Direct Synthesis of CuPd Icosahedra Supercrystals studied by in situ X-ray Scattering Article Swipe
Davide Derelli
,
Kilian Frank
,
Lukas Grote
,
Federica Mancini
,
Ann‐Christin Dippel
,
Olof Gutowski
,
Bert Nickel
,
Dorota Koziej
·
YOU?
·
· 2023
· Open Access
·
· DOI: https://doi.org/10.26434/chemrxiv-2023-shx8j
YOU?
·
· 2023
· Open Access
·
· DOI: https://doi.org/10.26434/chemrxiv-2023-shx8j
Nanocrystal self-assembly into supercrystals provides a versatile platform for creating novel materials and devices with tailored properties. While common self-assembly strategies imply the use of purified nanoparticles after synthesis, conversion of chemical precursors directly into nanocrystals and then supercrystals in simple procedures has been rarely reported. Here we study the nucleation and growth of CuPd icosahedra and their consecutive assembly into extended closed-packed face-centered cubic (fcc) supercrystals. To this end, we simultaneously and in situ measure X-ray total scattering with pair-distribution function analysis (TS-PDF) and small-angle X-ray scattering (SAXS). We find that the supercrystals formation is preceded by an intermediate dense phase of nanocrystals displaying short-range order (SRO). We further show that the organization of oleic acid/oleylamine surfactants into lamellar structures likely drives the emergence of the SRO phase and later of the supercrystals by creating an excluded volume to particle diffusion. The supercrystal formation as well as their disassembly are triggered by temperature. Our study demonstrates that depletion effects can be crucial in the direct synthesis of supercrystals. We also provide a general approach to investigate novel preparation routes of supercrystals in situ and across several length scales via X-ray scattering.
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- Type
- preprint
- Language
- en
- Landing Page
- https://doi.org/10.26434/chemrxiv-2023-shx8j
- https://chemrxiv.org/engage/api-gateway/chemrxiv/assets/orp/resource/item/656dea18cf8b3c3cd7c3ed3a/original/direct-synthesis-of-cu-pd-icosahedra-supercrystals-studied-by-in-situ-x-ray-scattering.pdf
- OA Status
- gold
- Cited By
- 2
- References
- 44
- Related Works
- 10
- OpenAlex ID
- https://openalex.org/W4389396557
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Raw OpenAlex JSON
- OpenAlex ID
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https://openalex.org/W4389396557Canonical identifier for this work in OpenAlex
- DOI
-
https://doi.org/10.26434/chemrxiv-2023-shx8jDigital Object Identifier
- Title
-
Direct Synthesis of CuPd Icosahedra Supercrystals studied by in situ X-ray ScatteringWork title
- Type
-
preprintOpenAlex work type
- Language
-
enPrimary language
- Publication year
-
2023Year of publication
- Publication date
-
2023-12-06Full publication date if available
- Authors
-
Davide Derelli, Kilian Frank, Lukas Grote, Federica Mancini, Ann‐Christin Dippel, Olof Gutowski, Bert Nickel, Dorota KoziejList of authors in order
- Landing page
-
https://doi.org/10.26434/chemrxiv-2023-shx8jPublisher landing page
- PDF URL
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https://chemrxiv.org/engage/api-gateway/chemrxiv/assets/orp/resource/item/656dea18cf8b3c3cd7c3ed3a/original/direct-synthesis-of-cu-pd-icosahedra-supercrystals-studied-by-in-situ-x-ray-scattering.pdfDirect link to full text PDF
- Open access
-
YesWhether a free full text is available
- OA status
-
goldOpen access status per OpenAlex
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https://chemrxiv.org/engage/api-gateway/chemrxiv/assets/orp/resource/item/656dea18cf8b3c3cd7c3ed3a/original/direct-synthesis-of-cu-pd-icosahedra-supercrystals-studied-by-in-situ-x-ray-scattering.pdfDirect OA link when available
- Concepts
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Small-angle X-ray scattering, Nucleation, Scattering, Materials science, Lamellar structure, Nanocrystal, Nanotechnology, Phase (matter), Self-assembly, Chemical physics, Chemical engineering, Chemistry, Optics, Physics, Composite material, Organic chemistry, EngineeringTop concepts (fields/topics) attached by OpenAlex
- Cited by
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2Total citation count in OpenAlex
- Citations by year (recent)
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2024: 1, 2023: 1Per-year citation counts (last 5 years)
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44Number of works referenced by this work
- Related works (count)
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10Other works algorithmically related by OpenAlex
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