Engineering Peripheral Metal‐Oxide Catalysis: Interparticle Spacing in Cu/ZrO 2 Catalysts for Methanol Synthesis by CO 2 Hydrogenation Article Swipe
Iván López‐Luque
,
Jannis Hack
,
Tania Ródenas
,
Wilson Henao
,
Bernat Mundet
,
Prathamesh Patil
,
Christian M. Pichler
,
Carlo Marini
,
Giovanni Agostini
,
Daniel M. Meier
,
Gonzalo Prieto
·
YOU?
·
· 2025
· Open Access
·
· DOI: https://doi.org/10.1002/anie.202420126
YOU?
·
· 2025
· Open Access
·
· DOI: https://doi.org/10.1002/anie.202420126
The periphery surrounding oxide‐supported metal nanoparticles plays a crucial role in many catalytic reactions that exhibit strong metal‐oxide promotional effects. Engineering this catalytically active periphery, where kinetically relevant surface intermediates are efficiently turned over, offers a pathway to optimized performance, yet it remains challenging due to the need for precise control over nanospatial catalyst features. Herein, we address this subject for the relevant case of methanol synthesis by CO 2 hydrogenation on Cu/ZrO 2 catalysts. The methanol synthesis rate reaches a maximum at a surface‐to‐surface Cu interparticle distance of ca. 15 nm. Operando modulation–excitation diffuse reflectance infrared spectroscopy reveals that this optimal spacing maximizes the fraction of surface‐bound HCOO* intermediates, stabilized on coordinatively unsaturated Zr(IV) Lewis acid sites on the ZrO 2 support, which are dynamically involved in catalysis. This particle spacing represents a shift in the reaction's kinetic control regime and the apparent activation energy for methanol synthesis. Engineering Cu interparticle spacing to the optimal value results in exceptionally high metal‐specific methanol formation rates under industrially relevant reaction conditions. More broadly, our findings highlight that, beyond metal particle size, interparticle spacing is a key design parameter for catalyst systems featuring functional metal‐oxide interfaces.
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- Type
- article
- Language
- en
- Landing Page
- https://doi.org/10.1002/anie.202420126
- https://onlinelibrary.wiley.com/doi/pdfdirect/10.1002/anie.202420126
- OA Status
- hybrid
- Cited By
- 2
- References
- 52
- Related Works
- 10
- OpenAlex ID
- https://openalex.org/W4412765449
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https://openalex.org/W4412765449Canonical identifier for this work in OpenAlex
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https://doi.org/10.1002/anie.202420126Digital Object Identifier
- Title
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Engineering Peripheral Metal‐Oxide Catalysis: Interparticle Spacing in Cu/ZrO 2 Catalysts for Methanol Synthesis by CO 2 HydrogenationWork title
- Type
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articleOpenAlex work type
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enPrimary language
- Publication year
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2025Year of publication
- Publication date
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2025-07-29Full publication date if available
- Authors
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Iván López‐Luque, Jannis Hack, Tania Ródenas, Wilson Henao, Bernat Mundet, Prathamesh Patil, Christian M. Pichler, Carlo Marini, Giovanni Agostini, Daniel M. Meier, Gonzalo PrietoList of authors in order
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https://doi.org/10.1002/anie.202420126Publisher landing page
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https://onlinelibrary.wiley.com/doi/pdfdirect/10.1002/anie.202420126Direct link to full text PDF
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YesWhether a free full text is available
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hybridOpen access status per OpenAlex
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https://onlinelibrary.wiley.com/doi/pdfdirect/10.1002/anie.202420126Direct OA link when available
- Concepts
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Catalysis, Methanol, Oxide, Metal, Nanoparticle, Materials science, Inorganic chemistry, Chemical engineering, Heterogeneous catalysis, Chemistry, Nanotechnology, Organic chemistry, EngineeringTop concepts (fields/topics) attached by OpenAlex
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2Total citation count in OpenAlex
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2025: 2Per-year citation counts (last 5 years)
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52Number of works referenced by this work
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10Other works algorithmically related by OpenAlex
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| abstract_inverted_index.relevant | 28, 63, 168 |
| abstract_inverted_index.support, | 123 |
| abstract_inverted_index.catalytic | 13 |
| abstract_inverted_index.features. | 55 |
| abstract_inverted_index.featuring | 191 |
| abstract_inverted_index.formation | 164 |
| abstract_inverted_index.highlight | 175 |
| abstract_inverted_index.maximizes | 104 |
| abstract_inverted_index.optimized | 39 |
| abstract_inverted_index.parameter | 187 |
| abstract_inverted_index.periphery | 2 |
| abstract_inverted_index.reactions | 14 |
| abstract_inverted_index.synthesis | 67, 78 |
| abstract_inverted_index.activation | 145 |
| abstract_inverted_index.catalysis. | 129 |
| abstract_inverted_index.catalysts. | 75 |
| abstract_inverted_index.functional | 192 |
| abstract_inverted_index.periphery, | 25 |
| abstract_inverted_index.reaction's | 138 |
| abstract_inverted_index.represents | 133 |
| abstract_inverted_index.stabilized | 111 |
| abstract_inverted_index.synthesis. | 149 |
| abstract_inverted_index.Engineering | 21, 150 |
| abstract_inverted_index.challenging | 44 |
| abstract_inverted_index.conditions. | 170 |
| abstract_inverted_index.dynamically | 126 |
| abstract_inverted_index.efficiently | 32 |
| abstract_inverted_index.interfaces. | 194 |
| abstract_inverted_index.kinetically | 27 |
| abstract_inverted_index.nanospatial | 53 |
| abstract_inverted_index.promotional | 19 |
| abstract_inverted_index.reflectance | 96 |
| abstract_inverted_index.surrounding | 3 |
| abstract_inverted_index.unsaturated | 114 |
| abstract_inverted_index.industrially | 167 |
| abstract_inverted_index.performance, | 40 |
| abstract_inverted_index.spectroscopy | 98 |
| abstract_inverted_index.catalytically | 23 |
| abstract_inverted_index.exceptionally | 160 |
| abstract_inverted_index.hydrogenation | 71 |
| abstract_inverted_index.intermediates | 30 |
| abstract_inverted_index.interparticle | 87, 152, 181 |
| abstract_inverted_index.metal‐oxide | 18, 193 |
| abstract_inverted_index.nanoparticles | 6 |
| abstract_inverted_index.coordinatively | 113 |
| abstract_inverted_index.intermediates, | 110 |
| abstract_inverted_index.surface‐bound | 108 |
| abstract_inverted_index.metal‐specific | 162 |
| abstract_inverted_index.oxide‐supported | 4 |
| abstract_inverted_index.surface‐to‐surface | 85 |
| abstract_inverted_index.modulation–excitation | 94 |
| cited_by_percentile_year.max | 97 |
| cited_by_percentile_year.min | 95 |
| corresponding_author_ids | https://openalex.org/A5050725435 |
| countries_distinct_count | 4 |
| institutions_distinct_count | 11 |
| corresponding_institution_ids | https://openalex.org/I134820265, https://openalex.org/I4210135619, https://openalex.org/I60053951 |
| citation_normalized_percentile.value | 0.80860098 |
| citation_normalized_percentile.is_in_top_1_percent | False |
| citation_normalized_percentile.is_in_top_10_percent | True |