Dispensing Single Drops as Electrochemical Reactors Article Swipe

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Shokoufeh Rastgar , Sebastian Pleis , Yanzhen Zhang , Günther Wittstock ·

YOU? · · 2022 · Open Access · · DOI: https://doi.org/10.1002/celc.202200004

A strategy is proposed to generate single microdrops with femtoliter to microliter volumes as a liquid reactor and to guide them towards a reactive surface within a viscous carrier liquid. Reactions of the drop content with the surface are exemplified by exhaustive electrolysis of the reactor content, making use of an ion‐conducting pathway through the carrier liquid. The mechanisms by which the redox‐active species from the aqueous drop reach the electrode surface were established by a combination of time‐lapse microscopy of the drop shape, chronoamperometric recording of the single drop electrolysis, and modelling of the reaction‐transport problem, showing that partitioning over the liquid‐liquid interface must be a key step in this mechanism. The possibilities of reagent delivery and external triggering of a reaction are expanded by the possibility for controlled addition of further dissolved reactants to the liquid microreactor.

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Microreactor Electrolysis Drop (telecommunication) Reagent Chemistry Redox Electrochemistry Aqueous solution Chemical engineering Electrode Analytical Chemistry (journal) Chromatography Inorganic chemistry Organic chemistry Catalysis Computer science Electrolyte Physical chemistry Engineering Telecommunications

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Type: article
Language: en
Landing Page: https://doi.org/10.1002/celc.202200004
PDF: https://onlinelibrary.wiley.com/doi/pdfdirect/10.1002/celc.202200004
OA Status: hybrid
Cited By: 2
References: 61
Related Works: 10
OpenAlex ID: https://openalex.org/W4206068499

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DOI: https://doi.org/10.1002/celc.202200004

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Title: Dispensing Single Drops as Electrochemical Reactors

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Type: article

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Language: en

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Publication year: 2022

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Publication date: 2022-01-21

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Authors: Shokoufeh Rastgar, Sebastian Pleis, Yanzhen Zhang, Günther Wittstock

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Landing page: https://doi.org/10.1002/celc.202200004

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Concepts: Microreactor, Electrolysis, Drop (telecommunication), Reagent, Chemistry, Redox, Electrochemistry, Aqueous solution, Chemical engineering, Electrode, Analytical Chemistry (journal), Chromatography, Inorganic chemistry, Organic chemistry, Catalysis, Computer science, Electrolyte, Physical chemistry, Engineering, Telecommunications

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Cited by: 2

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Citations by year (recent): 2024: 1, 2022: 1

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