Detection and Characterization of TiO2 Nanomaterials in Sludge from Wastewater Treatment Plants of Chihuahua State, Mexico Article Swipe
Juan Reyes-Herrera
,
Damaris Acosta-Slane
,
Hiram Castillo‐Michel
,
A. Real
,
Katarina Vogel‐Mikuš
,
Federico Benetti
,
Marco Roman
,
Julie Villanova
,
María Cecilia Valles-Aragón
·
YOU?
·
· 2022
· Open Access
·
· DOI: https://doi.org/10.3390/nano12050744
YOU?
·
· 2022
· Open Access
·
· DOI: https://doi.org/10.3390/nano12050744
TiO2 nanoparticles (TiO2-NPs) have a wide range of industrial applications (paintings, sunscreens, food and cosmetics) and is one of the most intensively used nanomaterials worldwide. Leaching from commercial products TiO2-NPs are predicted to significantly accumulate in wastewater sludges, which are then often used as soil amendment. In this work, sludge samples from four wastewater treatment plants of the Chihuahua State in Mexico were obtained during spring and summer (2017). A comprehensive characterization study was performed by X-ray based (laboratory and synchrotron) techniques and electron microscopy. Ti was detected in all sludge samples (1810–2760 mg/kg) mainly as TiO2 particles ranging from 40 nm up to hundreds of nm. Micro-XANES data was analyzed by principal component analysis and linear combination fitting enabling the identification of three predominant Ti species: anatase, rutile and ilmenite. Micro-XANES from the smaller Ti particles was predominantly anatase (68% + 32% rutile), suggesting these TiO2-NPs originate from paintings and cosmetics. TEM imaging confirmed the presence of nanoscale Ti with smooth surface morphologies resembling engineered TiO2-NPs. The size and crystalline phase of TiO2-NPs in the sludge from this region suggest increased reactivity and potential toxicity to agro-systems. Further studies should be dedicated to evaluating this.
Related Topics
Concepts
Anatase
Rutile
Nanomaterials
Materials science
Wastewater
Characterization (materials science)
Nanoparticle
Leaching (pedology)
Environmental chemistry
Amendment
Chemical engineering
Nanotechnology
Chemistry
Environmental science
Environmental engineering
Photocatalysis
Soil water
Biochemistry
Engineering
Law
Soil science
Catalysis
Political science
Metadata
- Type
- article
- Language
- en
- Landing Page
- https://doi.org/10.3390/nano12050744
- https://www.mdpi.com/2079-4991/12/5/744/pdf?version=1645617054
- OA Status
- gold
- Cited By
- 11
- References
- 71
- Related Works
- 10
- OpenAlex ID
- https://openalex.org/W4213414797
All OpenAlex metadata
Raw OpenAlex JSON
- OpenAlex ID
-
https://openalex.org/W4213414797Canonical identifier for this work in OpenAlex
- DOI
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https://doi.org/10.3390/nano12050744Digital Object Identifier
- Title
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Detection and Characterization of TiO2 Nanomaterials in Sludge from Wastewater Treatment Plants of Chihuahua State, MexicoWork title
- Type
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articleOpenAlex work type
- Language
-
enPrimary language
- Publication year
-
2022Year of publication
- Publication date
-
2022-02-23Full publication date if available
- Authors
-
Juan Reyes-Herrera, Damaris Acosta-Slane, Hiram Castillo‐Michel, A. Real, Katarina Vogel‐Mikuš, Federico Benetti, Marco Roman, Julie Villanova, María Cecilia Valles-AragónList of authors in order
- Landing page
-
https://doi.org/10.3390/nano12050744Publisher landing page
- PDF URL
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https://www.mdpi.com/2079-4991/12/5/744/pdf?version=1645617054Direct link to full text PDF
- Open access
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YesWhether a free full text is available
- OA status
-
goldOpen access status per OpenAlex
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https://www.mdpi.com/2079-4991/12/5/744/pdf?version=1645617054Direct OA link when available
- Concepts
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Anatase, Rutile, Nanomaterials, Materials science, Wastewater, Characterization (materials science), Nanoparticle, Leaching (pedology), Environmental chemistry, Amendment, Chemical engineering, Nanotechnology, Chemistry, Environmental science, Environmental engineering, Photocatalysis, Soil water, Biochemistry, Engineering, Law, Soil science, Catalysis, Political scienceTop concepts (fields/topics) attached by OpenAlex
- Cited by
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11Total citation count in OpenAlex
- Citations by year (recent)
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2025: 4, 2024: 4, 2023: 1, 2022: 2Per-year citation counts (last 5 years)
- References (count)
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71Number of works referenced by this work
- Related works (count)
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10Other works algorithmically related by OpenAlex
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| abstract_inverted_index.Chihuahua | 58 |
| abstract_inverted_index.TiO2-NPs. | 166 |
| abstract_inverted_index.component | 113 |
| abstract_inverted_index.confirmed | 154 |
| abstract_inverted_index.dedicated | 192 |
| abstract_inverted_index.ilmenite. | 130 |
| abstract_inverted_index.increased | 181 |
| abstract_inverted_index.nanoscale | 158 |
| abstract_inverted_index.originate | 147 |
| abstract_inverted_index.paintings | 149 |
| abstract_inverted_index.particles | 97, 136 |
| abstract_inverted_index.performed | 74 |
| abstract_inverted_index.potential | 184 |
| abstract_inverted_index.predicted | 31 |
| abstract_inverted_index.principal | 112 |
| abstract_inverted_index.treatment | 54 |
| abstract_inverted_index.(TiO2-NPs) | 2 |
| abstract_inverted_index.accumulate | 34 |
| abstract_inverted_index.amendment. | 45 |
| abstract_inverted_index.commercial | 27 |
| abstract_inverted_index.cosmetics) | 14 |
| abstract_inverted_index.cosmetics. | 151 |
| abstract_inverted_index.engineered | 165 |
| abstract_inverted_index.evaluating | 194 |
| abstract_inverted_index.industrial | 8 |
| abstract_inverted_index.reactivity | 182 |
| abstract_inverted_index.resembling | 164 |
| abstract_inverted_index.suggesting | 144 |
| abstract_inverted_index.techniques | 81 |
| abstract_inverted_index.wastewater | 36, 53 |
| abstract_inverted_index.worldwide. | 24 |
| abstract_inverted_index.(laboratory | 78 |
| abstract_inverted_index.(paintings, | 10 |
| abstract_inverted_index.Micro-XANES | 107, 131 |
| abstract_inverted_index.combination | 117 |
| abstract_inverted_index.crystalline | 170 |
| abstract_inverted_index.intensively | 21 |
| abstract_inverted_index.microscopy. | 84 |
| abstract_inverted_index.predominant | 124 |
| abstract_inverted_index.sunscreens, | 11 |
| abstract_inverted_index.(1810–2760 | 92 |
| abstract_inverted_index.applications | 9 |
| abstract_inverted_index.morphologies | 163 |
| abstract_inverted_index.synchrotron) | 80 |
| abstract_inverted_index.agro-systems. | 187 |
| abstract_inverted_index.comprehensive | 70 |
| abstract_inverted_index.nanomaterials | 23 |
| abstract_inverted_index.nanoparticles | 1 |
| abstract_inverted_index.predominantly | 138 |
| abstract_inverted_index.significantly | 33 |
| abstract_inverted_index.identification | 121 |
| abstract_inverted_index.characterization | 71 |
| cited_by_percentile_year.max | 98 |
| cited_by_percentile_year.min | 89 |
| corresponding_author_ids | https://openalex.org/A5004215048 |
| countries_distinct_count | 5 |
| institutions_distinct_count | 9 |
| corresponding_institution_ids | https://openalex.org/I142652706 |
| sustainable_development_goals[0].id | https://metadata.un.org/sdg/6 |
| sustainable_development_goals[0].score | 0.8600000143051147 |
| sustainable_development_goals[0].display_name | Clean water and sanitation |
| citation_normalized_percentile.value | 0.68768694 |
| citation_normalized_percentile.is_in_top_1_percent | False |
| citation_normalized_percentile.is_in_top_10_percent | False |