Electrochemical Detection of Acetaminophen in Pharmaceuticals Using Rod-Shaped α-Bi2O3 Prepared via Reverse Co-Precipitation Article Swipe
Ljubica Andjelković
,
Slađana Đurđić
,
Dalibor Stanković
,
Aleksandar Kremenović
,
Vladimir B. Pavlović
,
Dejan Jeremić
,
Marija Šuljagić
·
YOU?
·
· 2024
· Open Access
·
· DOI: https://doi.org/10.3390/chemosensors12070122
YOU?
·
· 2024
· Open Access
·
· DOI: https://doi.org/10.3390/chemosensors12070122
This study employed a novel synthetic approach involving a modified reverse co-precipitation method utilizing glacial acetic acid to synthesize α-Bi2O3. X-ray powder diffraction and scanning and transmission electron microscopy analyses revealed the formation of a rod-like α-Bi2O3 microstructure. The prepared material was utilized to modify a glassy carbon paste (GCP) electrode for the development of an electrochemical sensor for acetaminophen (APAP) detection using differential pulse voltammetry (DPV). Cyclic voltammetry studies revealed that the GCP@Bi2O3 electrode exhibited enhanced electrochemical properties compared to the bare GCP. The designed GCP@Bi2O3 sensor detected APAP in the linear concentration range from 0.05 to 12.00 µM, with LOQ and LOD of 36 nM and 10 nM, respectively. Additionally, the developed sensor demonstrated sufficient precision, repeatability, and selectivity toward APAP detection. The recovery values between the declared and found APAP content in a pharmaceutical formulation (Caffetin®) displayed the advantageous accuracy, precision, and applicability of the GCP@Bi2O3 sensor and the developed DPV method for real-time APAP detection in pharmaceuticals, with minimal interference from the matrix effect.
Related Topics
Concepts
Differential pulse voltammetry
Materials science
Electrochemical gas sensor
Cyclic voltammetry
Electrode
Electrochemistry
Detection limit
Acetic acid
Acetaminophen
Repeatability
Nuclear chemistry
Chromatography
Chemistry
Organic chemistry
Biochemistry
Physical chemistry
Metadata
- Type
- article
- Language
- en
- Landing Page
- https://doi.org/10.3390/chemosensors12070122
- OA Status
- gold
- Cited By
- 6
- References
- 115
- Related Works
- 10
- OpenAlex ID
- https://openalex.org/W4400246704
All OpenAlex metadata
Raw OpenAlex JSON
- OpenAlex ID
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https://openalex.org/W4400246704Canonical identifier for this work in OpenAlex
- DOI
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https://doi.org/10.3390/chemosensors12070122Digital Object Identifier
- Title
-
Electrochemical Detection of Acetaminophen in Pharmaceuticals Using Rod-Shaped α-Bi2O3 Prepared via Reverse Co-PrecipitationWork title
- Type
-
articleOpenAlex work type
- Language
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enPrimary language
- Publication year
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2024Year of publication
- Publication date
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2024-07-02Full publication date if available
- Authors
-
Ljubica Andjelković, Slađana Đurđić, Dalibor Stanković, Aleksandar Kremenović, Vladimir B. Pavlović, Dejan Jeremić, Marija ŠuljagićList of authors in order
- Landing page
-
https://doi.org/10.3390/chemosensors12070122Publisher landing page
- Open access
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YesWhether a free full text is available
- OA status
-
goldOpen access status per OpenAlex
- OA URL
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https://doi.org/10.3390/chemosensors12070122Direct OA link when available
- Concepts
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Differential pulse voltammetry, Materials science, Electrochemical gas sensor, Cyclic voltammetry, Electrode, Electrochemistry, Detection limit, Acetic acid, Acetaminophen, Repeatability, Nuclear chemistry, Chromatography, Chemistry, Organic chemistry, Biochemistry, Physical chemistryTop concepts (fields/topics) attached by OpenAlex
- Cited by
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6Total citation count in OpenAlex
- Citations by year (recent)
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2025: 4, 2024: 2Per-year citation counts (last 5 years)
- References (count)
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115Number of works referenced by this work
- Related works (count)
-
10Other works algorithmically related by OpenAlex
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