Green Synthesis of ZnO/SnO2 Hybrid Nanocomposite for Degradation of Cationic and Anionic Dyes under Sunlight Radiation Article Swipe
Naaser A. Y. Abduh
,
Abdel-Basit Al-Odayni
·
YOU?
·
· 2023
· Open Access
·
· DOI: https://doi.org/10.3390/ma16237398
YOU?
·
· 2023
· Open Access
·
· DOI: https://doi.org/10.3390/ma16237398
The aim of this work was to biosynthesize SnO2-decorated ZnO (ZT) nanocomposites (NCs) of different Sn content (10, 20, and 30 mol%), namely, ZT10, ZT20, and ZT30, using Olea europaea leaf aqueous extract-based phytocompounds as nanoparticle facilitating agents for application as effective photocatalyst in the removal of dyes from polluted water. The obtained ZT NCs were characterized using various techniques, including FTIR, XRD, TGA, TEM, EDS, UV–Vis, PL, and BET surface area. X-ray diffraction patterns show that rutile SnO2 and hexagonal ZnO coexist in the composites, and their crystallite size (D) is affected by the SnO2 ratio; the obtained D-values were 17.24, 19.07, 13.99, 6.45, and 12.30 nm for ZnO, SnO2, ZT10, ZT20, and ZT30, respectively. The direct band gaps of the ZT heterostructure increase with increasing SnO2 ratio (band gap = 3.10, 3.45, 3.14, 3.17, and 3.21 eV, respectively). TEM spectroscopy revealed nanorod and spherical grain morphologies of the composites, while EDS confirmed the elemental composition, the element ratio, and the composite’s purity. All catalysts exhibit type III isotherm with macropore structure. The photocatalytic efficiency against cationic (methylene blue (MB), rhodamine B (RB)), and anionic (methyl orange (MO)) dyes, under sunlight, was optimal with ZT20. The results revealed almost complete degradation at 55, 65, and 55 min, respectively. Hence, it is evident that incorporating SnO2 improves the photocatalyst’s performance, with an apparent optimal enhancement at 20 mol% Sn decorating ZT NCs. More interestingly, the catalyst stability and activity remained unaffected even after four activating cycles.
Related Topics
Concepts
Photocatalysis
Materials science
Methyl orange
Nanocomposite
Rhodamine B
Cationic polymerization
Aqueous solution
Chemical engineering
BET theory
Nuclear chemistry
Crystallite
Rutile
Band gap
Catalysis
Nanotechnology
Chemistry
Organic chemistry
Polymer chemistry
Engineering
Optoelectronics
Metallurgy
Metadata
- Type
- article
- Language
- en
- Landing Page
- https://doi.org/10.3390/ma16237398
- https://www.mdpi.com/1996-1944/16/23/7398/pdf?version=1701167633
- OA Status
- gold
- Cited By
- 6
- References
- 53
- Related Works
- 10
- OpenAlex ID
- https://openalex.org/W4389085446
All OpenAlex metadata
Raw OpenAlex JSON
- OpenAlex ID
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https://openalex.org/W4389085446Canonical identifier for this work in OpenAlex
- DOI
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https://doi.org/10.3390/ma16237398Digital Object Identifier
- Title
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Green Synthesis of ZnO/SnO2 Hybrid Nanocomposite for Degradation of Cationic and Anionic Dyes under Sunlight RadiationWork title
- Type
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articleOpenAlex work type
- Language
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enPrimary language
- Publication year
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2023Year of publication
- Publication date
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2023-11-28Full publication date if available
- Authors
-
Naaser A. Y. Abduh, Abdel-Basit Al-OdayniList of authors in order
- Landing page
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https://doi.org/10.3390/ma16237398Publisher landing page
- PDF URL
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https://www.mdpi.com/1996-1944/16/23/7398/pdf?version=1701167633Direct link to full text PDF
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YesWhether a free full text is available
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goldOpen access status per OpenAlex
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https://www.mdpi.com/1996-1944/16/23/7398/pdf?version=1701167633Direct OA link when available
- Concepts
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Photocatalysis, Materials science, Methyl orange, Nanocomposite, Rhodamine B, Cationic polymerization, Aqueous solution, Chemical engineering, BET theory, Nuclear chemistry, Crystallite, Rutile, Band gap, Catalysis, Nanotechnology, Chemistry, Organic chemistry, Polymer chemistry, Engineering, Optoelectronics, MetallurgyTop concepts (fields/topics) attached by OpenAlex
- Cited by
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6Total citation count in OpenAlex
- Citations by year (recent)
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2025: 4, 2024: 2Per-year citation counts (last 5 years)
- References (count)
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53Number of works referenced by this work
- Related works (count)
-
10Other works algorithmically related by OpenAlex
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