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Suhui Liu , Xiaomin Li , Xiaoqing Wang , Ye Li , Feifei Zhang , Libo Li , Jinping Li , Jiangfeng Yang ·

YOU? · · 2024 · Open Access · · DOI: https://doi.org/10.1021/cbe.3c00037

Titanium (Ti)-based metal-organic frameworks (Ti-MOFs) have attracted intensive research attention due to their low toxicity and high abundance of titanium. However, limited by the high reactivity of titanium species in the reaction system, the construction of Ti-MOFs still faces great challenges. Herein, we successfully introduced Ti into MOF-74 using a one-pot method. Powder X-ray diffraction (PXRD) combined with X-ray photoelectron spectroscopy (XPS) and inductively coupled plasma (ICP) spectroscopy confirmed that the Ti(IV) ions were uniformly inserted into the MOF-74 structure. Our scanning electron microscopy (SEM)/energy-dispersive spectrometry (EDS) analysis showed that the Ti content was up to 44% with good sample homogeneity. The adsorption selectivity of Ti_0.44/Ni_0.56-MOF-74 at 1.0 bar and 298 K for C₂H₂/C₂H₄ and C₂H₂/CO₂ (50/50, v/v) mixtures was 4.9 and 6.8, respectively, which are higher than that of pristine Ni-MOF-74. The results of our breakthrough simulation experiments revealed that the adsorption and separation performances of Ti_0.44/Ni_0.56-MOF-74 were greatly improved. This study provided insights for the construction of Ti-based bimetallic MOFs used for the separation of light hydrocarbons.

Related Topics

Bimetallic Strip

X-Ray Photoelectron Spectroscopy

Titanium

Materials Science

Scanning Electron Microscope

$Powder Diffraction$

Energy-Dispersive X-Ray Spectroscopy

Metal–Organic Framework

Concepts

Bimetallic strip X-ray photoelectron spectroscopy Titanium Materials science Scanning electron microscope Adsorption Metal Reactivity (psychology) Powder diffraction Selectivity Spectroscopy Energy-dispersive X-ray spectroscopy Metal-organic framework Analytical Chemistry (journal) Chemical engineering Nuclear chemistry Catalysis Crystallography Metallurgy Physical chemistry Chemistry Organic chemistry Composite material Medicine Pathology Quantum mechanics Alternative medicine Physics Engineering

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Type: article
Language: en
Landing Page: https://doi.org/10.1021/cbe.3c00037
PDF: https://pubs.acs.org/doi/pdf/10.1021/cbe.3c00037
OA Status: diamond
Cited By: 8
References: 45
Related Works: 10
OpenAlex ID: https://openalex.org/W4390590954

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OpenAlex ID: https://openalex.org/W4390590954

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DOI: https://doi.org/10.1021/cbe.3c00037

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Title: Construction of a Ti-Based Bimetallic Metal–Organic Framework Using a One-Pot Method for Efficient C₂H₂/C₂H₄ and C₂H₂/CO₂ Separation

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Type: article

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Language: en

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Publication year: 2024

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Publication date: 2024-01-04

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Authors: Suhui Liu, Xiaomin Li, Xiaoqing Wang, Ye Li, Feifei Zhang, Libo Li, Jinping Li, Jiangfeng Yang

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Landing page: https://doi.org/10.1021/cbe.3c00037

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PDF URL: https://pubs.acs.org/doi/pdf/10.1021/cbe.3c00037

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Concepts: Bimetallic strip, X-ray photoelectron spectroscopy, Titanium, Materials science, Scanning electron microscope, Adsorption, Metal, Reactivity (psychology), Powder diffraction, Selectivity, Spectroscopy, Energy-dispersive X-ray spectroscopy, Metal-organic framework, Analytical Chemistry (journal), Chemical engineering, Nuclear chemistry, Catalysis, Crystallography, Metallurgy, Physical chemistry, Chemistry, Organic chemistry, Composite material, Medicine, Pathology, Quantum mechanics, Alternative medicine, Physics, Engineering

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Cited by: 8

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Citations by year (recent): 2025: 5, 2024: 3

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References (count): 45

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Related works (count): 10

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Construction of a Ti-Based Bimetallic Metal–Organic Framework Using a One-Pot Method for Efficient C2H2/C2H4 and C2H2/CO2 Separation Article Swipe

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Construction of a Ti-Based Bimetallic Metal–Organic Framework Using a One-Pot Method for Efficient C₂H₂/C₂H₄ and C₂H₂/CO₂ Separation Article Swipe