Enhancing Cellulose and Lignin Fractionation from Acacia Wood: Optimized Parameters Using a Deep Eutectic Solvent System and Solvent Recovery Article Swipe
Solange Magalhães
,
María José Aliaño–González
,
M Rodrigues
,
Catarina Fernandes
,
Cátia V.T. Mendes
,
M. G. Carvalho
,
Luís Alves
,
Bruno Medronho
,
Maria G. Rasteiro
·
YOU?
·
· 2024
· Open Access
·
· DOI: https://doi.org/10.3390/molecules29153495
YOU?
·
· 2024
· Open Access
·
· DOI: https://doi.org/10.3390/molecules29153495
Cellulose and lignin, sourced from biomass, hold potential for innovative bioprocesses and biomaterials. However, traditional fractionation and purification methods often rely on harmful chemicals and high temperatures, making these processes both hazardous and costly. This study introduces a sustainable approach for fractionating acacia wood, focusing on both cellulose and lignin extraction using a deep eutectic solvent (DES) composed of choline chloride (ChCl) and levulinic acid (LA). A design of experiment was employed for the optimization of the most relevant fractionation parameters: time and temperature. In the case of the lignin, both parameters were found to be significant variables in the fractionation process (p-values of 0.0128 and 0.0319 for time and temperature, respectively), with a positive influence. Likewise, in the cellulose case, time and temperature also demonstrated a positive effect, with p-values of 0.0103 and 0.028, respectively. An optimization study was finally conducted to determine the maximum fractionation yield of lignin and cellulose. The optimized conditions were found to be 15% (w/v) of the wood sample in 1:3 ChCl:LA under a treatment temperature of 160 °C for 8 h. The developed method was validated through repeatability and intermediate precision studies, which yielded a coefficient of variation lower than 5%. The recovery and reuse of DES were successfully evaluated, revealing remarkable fractionation yields even after five cycles. This work demonstrates the feasibility of selectively extracting lignin and cellulose from woody biomass using a sustainable solvent, thus paving the way for valorization of invasive species biomass.
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Metadata
- Type
- article
- Language
- en
- Landing Page
- https://doi.org/10.3390/molecules29153495
- OA Status
- gold
- Cited By
- 5
- References
- 49
- Related Works
- 10
- OpenAlex ID
- https://openalex.org/W4400974660
All OpenAlex metadata
Raw OpenAlex JSON
- OpenAlex ID
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https://openalex.org/W4400974660Canonical identifier for this work in OpenAlex
- DOI
-
https://doi.org/10.3390/molecules29153495Digital Object Identifier
- Title
-
Enhancing Cellulose and Lignin Fractionation from Acacia Wood: Optimized Parameters Using a Deep Eutectic Solvent System and Solvent RecoveryWork title
- Type
-
articleOpenAlex work type
- Language
-
enPrimary language
- Publication year
-
2024Year of publication
- Publication date
-
2024-07-25Full publication date if available
- Authors
-
Solange Magalhães, María José Aliaño–González, M Rodrigues, Catarina Fernandes, Cátia V.T. Mendes, M. G. Carvalho, Luís Alves, Bruno Medronho, Maria G. RasteiroList of authors in order
- Landing page
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https://doi.org/10.3390/molecules29153495Publisher landing page
- Open access
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YesWhether a free full text is available
- OA status
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goldOpen access status per OpenAlex
- OA URL
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https://doi.org/10.3390/molecules29153495Direct OA link when available
- Concepts
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Deep eutectic solvent, Lignin, Cellulose, Fractionation, Solvent, Chemistry, Acacia, Organic chemistry, Eutectic system, Pulp and paper industry, Chromatography, Chemical engineering, Botany, Biology, Alloy, EngineeringTop concepts (fields/topics) attached by OpenAlex
- Cited by
-
5Total citation count in OpenAlex
- Citations by year (recent)
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2025: 3, 2024: 2Per-year citation counts (last 5 years)
- References (count)
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49Number of works referenced by this work
- Related works (count)
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10Other works algorithmically related by OpenAlex
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| corresponding_author_ids | https://openalex.org/A5044211431, https://openalex.org/A5042614701 |
| countries_distinct_count | 3 |
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| corresponding_institution_ids | https://openalex.org/I39147953, https://openalex.org/I71503853, https://openalex.org/I76903346 |
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| sustainable_development_goals[0].display_name | Responsible consumption and production |
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| citation_normalized_percentile.is_in_top_10_percent | False |