Electrochemical Dehydrogenative Acetalization Protection of Alcohols with Tetrahydrofuran Article Swipe
Related Concepts
Tetrahydrofuran
Electrochemistry
Chemistry
Organic chemistry
Electrode
Solvent
Physical chemistry
Raolin Huang
,
Congjun Yu
,
Frédéric W. Patureau
·
YOU?
·
· 2021
· Open Access
·
· DOI: https://doi.org/10.1002/celc.202101155
· OA: W3204322308
YOU?
·
· 2021
· Open Access
·
· DOI: https://doi.org/10.1002/celc.202101155
· OA: W3204322308
A mild, facile, and environmentally friendly electrochemical protocol for the C(sp 3 )−H/O−H cross dehydrogenative coupling between various alcohols and tetrahydrofuran with H 2 evolution is herein reported. This synthetic strategy does not require external oxidants nor catalysts. The broad functional group compatibility includes hydroxyl, halogens, olefins as well as an alkyne. Initial mechanistic investigations were conducted. The method provides a green and efficient hydroxyl group protection.
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