Depth profiling of W Ta based fusion-relevant samples using picosecond laser ablation Article Swipe
Shweta Soni
,
Sahithya Atikukke
,
Matej Veis
,
Nima Bolouki
,
Pavol Ďurina
,
Pavel Dvořák
,
Martina Mrkvičková
,
E. Grigore
,
P. Veis
·
YOU?
·
· 2024
· Open Access
·
· DOI: https://doi.org/10.1016/j.sab.2024.106930
YOU?
·
· 2024
· Open Access
·
· DOI: https://doi.org/10.1016/j.sab.2024.106930
This study presents a detailed picosecond LIBS analysis of WTa coatings on Molybdenum substrate with varying layer thicknesses using ps-LIBS for fusion relevant applications. Ps-LIBS is performed on three WTa layers; two with deuterium (∼7μm thickness) and one without deuterium (∼1μm thickness). The LIBS measurements are conducted under argon gas flow at 5±0.2 mbar pressure with different laser pulse energies (1 mJ, 3 mJ) and 100 spectra are recorded consecutively at one spot on the sample for different set of gate delay/gate width (200/200 ns, 300/300 ns, 450/450 ns). The obtained LIBS and Glow-Discharge Optical Emission Spectroscopy (GDOES) depth profiles are compared with the confocal microscopic measurements showing good agreement. Additionally, the ablation rate and layer thickness are calculated for different experimental conditions. The Calibration-Free LIBS approach is used for elemental analysis and the results are compared with GDOES results. The capability of ps-LIBS to quantify Ta in WTa alloy is explored for 2 at.% of Ta. However, due to higher ablation rate of laser and thin coating in WTaD sample, the layer is irradiated in few laser pulse and therefore, CF-LIBS analysis is not performed for it.
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- Type
- article
- Language
- en
- Landing Page
- https://doi.org/10.1016/j.sab.2024.106930
- OA Status
- hybrid
- References
- 36
- Related Works
- 10
- OpenAlex ID
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All OpenAlex metadata
Raw OpenAlex JSON
- OpenAlex ID
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https://openalex.org/W4395664220Canonical identifier for this work in OpenAlex
- DOI
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https://doi.org/10.1016/j.sab.2024.106930Digital Object Identifier
- Title
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Depth profiling of W Ta based fusion-relevant samples using picosecond laser ablationWork title
- Type
-
articleOpenAlex work type
- Language
-
enPrimary language
- Publication year
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2024Year of publication
- Publication date
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2024-04-26Full publication date if available
- Authors
-
Shweta Soni, Sahithya Atikukke, Matej Veis, Nima Bolouki, Pavol Ďurina, Pavel Dvořák, Martina Mrkvičková, E. Grigore, P. VeisList of authors in order
- Landing page
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https://doi.org/10.1016/j.sab.2024.106930Publisher landing page
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YesWhether a free full text is available
- OA status
-
hybridOpen access status per OpenAlex
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https://doi.org/10.1016/j.sab.2024.106930Direct OA link when available
- Concepts
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Materials science, Picosecond, Laser ablation, Analytical Chemistry (journal), Laser-induced breakdown spectroscopy, Ablation, Argon, Laser, Deuterium, Coating, Optics, Chemistry, Nanotechnology, Atomic physics, Aerospace engineering, Organic chemistry, Physics, Chromatography, EngineeringTop concepts (fields/topics) attached by OpenAlex
- Cited by
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0Total citation count in OpenAlex
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36Number of works referenced by this work
- Related works (count)
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10Other works algorithmically related by OpenAlex
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