Development of highly stable conductive multiwalled carbon nanotube ink using covalent and non-covalent functionalization for electrochemical sensors Article Swipe
Ana Elisa Ferreira Oliveira
,
Arnaldo César Pereira
,
Lucas Franco Ferreira
·
YOU?
·
· 2021
· Open Access
·
· DOI: https://doi.org/10.5599/jese.1134
YOU?
·
· 2021
· Open Access
·
· DOI: https://doi.org/10.5599/jese.1134
The purpose of this work was the fabrication of a conductive carbon nanotube (CNT) ink. The proposed CNT ink remained remarkably stable over several months. The method includes combining the covalent and non-covalent functionalization, resulting in ink that exhibits excellent storage stability. The covalent functionalization was performed in the acid medium using H2SO4 and HNO3, while the non-covalent functionalization used sodium dodecyl sulfate (SDS) and ultrasonication. The materials were characterized by Fourier transform infrared spectroscopy (FTIR), scanning electron microscopy (SEM), electrochemical impedance spectroscopy (EIS), and cyclic voltammetry (CV). FTIR and SEM confirmed that at the non-covalent functionalization, SDS was successfully adsorbed on the f-CNT surface, while at the covalent functionalization, the functional groups (-COOH, C=O and -OH) were inserted into the CNT surface. Voltammetry and EIS indicated that SDS in the presence of functional groups facilitates electron transfer by improved electrical conductivity. The final product was a well-dispersed CNT ink with an average ohmic resistance of 18.62 kΩ. This indicates that CNT ink can be used in the fabrication of electrochemical sensors.
Related Topics
Concepts
Surface modification
Covalent bond
Cyclic voltammetry
Fourier transform infrared spectroscopy
Materials science
Carbon nanotube
Chemical engineering
Dielectric spectroscopy
Chemical modification
Scanning electron microscope
Nanotechnology
Electrochemistry
Polymer chemistry
Chemistry
Organic chemistry
Composite material
Electrode
Engineering
Physical chemistry
Metadata
- Type
- article
- Language
- en
- Landing Page
- https://doi.org/10.5599/jese.1134
- https://pub.iapchem.org/ojs/index.php/JESE/article/download/1134/1368
- OA Status
- diamond
- Cited By
- 4
- References
- 82
- Related Works
- 10
- OpenAlex ID
- https://openalex.org/W4200409010
All OpenAlex metadata
Raw OpenAlex JSON
- OpenAlex ID
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https://openalex.org/W4200409010Canonical identifier for this work in OpenAlex
- DOI
-
https://doi.org/10.5599/jese.1134Digital Object Identifier
- Title
-
Development of highly stable conductive multiwalled carbon nanotube ink using covalent and non-covalent functionalization for electrochemical sensorsWork title
- Type
-
articleOpenAlex work type
- Language
-
enPrimary language
- Publication year
-
2021Year of publication
- Publication date
-
2021-12-02Full publication date if available
- Authors
-
Ana Elisa Ferreira Oliveira, Arnaldo César Pereira, Lucas Franco FerreiraList of authors in order
- Landing page
-
https://doi.org/10.5599/jese.1134Publisher landing page
- PDF URL
-
https://pub.iapchem.org/ojs/index.php/JESE/article/download/1134/1368Direct link to full text PDF
- Open access
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YesWhether a free full text is available
- OA status
-
diamondOpen access status per OpenAlex
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https://pub.iapchem.org/ojs/index.php/JESE/article/download/1134/1368Direct OA link when available
- Concepts
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Surface modification, Covalent bond, Cyclic voltammetry, Fourier transform infrared spectroscopy, Materials science, Carbon nanotube, Chemical engineering, Dielectric spectroscopy, Chemical modification, Scanning electron microscope, Nanotechnology, Electrochemistry, Polymer chemistry, Chemistry, Organic chemistry, Composite material, Electrode, Engineering, Physical chemistryTop concepts (fields/topics) attached by OpenAlex
- Cited by
-
4Total citation count in OpenAlex
- Citations by year (recent)
-
2024: 1, 2022: 3Per-year citation counts (last 5 years)
- References (count)
-
82Number of works referenced by this work
- Related works (count)
-
10Other works algorithmically related by OpenAlex
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| publication_date | 2021-12-02 |
| publication_year | 2021 |
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