Capabilities of Grazing Incidence X-ray Diffraction in the Investigation of Amorphous Mixed Oxides with Variable Composition Article Swipe
Elisabetta Achilli
,
Filippo Annoni
,
N. Armani
,
M. Patrini
,
Marina Cornelli
,
Leonardo Celada
,
Melanie Micali
,
A. Terrasi
,
Paolo Ghigna
,
Gianluca Timò
·
YOU?
·
· 2022
· Open Access
·
· DOI: https://doi.org/10.3390/ma15062144
YOU?
·
· 2022
· Open Access
·
· DOI: https://doi.org/10.3390/ma15062144
X-ray Diffraction has been fully exploited as a probe to investigate crystalline materials. However, very little research has been carried out to unveil its potentialities towards amorphous materials. In this work, we demonstrated the capabilities of Grazing Incidence X-ray Diffraction (GIXRD) as a simple and fast tool to obtain quantitative information about the composition of amorphous mixed oxides. In particular, we evidenced that low angle scattering features, associated with local structure parameters, show a significant trend as a function of the oxide composition. This evolution can be quantified by interpolating GIXRD data with a linear combination of basic analytical functions, making it possible to build up GIXRD peak-sample composition calibration curves. As a case study, the present method was demonstrated on Ta2O5–SiO2 amorphous films deposited by RF-magnetron sputtering. GIXRD results were validated by independent measurement of the oxide composition using Rutherford Backscattering Spectrometry (RBS). These materials are attracting interest in different industrial sectors and, in particular, in photovoltaics as anti-reflection coatings. Eventually, the optical properties measured by spectroscopic ellipsometry were correlated to the chemical composition of the film. The obtained results highlighted not only a correlation between diffraction features and the composition of amorphous films but also revealed a simple and fast strategy to characterize amorphous thin oxides of industrial interest.
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- Type
- article
- Language
- en
- Landing Page
- https://doi.org/10.3390/ma15062144
- https://www.mdpi.com/1996-1944/15/6/2144/pdf?version=1647773863
- OA Status
- gold
- Cited By
- 6
- References
- 16
- Related Works
- 10
- OpenAlex ID
- https://openalex.org/W4221115315
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https://openalex.org/W4221115315Canonical identifier for this work in OpenAlex
- DOI
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https://doi.org/10.3390/ma15062144Digital Object Identifier
- Title
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Capabilities of Grazing Incidence X-ray Diffraction in the Investigation of Amorphous Mixed Oxides with Variable CompositionWork title
- Type
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articleOpenAlex work type
- Language
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enPrimary language
- Publication year
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2022Year of publication
- Publication date
-
2022-03-15Full publication date if available
- Authors
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Elisabetta Achilli, Filippo Annoni, N. Armani, M. Patrini, Marina Cornelli, Leonardo Celada, Melanie Micali, A. Terrasi, Paolo Ghigna, Gianluca TimòList of authors in order
- Landing page
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https://doi.org/10.3390/ma15062144Publisher landing page
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https://www.mdpi.com/1996-1944/15/6/2144/pdf?version=1647773863Direct link to full text PDF
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YesWhether a free full text is available
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goldOpen access status per OpenAlex
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https://www.mdpi.com/1996-1944/15/6/2144/pdf?version=1647773863Direct OA link when available
- Concepts
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Amorphous solid, Materials science, Diffraction, Scattering, Analytical Chemistry (journal), Chemical composition, Optics, Sputter deposition, Sputtering, Thin film, Crystallography, Nanotechnology, Physics, Chemistry, Thermodynamics, ChromatographyTop concepts (fields/topics) attached by OpenAlex
- Cited by
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6Total citation count in OpenAlex
- Citations by year (recent)
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2025: 1, 2024: 4, 2023: 1Per-year citation counts (last 5 years)
- References (count)
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16Number of works referenced by this work
- Related works (count)
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10Other works algorithmically related by OpenAlex
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