Biomedical NiTi and β-Ti Alloys: From Composition, Microstructure and Thermo-Mechanics to Application Article Swipe
Adelaide Nespoli
,
Francesca Passaretti
,
László Szentmiklósi
,
Boglárka Maróti
,
E. Placidi
,
Michele Cassetta
,
Rickey Y. Yada
,
David H. Farrar
,
Kun Tian
·
YOU?
·
· 2022
· Open Access
·
· DOI: https://doi.org/10.3390/met12030406
YOU?
·
· 2022
· Open Access
·
· DOI: https://doi.org/10.3390/met12030406
A comprehensive, bottoms-up characterization of two of the most widely used biomedical Ti-containing alloys, NiTi and β-Ti, was carried out applying a novel combination of neutron diffraction, neutron prompt-gamma activation, surface morphology, thermal analysis and mechanical tests, to relate composition, microstructure and physical-chemical-mechanical properties to unknown processing history. The commercial specimens studied are rectangular (0.43 × 0.64 mm~0.017 × 0.025 inch) wires, in both pre-formed U-shape and straight extended form. Practical performance was quantitatively linked to the influence of alloying elements, microstructure and thermo-mechanical processing. Results demonstrated that the microstructure and phase composition of β-Ti strongly depended on the composition, phase-stabilizing elements in particular, in that the 10.2 wt.% Mo content in Azdent resulted in 41.2% α phase, while Ormco with 11.6 wt.% Mo contained only β phase. Although the existence of α phase is probable in the meta-stable alloy, the α phase has never been quantified before. Further, the phase transformation behavior of NiTi directly arose from the microstructure, whilst being highly influenced by thermo-mechanical history. A strong correlation (r = 0.878) was established between phase transformation temperature and the force levels observed in bending test at body temperature, reconfirming that structure determines performance, while also being highly influenced by thermo-mechanical history. The novel methodology described is evidenced as generating a predictive profile of the eventual biomechanical properties and practical performance of the commercial materials. Overall, the work encompasses a reproducible and comprehensive approach expected to aid in future optimization and rational design of devices of metallic origin.
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Metadata
- Type
- article
- Language
- en
- Landing Page
- https://doi.org/10.3390/met12030406
- https://www.mdpi.com/2075-4701/12/3/406/pdf?version=1645886534
- OA Status
- gold
- Cited By
- 33
- References
- 41
- Related Works
- 10
- OpenAlex ID
- https://openalex.org/W4214748058
All OpenAlex metadata
Raw OpenAlex JSON
- OpenAlex ID
-
https://openalex.org/W4214748058Canonical identifier for this work in OpenAlex
- DOI
-
https://doi.org/10.3390/met12030406Digital Object Identifier
- Title
-
Biomedical NiTi and β-Ti Alloys: From Composition, Microstructure and Thermo-Mechanics to ApplicationWork title
- Type
-
articleOpenAlex work type
- Language
-
enPrimary language
- Publication year
-
2022Year of publication
- Publication date
-
2022-02-25Full publication date if available
- Authors
-
Adelaide Nespoli, Francesca Passaretti, László Szentmiklósi, Boglárka Maróti, E. Placidi, Michele Cassetta, Rickey Y. Yada, David H. Farrar, Kun TianList of authors in order
- Landing page
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https://doi.org/10.3390/met12030406Publisher landing page
- PDF URL
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https://www.mdpi.com/2075-4701/12/3/406/pdf?version=1645886534Direct link to full text PDF
- Open access
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YesWhether a free full text is available
- OA status
-
goldOpen access status per OpenAlex
- OA URL
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https://www.mdpi.com/2075-4701/12/3/406/pdf?version=1645886534Direct OA link when available
- Concepts
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Microstructure, Materials science, Nickel titanium, Shape-memory alloy, Phase (matter), Alloy, Neutron diffraction, Titanium alloy, Bending, Composite material, Metallurgy, Crystallography, Chemistry, Crystal structure, Organic chemistryTop concepts (fields/topics) attached by OpenAlex
- Cited by
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33Total citation count in OpenAlex
- Citations by year (recent)
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2025: 6, 2024: 9, 2023: 10, 2022: 8Per-year citation counts (last 5 years)
- References (count)
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41Number of works referenced by this work
- Related works (count)
-
10Other works algorithmically related by OpenAlex
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