Comparative examination of the physical parameters of the sol gel produced compounds La0.5Ag0.1Ca0.4MnO3 and La0.6Ca0.3Ag0.1MnO3 Article Swipe
Mohammed Rasheed
,
N. Assoudi
,
A. Chaabani
,
I. Walha
,
E. Dhahri
,
R. Barillé
·
YOU?
·
· 2022
· Open Access
·
· DOI: https://doi.org/10.21203/rs.3.rs-1490041/v1
YOU?
·
· 2022
· Open Access
·
· DOI: https://doi.org/10.21203/rs.3.rs-1490041/v1
In this paper, the physical characteristics of La 0.5 Ag 0.1 Ca 0.4 MnO 3 and La 0.6 Ca 0.3 Ag 0.1 MnO 3 compounds have been studied. Structural analysis by XRD showed that both samples crystallize in an orthorhombic structure. For the La 0.5 Ag 0.1 Ca 0.4 MnO 3 sample it can be seen that there are two bands: the first is due to the stretching Mn-O bond the υ S vibration mode, relates to the internal motion of a length-changing Mn-O, whereas the second corresponds to the υ b bonding mode, which is sensitive to a change in the Mn-O-Mn angle. For the compound La 0.6 Ca 0.3 Ag 0.1 MnO 3 the υ b band is absent. The magnetic measurements show that the two compounds have a single transition from the PM state to the FM state with an increase in the Curie transition temperature T c for the compound La 0.6 Ca 0.3 Ag 0.1 MnO 3 . Similarly, the substitution of silver in calcium increases the value of the magnetization at low temperature. We also studied the magnetocaloric effect of our compounds. This study shows a significant change in magnetic entropy ΔS M that took place around their magnetic transition temperatures T c . Under the influence of a 5 T magnetic field. The largest fluctuation in magnetic entropy is in the order of -8.67 J/kg.K for the compound La 0.6 Ca 0.3 Ag 0.1 MnO 3 this value is considered significant. The magnetocaloric results indicate that the compound La 0.6 Ca 0.3 Ag 0.1 MnO 3 is the best sample which has a large RCP which suggests its good candidate in the field of magnetic cold. Based on the Banarjee criterion and Landau theory, a second-order transition is observed for both samples in the vicinity of the Curie transition T C . The experimentally obtained value of ΔS M is smaller than the theoretically calculated one, which proves that the transition is an unconventional transition even under the influence of a 5 T magnetic field.
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- Type
- preprint
- Language
- en
- Landing Page
- https://doi.org/10.21203/rs.3.rs-1490041/v1
- https://www.researchsquare.com/article/rs-1490041/latest.pdf
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- Title
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Comparative examination of the physical parameters of the sol gel produced compounds La0.5Ag0.1Ca0.4MnO3 and La0.6Ca0.3Ag0.1MnO3Work title
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preprintOpenAlex work type
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enPrimary language
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2022Year of publication
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2022-03-31Full publication date if available
- Authors
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Mohammed Rasheed, N. Assoudi, A. Chaabani, I. Walha, E. Dhahri, R. BarilléList of authors in order
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https://doi.org/10.21203/rs.3.rs-1490041/v1Publisher landing page
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https://www.researchsquare.com/article/rs-1490041/latest.pdfDirect link to full text PDF
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YesWhether a free full text is available
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greenOpen access status per OpenAlex
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Materials scienceTop concepts (fields/topics) attached by OpenAlex
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0Total citation count in OpenAlex
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| abstract_inverted_index.angle. | 104 |
| abstract_inverted_index.around | 203 |
| abstract_inverted_index.bands: | 61 |
| abstract_inverted_index.change | 100, 194 |
| abstract_inverted_index.effect | 185 |
| abstract_inverted_index.field. | 219, 342 |
| abstract_inverted_index.motion | 80 |
| abstract_inverted_index.paper, | 3 |
| abstract_inverted_index.proves | 325 |
| abstract_inverted_index.sample | 52, 267 |
| abstract_inverted_index.second | 87 |
| abstract_inverted_index.showed | 33 |
| abstract_inverted_index.silver | 168 |
| abstract_inverted_index.single | 132 |
| abstract_inverted_index.Mn-O-Mn | 103 |
| abstract_inverted_index.absent. | 121 |
| abstract_inverted_index.bonding | 93 |
| abstract_inverted_index.calcium | 170 |
| abstract_inverted_index.entropy | 197, 225 |
| abstract_inverted_index.largest | 221 |
| abstract_inverted_index.relates | 76 |
| abstract_inverted_index.results | 251 |
| abstract_inverted_index.samples | 36, 299 |
| abstract_inverted_index.smaller | 318 |
| abstract_inverted_index.studied | 182 |
| abstract_inverted_index.theory, | 291 |
| abstract_inverted_index.whereas | 85 |
| abstract_inverted_index.Abstract | 0 |
| abstract_inverted_index.Banarjee | 287 |
| abstract_inverted_index.analysis | 30 |
| abstract_inverted_index.compound | 107, 154, 235, 255 |
| abstract_inverted_index.increase | 144 |
| abstract_inverted_index.indicate | 252 |
| abstract_inverted_index.internal | 79 |
| abstract_inverted_index.magnetic | 123, 196, 205, 218, 224, 282, 341 |
| abstract_inverted_index.observed | 296 |
| abstract_inverted_index.obtained | 312 |
| abstract_inverted_index.physical | 5 |
| abstract_inverted_index.studied. | 28 |
| abstract_inverted_index.suggests | 274 |
| abstract_inverted_index.vicinity | 302 |
| abstract_inverted_index.candidate | 277 |
| abstract_inverted_index.compounds | 25, 129 |
| abstract_inverted_index.criterion | 288 |
| abstract_inverted_index.increases | 171 |
| abstract_inverted_index.influence | 213, 336 |
| abstract_inverted_index.sensitive | 97 |
| abstract_inverted_index.vibration | 74 |
| abstract_inverted_index.Similarly, | 164 |
| abstract_inverted_index.Structural | 29 |
| abstract_inverted_index.calculated | 322 |
| abstract_inverted_index.compounds. | 188 |
| abstract_inverted_index.considered | 247 |
| abstract_inverted_index.stretching | 68 |
| abstract_inverted_index.structure. | 41 |
| abstract_inverted_index.transition | 133, 148, 206, 294, 306, 328, 332 |
| abstract_inverted_index.corresponds | 88 |
| abstract_inverted_index.crystallize | 37 |
| abstract_inverted_index.fluctuation | 222 |
| abstract_inverted_index.significant | 193 |
| abstract_inverted_index.temperature | 149 |
| abstract_inverted_index.measurements | 124 |
| abstract_inverted_index.orthorhombic | 40 |
| abstract_inverted_index.second-order | 293 |
| abstract_inverted_index.significant. | 248 |
| abstract_inverted_index.substitution | 166 |
| abstract_inverted_index.temperature. | 179 |
| abstract_inverted_index.temperatures | 207 |
| abstract_inverted_index.magnetization | 176 |
| abstract_inverted_index.theoretically | 321 |
| abstract_inverted_index.experimentally | 311 |
| abstract_inverted_index.magnetocaloric | 184, 250 |
| abstract_inverted_index.unconventional | 331 |
| abstract_inverted_index.characteristics | 6 |
| abstract_inverted_index.length-changing | 83 |
| cited_by_percentile_year | |
| countries_distinct_count | 3 |
| institutions_distinct_count | 6 |
| citation_normalized_percentile.value | 0.01573233 |
| citation_normalized_percentile.is_in_top_1_percent | False |
| citation_normalized_percentile.is_in_top_10_percent | False |