Enhanced Nitric Oxide Electroreduction to Ammonia via Modulating Spin‐Polarization of Fe Single‐Atom Catalysts Article Swipe

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Jialing Song , Zhiyi Wei , Lupeng Han , Zhenlin Wang , Chenghao Fan , Donglin Han , Chunwei Dong , Haiyan Duan , Xiyang Wang , Sam Fong Yau Li , Eslam M. Hamed , Ming Xie , Emiliano Cortés , Dengsong Zhang ·

YOU? · · 2025 · Open Access · · DOI: https://doi.org/10.1002/adfm.202523040

Electrochemical nitric oxide reduction (NORR) offers a sustainable pathway to ammonia (NH 3 ) while removing toxic NO from industrial emissions. However, high efficiency is hindered by the difficulty of synchronizing multi‐proton/electron transfers to accelerate NO hydrogenation and suppress competing hydrogen evolution. Here, an Fe single‐atom catalyst (FeSAC) is reported that achieves record NORR activity through spin‐state engineering. Using a top‐down electrospinning approach, self‐supported S,N‐doped carbon fiber films hosting Fe‐N 3 S 1 sites are fabricated. This catalyst delivers an NH 3 yield rate of 140.58 µmol h −1 cm −2 with a Faradaic efficiency of 96.28%, outperforming nearly all reported SACs. Mechanistic analysis reveals that sulfur doping induces a high‐spin Fe 3+ → low‐spin Fe 2+ transition, suppressing spin polarization, strengthening NO adsorption, and facilitating proton supply to accelerate hydrogenation. These results establish spin‐state modulation as a powerful paradigm for designing next‐generation single‐atom catalysts for complex multi‐proton/electron electrocatalytic transformations, such as the electrosynthesis of ammonia.

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Type: article
Language: en
Landing Page: https://doi.org/10.1002/adfm.202523040
OA Status: hybrid
References: 43
OpenAlex ID: https://openalex.org/W4415946996

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DOI: https://doi.org/10.1002/adfm.202523040

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Title: Enhanced Nitric Oxide Electroreduction to Ammonia via Modulating Spin‐Polarization of Fe Single‐Atom Catalysts

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Type: article

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Language: en

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Publication year: 2025

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Publication date: 2025-11-05

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Authors: Jialing Song, Zhiyi Wei, Lupeng Han, Zhenlin Wang, Chenghao Fan, Donglin Han, Chunwei Dong, Haiyan Duan, Xiyang Wang, Sam Fong Yau Li, Eslam M. Hamed, Ming Xie, Emiliano Cortés, Dengsong Zhang

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Landing page: https://doi.org/10.1002/adfm.202523040

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primary_location.landing_page_url	https://doi.org/10.1002/adfm.202523040
publication_date	2025-11-05
publication_year	2025
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referenced_works_count	43
abstract_inverted_index.)	14
abstract_inverted_index.1	73
abstract_inverted_index.3	13, 71, 82
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abstract_inverted_index.h	88
abstract_inverted_index.2+	117
abstract_inverted_index.3+	113
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abstract_inverted_index.NH	81
abstract_inverted_index.NO	18, 36, 123
abstract_inverted_index.an	44, 80
abstract_inverted_index.as	137, 152
abstract_inverted_index.by	27
abstract_inverted_index.cm	90
abstract_inverted_index.is	25, 49
abstract_inverted_index.of	30, 85, 96, 155
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abstract_inverted_index.all	100
abstract_inverted_index.and	38, 125
abstract_inverted_index.are	75
abstract_inverted_index.for	141, 146
abstract_inverted_index.the	28, 153
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abstract_inverted_index.This	77
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abstract_inverted_index.−2	91
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abstract_inverted_index.These	132
abstract_inverted_index.Using	59
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abstract_inverted_index.films	68
abstract_inverted_index.oxide	3
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abstract_inverted_index.(NORR)	5
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abstract_inverted_index.doping	108
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abstract_inverted_index.nitric	2
abstract_inverted_index.offers	6
abstract_inverted_index.proton	127
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abstract_inverted_index.sulfur	107
abstract_inverted_index.supply	128
abstract_inverted_index.(FeSAC)	48
abstract_inverted_index.96.28%,	97
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abstract_inverted_index.low‐spin	115
abstract_inverted_index.modulation	136
abstract_inverted_index.top‐down	61
abstract_inverted_index.Mechanistic	103
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abstract_inverted_index.adsorption,	124
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abstract_inverted_index.engineering.	58
abstract_inverted_index.facilitating	126
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abstract_inverted_index.outperforming	98
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abstract_inverted_index.single‐atom	46, 144
abstract_inverted_index.strengthening	122
abstract_inverted_index.synchronizing	31
abstract_inverted_index.hydrogenation.	131
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abstract_inverted_index.electrocatalytic	149
abstract_inverted_index.electrosynthesis	154
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corresponding_institution_ids	https://openalex.org/I113940042, https://openalex.org/I8204097
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