Early crystallization of amorphous selenium under high pressure studied by synchrotron XRD method Article Swipe
Shuhua Yuan
,
Luhong Wang
,
Fuyang Liu
,
Jay D. Bass
,
Yingzhe Li
,
Paul A. Ginsberg
,
Dongzhou Zhang
,
Vitali B. Prakapenka
,
Sergey N. Tkachev
,
Haozhe Liu
·
YOU?
·
· 2023
· Open Access
·
· DOI: https://doi.org/10.1088/1361-648x/acc8b0
YOU?
·
· 2023
· Open Access
·
· DOI: https://doi.org/10.1088/1361-648x/acc8b0
The amorphous selenium (a-Se) was studied via x-ray diffraction (XRD) under pressures ranging from ambient pressure up to 30 GPa at room temperature to study its high-pressure behavior. Two compressional experiments on a-Se samples, with and without heat treatment, respectively, were conducted. Contrary to the previous reports that a-Se crystallized abruptly at around 12 GPa, in this work we report an early partially crystallized state at 4.9 GPa before completing the crystallization at around 9.5 GPa based on in-situ high pressure XRD measurements on the a-Se with 70 °C heat treatment. In comparison, crystallization pressure on another a-Se sample without thermal treatment history was observed to be 12.7 GPa, consistent with the previously reported crystallization pressure. Thus, it is proposed in this work that prior heat treatment of a-Se can result in an earlier crystallization under high pressure, which helps to understand the possible mechanism caused by the previous controversial reports on pressure induced crystallization behavior in a-Se.
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- Type
- article
- Language
- en
- Landing Page
- https://doi.org/10.1088/1361-648x/acc8b0
- OA Status
- hybrid
- Cited By
- 4
- References
- 44
- Related Works
- 10
- OpenAlex ID
- https://openalex.org/W4361195781
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https://doi.org/10.1088/1361-648x/acc8b0Digital Object Identifier
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Early crystallization of amorphous selenium under high pressure studied by synchrotron XRD methodWork title
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articleOpenAlex work type
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enPrimary language
- Publication year
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2023Year of publication
- Publication date
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2023-03-29Full publication date if available
- Authors
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Shuhua Yuan, Luhong Wang, Fuyang Liu, Jay D. Bass, Yingzhe Li, Paul A. Ginsberg, Dongzhou Zhang, Vitali B. Prakapenka, Sergey N. Tkachev, Haozhe LiuList of authors in order
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https://doi.org/10.1088/1361-648x/acc8b0Publisher landing page
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YesWhether a free full text is available
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hybridOpen access status per OpenAlex
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https://doi.org/10.1088/1361-648x/acc8b0Direct OA link when available
- Concepts
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Crystallization, Selenium, Amorphous solid, Materials science, High pressure, Ambient pressure, Diffraction, Synchrotron, Crystallography, Analytical Chemistry (journal), Thermodynamics, Chemistry, Metallurgy, Optics, Chromatography, PhysicsTop concepts (fields/topics) attached by OpenAlex
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4Total citation count in OpenAlex
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2025: 3, 2024: 1Per-year citation counts (last 5 years)
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10Other works algorithmically related by OpenAlex
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