Development of electrodeposited nanostructural poly (o-aminophenol) coating as a solid phase microextraction fiber for determination of bisphenol A Article Swipe

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Mohammad Saraji , Bahman Farajmand , Esmaeil Heydari Bafrouei ·

YOU? · · 2021 · Open Access · · DOI: https://doi.org/10.24200/amecj.v4.i02.142

In this research nanostructural poly (o-aminophenol) was synthesized by electropolymerization and used for solid phase microextraction procedure (SPME). Thin film of Poly (o-aminophenol) (4 µm thickness) was shaped by sweep potential for 45 min on the surface of stainless steel wire. Polymer was synthesized by potentiostat procedure too. Prepared polymer by sweep potential procedure showed nanostructures on the surface. Acetic anhydride was employed for derivatization of bisphenol A (BPh-A) and analysis of acetylated BPh-A was utilized by gas chromatography-flame ionization detector (GC-FID). Affecting parameters on derivatization and extraction such as amount of acetic anhydride, stirring rate, temperature, ionic strength and extraction time were optimized. The limit of detection (LOD) and relative standard divisions (RSDs%) were achieved 0.6 µgL-1 and less than 6.8%, respectively under optimized conditions. Finally proposed method was used for extraction of bisphenol A from leaching of baby and drinking water bottles. Relative recovery was achieved 98% for leaching from drinking bottle. In leaching from plastic baby bottle, bisphenol A (BPh-A) was detected in the range 5–15 µg L-1.

Related Topics

Flame Ionization Detector

Extraction (Chemistry)

Chromatography

Chemistry

Gas Chromatography–Mass Spectrometry

High-Performance Liquid Chromatography

Composite Material

Organic Chemistry

Mass Spectrometry

Environmental Science

Concepts

Solid-phase microextraction Bisphenol A Derivatization Acetic anhydride Detection limit Leaching (pedology) Materials science Gas chromatography Polymer Flame ionization detector Extraction (chemistry) Chromatography Chemistry Gas chromatography–mass spectrometry High-performance liquid chromatography Composite material Organic chemistry Epoxy Mass spectrometry Catalysis Environmental science Soil science Soil water

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Type: article
Language: en
Landing Page: https://doi.org/10.24200/amecj.v4.i02.142
PDF: http://journal.amecj.com/index.php/AMECJ-01/article/download/142/319
OA Status: hybrid
Cited By: 5
References: 38
Related Works: 10
OpenAlex ID: https://openalex.org/W3181405185

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OpenAlex ID: https://openalex.org/W3181405185

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DOI: https://doi.org/10.24200/amecj.v4.i02.142

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Title: Development of electrodeposited nanostructural poly (o-aminophenol) coating as a solid phase microextraction fiber for determination of bisphenol A

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Type: article

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Language: en

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Publication year: 2021

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Publication date: 2021-06-01

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Authors: Mohammad Saraji, Bahman Farajmand, Esmaeil Heydari Bafrouei

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Landing page: https://doi.org/10.24200/amecj.v4.i02.142

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PDF URL: https://journal.amecj.com/index.php/AMECJ-01/article/download/142/319

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OA status: hybrid

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Concepts: Solid-phase microextraction, Bisphenol A, Derivatization, Acetic anhydride, Detection limit, Leaching (pedology), Materials science, Gas chromatography, Polymer, Flame ionization detector, Extraction (chemistry), Chromatography, Chemistry, Gas chromatography–mass spectrometry, High-performance liquid chromatography, Composite material, Organic chemistry, Epoxy, Mass spectrometry, Catalysis, Environmental science, Soil science, Soil water

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Cited by: 5

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Citations by year (recent): 2023: 3, 2022: 2

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References (count): 38

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Related works (count): 10

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abstract_inverted_index.on	34, 56, 84
abstract_inverted_index.0.6	116
abstract_inverted_index.98%	148
abstract_inverted_index.The	104
abstract_inverted_index.and	10, 69, 86, 99, 109, 118, 140
abstract_inverted_index.for	12, 31, 63, 131, 149
abstract_inverted_index.gas	77
abstract_inverted_index.min	33
abstract_inverted_index.the	35, 57, 166
abstract_inverted_index.was	6, 26, 42, 61, 74, 129, 146, 163
abstract_inverted_index.µg	169
abstract_inverted_index.µm	24
abstract_inverted_index.L-1.	170
abstract_inverted_index.Poly	21
abstract_inverted_index.Thin	18
abstract_inverted_index.baby	139, 158
abstract_inverted_index.film	19
abstract_inverted_index.from	136, 151, 156
abstract_inverted_index.less	119
abstract_inverted_index.poly	4
abstract_inverted_index.such	88
abstract_inverted_index.than	120
abstract_inverted_index.this	1
abstract_inverted_index.time	101
abstract_inverted_index.too.	47
abstract_inverted_index.used	11, 130
abstract_inverted_index.were	102, 114
abstract_inverted_index.&nbsp	171
abstract_inverted_index.(LOD)	108
abstract_inverted_index.6.8%,	121
abstract_inverted_index.BPh-A	73
abstract_inverted_index.ionic	97
abstract_inverted_index.limit	105
abstract_inverted_index.phase	14
abstract_inverted_index.range	167
abstract_inverted_index.rate,	95
abstract_inverted_index.solid	13
abstract_inverted_index.steel	39
abstract_inverted_index.sweep	29, 51
abstract_inverted_index.under	123
abstract_inverted_index.water	142
abstract_inverted_index.wire.	40
abstract_inverted_index.5–15	168
abstract_inverted_index.Acetic	59
abstract_inverted_index.acetic	92
abstract_inverted_index.amount	90
abstract_inverted_index.method	128
abstract_inverted_index.shaped	27
abstract_inverted_index.showed	54
abstract_inverted_index.µgL-1	117
abstract_inverted_index.(BPh-A)	68, 162
abstract_inverted_index.(RSDs%)	113
abstract_inverted_index.(SPME).	17
abstract_inverted_index.Finally	126
abstract_inverted_index.Polymer	41
abstract_inverted_index.bottle,	159
abstract_inverted_index.bottle.	153
abstract_inverted_index.plastic	157
abstract_inverted_index.polymer	49
abstract_inverted_index.surface	36
abstract_inverted_index.Prepared	48
abstract_inverted_index.Relative	144
abstract_inverted_index.achieved	115, 147
abstract_inverted_index.analysis	70
abstract_inverted_index.bottles.	143
abstract_inverted_index.detected	164
abstract_inverted_index.detector	80
abstract_inverted_index.drinking	141, 152
abstract_inverted_index.employed	62
abstract_inverted_index.leaching	137, 150, 155
abstract_inverted_index.proposed	127
abstract_inverted_index.recovery	145
abstract_inverted_index.relative	110
abstract_inverted_index.research	2
abstract_inverted_index.standard	111
abstract_inverted_index.stirring	94
abstract_inverted_index.strength	98
abstract_inverted_index.surface.	58
abstract_inverted_index.utilized	75
abstract_inverted_index.(GC-FID).	81
abstract_inverted_index.Affecting	82
abstract_inverted_index.anhydride	60
abstract_inverted_index.bisphenol	66, 134, 160
abstract_inverted_index.detection	107
abstract_inverted_index.divisions	112
abstract_inverted_index.optimized	124
abstract_inverted_index.potential	30, 52
abstract_inverted_index.procedure	16, 46, 53
abstract_inverted_index.stainless	38
abstract_inverted_index.acetylated	72
abstract_inverted_index.anhydride,	93
abstract_inverted_index.extraction	87, 100, 132
abstract_inverted_index.ionization	79
abstract_inverted_index.optimized.	103
abstract_inverted_index.parameters	83
abstract_inverted_index.thickness)	25
abstract_inverted_index.conditions.	125
abstract_inverted_index.synthesized	7, 43
abstract_inverted_index.potentiostat	45
abstract_inverted_index.respectively	122
abstract_inverted_index.temperature,	96
abstract_inverted_index.derivatization	64, 85
abstract_inverted_index.nanostructural	3
abstract_inverted_index.nanostructures	55
abstract_inverted_index.(o-aminophenol)	5, 22
abstract_inverted_index.microextraction	15
abstract_inverted_index.chromatography-flame	78
abstract_inverted_index.electropolymerization	9
cited_by_percentile_year.max	97
cited_by_percentile_year.min	94
countries_distinct_count	1
institutions_distinct_count	3
sustainable_development_goals[0].id	https://metadata.un.org/sdg/6
sustainable_development_goals[0].score	0.75
sustainable_development_goals[0].display_name	Clean water and sanitation
citation_normalized_percentile.value	0.62059357
citation_normalized_percentile.is_in_top_1_percent	False
citation_normalized_percentile.is_in_top_10_percent	False