Biocomposites of Poly(Lactic Acid) and Microcrystalline Cellulose: Influence of the Coupling Agent on Thermomechanical and Absorption Characteristics Article Swipe
Emre Görgün
,
Alamry Ali
,
Md. Saiful Islam
·
YOU?
·
· 2024
· Open Access
·
· DOI: https://doi.org/10.1021/acsomega.3c08448
YOU?
·
· 2024
· Open Access
·
· DOI: https://doi.org/10.1021/acsomega.3c08448
In this study, poly(lactic acid) (PLA) and microcrystalline cellulose (MCC)-based green biocomposites were developed using a solution casting technique. Essentially, the bonding between PLA and MCC is quite feeble; therefore, the current study is conducted to strengthen the bonding by incorporating a coupling agent, thereby enhancing the overall quality of the biocomposites. Thus, the present study aimed to examine the influence of combined coupling agents-maleic anhydride (MAH) and maleic acid (MA) (MAH-MA)-on the properties of polylactic acid (PLA)/microcrystalline cellulose (MCC) biocomposites. The investigation also encompassed an examination of the impact of MCC loading (2, 3, and 5% w/w) into a PLA matrix. The Fourier transform infrared spectroscopy (FTIR) and scanning electron microscopy (SEM) examination revealed the interfacial interaction and adhesion among MCC, PLA, and coupling agents and the formation of biocomposites. The incorporation of MAH-MA led to improved mechanical properties of the PLA/MCC biocomposites. Furthermore, the incorporation of MAH-MA into the PLA/3 wt % MCC composite exhibited enhancements in both the tensile strength and tensile modulus, accompanied by a reduced elongation at break. In addition, it is worth noting that the thermogravimetric analysis (TGA) curve of the PLA composite with 3% w/w of MCC and MAH-MA displayed a significant decrease in weight beyond a temperature threshold of 492.65 °C. The water absorption demonstrates that the incorporation of MAH-MA into the PLA/MCC composite led to advantageous water barrier characteristics. The observed improvements were attributed to the efficient dispersion of MCC at the most favorable amount of coupling agents, along with the chemical interactions involving grafting and esterification between MCC and the MAH-MA coupling agent. Furthermore, the incorporation of MAH-MA into the PLA/3% (w/w) MCC composite exhibited enhancements in both the tensile strength and tensile modulus, accompanied by a reduction in the elongation percentage at break. The experimental results about water absorption demonstrate that the incorporation of MAH-MA into the PLA/MCC composite led to advantageous water barrier characteristics. These improvements were attributed to good MCC dispersion and the chemical interactions involving grafting and esterification between the MCC and the MAH-MA coupling agent.
Related Topics
Concepts
Microcrystalline cellulose
Materials science
Polylactic acid
Thermogravimetric analysis
Ultimate tensile strength
Absorption of water
Composite number
Fourier transform infrared spectroscopy
Maleic anhydride
Composite material
Lactic acid
Izod impact strength test
Cellulose
Dynamic mechanical analysis
Chemical engineering
Polymer chemistry
Polymer
Copolymer
Bacteria
Biology
Genetics
Engineering
Metadata
- Type
- article
- Language
- en
- Landing Page
- https://doi.org/10.1021/acsomega.3c08448
- https://pubs.acs.org/doi/pdf/10.1021/acsomega.3c08448
- OA Status
- gold
- Cited By
- 35
- References
- 48
- Related Works
- 10
- OpenAlex ID
- https://openalex.org/W4392286333
All OpenAlex metadata
Raw OpenAlex JSON
- OpenAlex ID
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https://openalex.org/W4392286333Canonical identifier for this work in OpenAlex
- DOI
-
https://doi.org/10.1021/acsomega.3c08448Digital Object Identifier
- Title
-
Biocomposites of Poly(Lactic Acid) and Microcrystalline Cellulose: Influence of the Coupling Agent on Thermomechanical and Absorption CharacteristicsWork title
- Type
-
articleOpenAlex work type
- Language
-
enPrimary language
- Publication year
-
2024Year of publication
- Publication date
-
2024-02-29Full publication date if available
- Authors
-
Emre Görgün, Alamry Ali, Md. Saiful IslamList of authors in order
- Landing page
-
https://doi.org/10.1021/acsomega.3c08448Publisher landing page
- PDF URL
-
https://pubs.acs.org/doi/pdf/10.1021/acsomega.3c08448Direct link to full text PDF
- Open access
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YesWhether a free full text is available
- OA status
-
goldOpen access status per OpenAlex
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https://pubs.acs.org/doi/pdf/10.1021/acsomega.3c08448Direct OA link when available
- Concepts
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Microcrystalline cellulose, Materials science, Polylactic acid, Thermogravimetric analysis, Ultimate tensile strength, Absorption of water, Composite number, Fourier transform infrared spectroscopy, Maleic anhydride, Composite material, Lactic acid, Izod impact strength test, Cellulose, Dynamic mechanical analysis, Chemical engineering, Polymer chemistry, Polymer, Copolymer, Bacteria, Biology, Genetics, EngineeringTop concepts (fields/topics) attached by OpenAlex
- Cited by
-
35Total citation count in OpenAlex
- Citations by year (recent)
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2025: 30, 2024: 5Per-year citation counts (last 5 years)
- References (count)
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48Number of works referenced by this work
- Related works (count)
-
10Other works algorithmically related by OpenAlex
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