Design and development of an electroanalytical sensor based on molecularly imprinted polyaniline for detection of thyroxine Article Swipe
Deepanmol Singh
,
Souradeep Roy
,
Neeraj Mahindroo
,
Ashish Mathur
·
YOU?
·
· 2023
· Open Access
·
· DOI: https://doi.org/10.21203/rs.3.rs-2810843/v1
YOU?
·
· 2023
· Open Access
·
· DOI: https://doi.org/10.21203/rs.3.rs-2810843/v1
Hypothyroidism and hyperthyroidism are one of the most frequently observed endocrine disorders in the world. Failure to undergo timely diagnosis and treatment often results in life-threatening events such as arrythmia, hypertension and cardiac arrest. Considering the various limitations of conventional diagnostic techniques, early, accurate and efficient diagnosis of these disorders is pivotal for their timely management. In the present work, a Molecularly Imprinted Polymer (MIP) based sensor is developed for the detection of thyroxine (T 4 ) – the key biomarker. This has been achieved by templating T 4 into polyaniline matrix supported on Indium Tin Oxide (ITO) coated glass electrodes. The chemical synthesis of polyaniline was done through oxidative polymerization and optimized using Response Surface Methodology (RSM). The optimum conditions for ultrasonication based extraction of T 4 from polyaniline matrix was 15min at 30°C with 75mM NaOH. The developed MIP based sensor was characterized using chromatographic, spectroscopic and electrochemical techniques. The sensor calibration was obtained within T 4 concentration range of 5pg/mL – 50pg/mL, with a calculated Limit of Detection (LoD) of7.96pM (6.16pg/mL). The developed MIP-based electroanalytical sensor was found to exhibit high degree of selectivity against various interferants, and thereby possessing huge prospects towards futuristic point-of-care applications.
Related Topics
Concepts
Polyaniline
Molecularly imprinted polymer
Detection limit
Materials science
Conductive polymer
Nanotechnology
Polymer
Polymerization
Selectivity
Chromatography
Chemistry
Catalysis
Composite material
Organic chemistry
Metadata
- Type
- preprint
- Language
- en
- Landing Page
- https://doi.org/10.21203/rs.3.rs-2810843/v1
- https://www.researchsquare.com/article/rs-2810843/latest.pdf
- OA Status
- green
- Cited By
- 4
- References
- 26
- Related Works
- 10
- OpenAlex ID
- https://openalex.org/W4365503886
All OpenAlex metadata
Raw OpenAlex JSON
- OpenAlex ID
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https://openalex.org/W4365503886Canonical identifier for this work in OpenAlex
- DOI
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https://doi.org/10.21203/rs.3.rs-2810843/v1Digital Object Identifier
- Title
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Design and development of an electroanalytical sensor based on molecularly imprinted polyaniline for detection of thyroxineWork title
- Type
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preprintOpenAlex work type
- Language
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enPrimary language
- Publication year
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2023Year of publication
- Publication date
-
2023-04-14Full publication date if available
- Authors
-
Deepanmol Singh, Souradeep Roy, Neeraj Mahindroo, Ashish MathurList of authors in order
- Landing page
-
https://doi.org/10.21203/rs.3.rs-2810843/v1Publisher landing page
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https://www.researchsquare.com/article/rs-2810843/latest.pdfDirect link to full text PDF
- Open access
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YesWhether a free full text is available
- OA status
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greenOpen access status per OpenAlex
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https://www.researchsquare.com/article/rs-2810843/latest.pdfDirect OA link when available
- Concepts
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Polyaniline, Molecularly imprinted polymer, Detection limit, Materials science, Conductive polymer, Nanotechnology, Polymer, Polymerization, Selectivity, Chromatography, Chemistry, Catalysis, Composite material, Organic chemistryTop concepts (fields/topics) attached by OpenAlex
- Cited by
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4Total citation count in OpenAlex
- Citations by year (recent)
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2025: 1, 2024: 2, 2023: 1Per-year citation counts (last 5 years)
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26Number of works referenced by this work
- Related works (count)
-
10Other works algorithmically related by OpenAlex
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| abstract_inverted_index.MIP | 141 |
| abstract_inverted_index.The | 102, 119, 139, 152, 175 |
| abstract_inverted_index.Tin | 96 |
| abstract_inverted_index.and | 2, 21, 32, 45, 112, 149, 191 |
| abstract_inverted_index.are | 4 |
| abstract_inverted_index.for | 53, 70, 122 |
| abstract_inverted_index.has | 83 |
| abstract_inverted_index.key | 80 |
| abstract_inverted_index.one | 5 |
| abstract_inverted_index.the | 7, 14, 36, 58, 71, 79 |
| abstract_inverted_index.was | 107, 132, 144, 155, 180 |
| abstract_inverted_index.– | 78, 164 |
| abstract_inverted_index.75mM | 137 |
| abstract_inverted_index.This | 82 |
| abstract_inverted_index.been | 84 |
| abstract_inverted_index.done | 108 |
| abstract_inverted_index.from | 129 |
| abstract_inverted_index.high | 184 |
| abstract_inverted_index.huge | 194 |
| abstract_inverted_index.into | 90 |
| abstract_inverted_index.most | 8 |
| abstract_inverted_index.such | 28 |
| abstract_inverted_index.with | 136, 166 |
| abstract_inverted_index.(ITO) | 98 |
| abstract_inverted_index.(LoD) | 172 |
| abstract_inverted_index.(MIP) | 65 |
| abstract_inverted_index.15min | 133 |
| abstract_inverted_index.30°C | 135 |
| abstract_inverted_index.Limit | 169 |
| abstract_inverted_index.NaOH. | 138 |
| abstract_inverted_index.Oxide | 97 |
| abstract_inverted_index.based | 66, 124, 142 |
| abstract_inverted_index.found | 181 |
| abstract_inverted_index.glass | 100 |
| abstract_inverted_index.often | 23 |
| abstract_inverted_index.range | 161 |
| abstract_inverted_index.their | 54 |
| abstract_inverted_index.these | 49 |
| abstract_inverted_index.using | 114, 146 |
| abstract_inverted_index.work, | 60 |
| abstract_inverted_index.(RSM). | 118 |
| abstract_inverted_index.5pg/mL | 163 |
| abstract_inverted_index.Indium | 95 |
| abstract_inverted_index.coated | 99 |
| abstract_inverted_index.degree | 185 |
| abstract_inverted_index.early, | 43 |
| abstract_inverted_index.events | 27 |
| abstract_inverted_index.matrix | 92, 131 |
| abstract_inverted_index.sensor | 67, 143, 153, 179 |
| abstract_inverted_index.timely | 19, 55 |
| abstract_inverted_index.within | 157 |
| abstract_inverted_index.world. | 15 |
| abstract_inverted_index.Failure | 16 |
| abstract_inverted_index.Polymer | 64 |
| abstract_inverted_index.Surface | 116 |
| abstract_inverted_index.against | 188 |
| abstract_inverted_index.arrest. | 34 |
| abstract_inverted_index.cardiac | 33 |
| abstract_inverted_index.exhibit | 183 |
| abstract_inverted_index.optimum | 120 |
| abstract_inverted_index.pivotal | 52 |
| abstract_inverted_index.present | 59 |
| abstract_inverted_index.results | 24 |
| abstract_inverted_index.thereby | 192 |
| abstract_inverted_index.through | 109 |
| abstract_inverted_index.towards | 196 |
| abstract_inverted_index.undergo | 18 |
| abstract_inverted_index.various | 37, 189 |
| abstract_inverted_index.50pg/mL, | 165 |
| abstract_inverted_index.Abstract | 0 |
| abstract_inverted_index.Response | 115 |
| abstract_inverted_index.accurate | 44 |
| abstract_inverted_index.achieved | 85 |
| abstract_inverted_index.chemical | 103 |
| abstract_inverted_index.observed | 10 |
| abstract_inverted_index.obtained | 156 |
| abstract_inverted_index.of7.96pM | 173 |
| abstract_inverted_index.Detection | 171 |
| abstract_inverted_index.Imprinted | 63 |
| abstract_inverted_index.MIP-based | 177 |
| abstract_inverted_index.detection | 72 |
| abstract_inverted_index.developed | 69, 140, 176 |
| abstract_inverted_index.diagnosis | 20, 47 |
| abstract_inverted_index.disorders | 12, 50 |
| abstract_inverted_index.efficient | 46 |
| abstract_inverted_index.endocrine | 11 |
| abstract_inverted_index.optimized | 113 |
| abstract_inverted_index.oxidative | 110 |
| abstract_inverted_index.prospects | 195 |
| abstract_inverted_index.supported | 93 |
| abstract_inverted_index.synthesis | 104 |
| abstract_inverted_index.thyroxine | 74 |
| abstract_inverted_index.treatment | 22 |
| abstract_inverted_index.arrythmia, | 30 |
| abstract_inverted_index.biomarker. | 81 |
| abstract_inverted_index.calculated | 168 |
| abstract_inverted_index.conditions | 121 |
| abstract_inverted_index.diagnostic | 41 |
| abstract_inverted_index.extraction | 125 |
| abstract_inverted_index.frequently | 9 |
| abstract_inverted_index.futuristic | 197 |
| abstract_inverted_index.possessing | 193 |
| abstract_inverted_index.templating | 87 |
| abstract_inverted_index.Considering | 35 |
| abstract_inverted_index.Methodology | 117 |
| abstract_inverted_index.Molecularly | 62 |
| abstract_inverted_index.calibration | 154 |
| abstract_inverted_index.electrodes. | 101 |
| abstract_inverted_index.limitations | 38 |
| abstract_inverted_index.management. | 56 |
| abstract_inverted_index.polyaniline | 91, 106, 130 |
| abstract_inverted_index.selectivity | 187 |
| abstract_inverted_index.techniques, | 42 |
| abstract_inverted_index.techniques. | 151 |
| abstract_inverted_index.(6.16pg/mL). | 174 |
| abstract_inverted_index.conventional | 40 |
| abstract_inverted_index.hypertension | 31 |
| abstract_inverted_index.applications. | 199 |
| abstract_inverted_index.characterized | 145 |
| abstract_inverted_index.concentration | 160 |
| abstract_inverted_index.interferants, | 190 |
| abstract_inverted_index.point-of-care | 198 |
| abstract_inverted_index.spectroscopic | 148 |
| abstract_inverted_index.Hypothyroidism | 1 |
| abstract_inverted_index.polymerization | 111 |
| abstract_inverted_index.electrochemical | 150 |
| abstract_inverted_index.hyperthyroidism | 3 |
| abstract_inverted_index.ultrasonication | 123 |
| abstract_inverted_index.chromatographic, | 147 |
| abstract_inverted_index.life-threatening | 26 |
| abstract_inverted_index.electroanalytical | 178 |
| cited_by_percentile_year.max | 96 |
| cited_by_percentile_year.min | 89 |
| countries_distinct_count | 1 |
| institutions_distinct_count | 4 |
| citation_normalized_percentile.value | 0.66861353 |
| citation_normalized_percentile.is_in_top_1_percent | False |
| citation_normalized_percentile.is_in_top_10_percent | False |