstract_inverted_index.(UV-DRS), | 56 |
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| abstract_inverted_index.catalysts | 150 |
| abstract_inverted_index.composite | 33, 112 |
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| abstract_inverted_index.establish | 219 |
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| abstract_inverted_index.explained | 257 |
| abstract_inverted_index.features, | 82 |
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| abstract_inverted_index.methylene | 103 |
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| abstract_inverted_index.microscopy | 61 |
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| abstract_inverted_index.composites, | 88 |
| abstract_inverted_index.conditions, | 184 |
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| abstract_inverted_index.mechanistic | 250 |
| abstract_inverted_index.parameters, | 116 |
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| abstract_inverted_index.techniques, | 43 |
| abstract_inverted_index.UV–visible | 52 |
| abstract_inverted_index.benzoquinone | 216 |
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| abstract_inverted_index.photoluminescence | 67 |
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