Dissipation Dynamics and Residue of Four Herbicides in Paddy Fields Using HPLC-MS/MS and GC-MS Article Swipe
Yu Qian
,
Ping Zhang
,
Yuhan He
,
Zhifeng Xu
,
Xiulong He
,
Yuan Hu
,
Hongjun Zhang
,
Lin He
·
YOU?
·
· 2019
· Open Access
·
· DOI: https://doi.org/10.3390/ijerph16020236
YOU?
·
· 2019
· Open Access
·
· DOI: https://doi.org/10.3390/ijerph16020236
The dissipation dynamics and residue of pyrazosulfuron-ethyl, bensulfuron-methyl, acetochlor, and butachlor in paddy fields at Good Agricultural Practices (GAP) condition were carefully investigated in this study. The four herbicides’ residues were determined based on a quick, easy, cheap, rugged, safe (QuEChERS) method coupled with HPLC-MS/MS and GC-MS. The limit of detection (LOD) for pyrazosulfuron-ethyl, bensulfuron-methyl, acetochlor, and butachlor in all matrices ranged from 0.04–1.0 ng. The limit of quantification (LOQ) of the four herbicides ranged from 0.01–0.1 mg/kg. Moreover, the average recoveries of the four herbicides ranged from 78.9–108% with relative standard deviations (RSDs) less than 15% at three different fortified levels for different matrices. The dissipation results indicated that the average half-lives (t1/2) of the four herbicides in soil were in the range of 3.5–17.8 days, and more than 95% of the four herbicides dissipated within 5 days in water. Furthermore, the final residues of the four herbicides were all below the LOQ at harvest time. Such results highlight the dissipation dynamics and residue of the four herbicides in a rice cropping system and contribute to risk assessment as well as scientific guidance on the proper and safe application of herbicides in paddy fields.
Related Topics
Concepts
Acetochlor
Quechers
Butachlor
Chemistry
Residue (chemistry)
Detection limit
Maximum Residue Limit
Paddy field
Mesotrione
Atrazine
Pesticide
Environmental chemistry
Chromatography
Pesticide residue
Toxicology
Agronomy
Weed control
Biology
Biochemistry
Metadata
- Type
- article
- Language
- en
- Landing Page
- https://doi.org/10.3390/ijerph16020236
- https://www.mdpi.com/1660-4601/16/2/236/pdf?version=1548156179
- OA Status
- gold
- Cited By
- 25
- References
- 56
- Related Works
- 10
- OpenAlex ID
- https://openalex.org/W2910646403
All OpenAlex metadata
Raw OpenAlex JSON
- OpenAlex ID
-
https://openalex.org/W2910646403Canonical identifier for this work in OpenAlex
- DOI
-
https://doi.org/10.3390/ijerph16020236Digital Object Identifier
- Title
-
Dissipation Dynamics and Residue of Four Herbicides in Paddy Fields Using HPLC-MS/MS and GC-MSWork title
- Type
-
articleOpenAlex work type
- Language
-
enPrimary language
- Publication year
-
2019Year of publication
- Publication date
-
2019-01-15Full publication date if available
- Authors
-
Yu Qian, Ping Zhang, Yuhan He, Zhifeng Xu, Xiulong He, Yuan Hu, Hongjun Zhang, Lin HeList of authors in order
- Landing page
-
https://doi.org/10.3390/ijerph16020236Publisher landing page
- PDF URL
-
https://www.mdpi.com/1660-4601/16/2/236/pdf?version=1548156179Direct link to full text PDF
- Open access
-
YesWhether a free full text is available
- OA status
-
goldOpen access status per OpenAlex
- OA URL
-
https://www.mdpi.com/1660-4601/16/2/236/pdf?version=1548156179Direct OA link when available
- Concepts
-
Acetochlor, Quechers, Butachlor, Chemistry, Residue (chemistry), Detection limit, Maximum Residue Limit, Paddy field, Mesotrione, Atrazine, Pesticide, Environmental chemistry, Chromatography, Pesticide residue, Toxicology, Agronomy, Weed control, Biology, BiochemistryTop concepts (fields/topics) attached by OpenAlex
- Cited by
-
25Total citation count in OpenAlex
- Citations by year (recent)
-
2025: 2, 2024: 3, 2023: 5, 2022: 7, 2021: 3Per-year citation counts (last 5 years)
- References (count)
-
56Number of works referenced by this work
- Related works (count)
-
10Other works algorithmically related by OpenAlex
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| referenced_works | https://openalex.org/W2765254365, https://openalex.org/W1997717391, https://openalex.org/W2088501253, https://openalex.org/W2054544326, https://openalex.org/W1975930834, https://openalex.org/W2763924716, https://openalex.org/W2789700328, https://openalex.org/W1997468944, https://openalex.org/W1974959491, https://openalex.org/W2040479383, https://openalex.org/W2049685661, https://openalex.org/W2073662769, https://openalex.org/W6632461760, https://openalex.org/W6687515022, https://openalex.org/W2323121744, https://openalex.org/W6693173492, https://openalex.org/W2522953853, https://openalex.org/W2601214017, https://openalex.org/W6610970196, https://openalex.org/W3215681709, https://openalex.org/W2046325455, https://openalex.org/W2383391617, https://openalex.org/W6697653596, https://openalex.org/W1964601964, https://openalex.org/W2023089930, https://openalex.org/W6688578083, https://openalex.org/W2501352054, https://openalex.org/W2049193429, https://openalex.org/W2011750475, https://openalex.org/W2044132668, https://openalex.org/W2416262342, https://openalex.org/W2739246115, https://openalex.org/W2088616161, https://openalex.org/W2074547921, https://openalex.org/W2074892463, https://openalex.org/W2018748796, https://openalex.org/W2020621001, https://openalex.org/W201981154, https://openalex.org/W2142225533, https://openalex.org/W2157451311, https://openalex.org/W2024541186, https://openalex.org/W1964001705, https://openalex.org/W2750085674, https://openalex.org/W2039139094, https://openalex.org/W2071717608, https://openalex.org/W2067118968, https://openalex.org/W2075888403, https://openalex.org/W1966148370, https://openalex.org/W2026543532, https://openalex.org/W2023925644, https://openalex.org/W2222884297, https://openalex.org/W1544818860, https://openalex.org/W2200827407, https://openalex.org/W2297766092, https://openalex.org/W315334025, https://openalex.org/W2264143704 |
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