Hematite α‐Fe2O3(0001) in Top and Side View: Resolving Long‐Standing Controversies about Its Surface Structure Article Swipe
Jesús Redondo
,
Jan Michalička
,
Florian Kraushofer
,
Giada Franceschi
,
Břetislav Šmíd
,
Nishant Kumar
,
Ondřej Man
,
Matthias Blatnik
,
Dominik Wrana
,
Benjamín Mallada
,
Martin Švec
,
Gareth S. Parkinson
,
Martin Setvín
,
Michele Riva
,
Ulrike Diebold
,
Jan Čechal
·
YOU?
·
· 2023
· Open Access
·
· DOI: https://doi.org/10.1002/admi.202300602
YOU?
·
· 2023
· Open Access
·
· DOI: https://doi.org/10.1002/admi.202300602
Hematite is a common iron oxide found in nature, and the α ‐Fe 2 O 3 (0001) plane is prevalent on the nanomaterial utilized in photo‐ and electrocatalytic applications. The atomic‐scale structure of the surface remains controversial despite decades of study, partly because it depends on sample history as well as the preparation conditions. Here, a comprehensive study is performed using an arsenal of surface techniques (non‐contact atomic force microscopy, scanning tunneling microscopy, low‐energy electron diffraction, and X‐ray photoemission spectroscopy) complemented by analyses of the near surface region by high‐resolution transmission electron microscopy and electron energy loss spectroscopy. The results show that the so‐called “bi‐phase” termination forms even under highly oxidizing conditions; a (1 × 1) surface is only observed in the presence of impurities. Furthermore, it is shown that the biphase is actually a continuous layer distorted due to a mismatch with the subsurface layers, and thus not the proposed mixture of FeO(111) and α ‐Fe 2 O 3 (0001) phases. Overall, the results show how combining surface and cross‐sectional imaging provides a full view that can be essential for understanding the role of the near‐surface region on oxide surface properties.
Related Topics
Concepts
Hematite
Materials science
Oxide
Transmission electron microscopy
Scanning tunneling microscope
Electron energy loss spectroscopy
Nanomaterials
Energy-dispersive X-ray spectroscopy
Spectroscopy
Electron diffraction
Oxidizing agent
Iron oxide
Photoemission electron microscopy
Surface energy
Scanning electron microscope
Impurity
Nanotechnology
Analytical Chemistry (journal)
Diffraction
Electron microscope
Optics
Chemistry
Metallurgy
Physics
Composite material
Chromatography
Organic chemistry
Quantum mechanics
Metadata
- Type
- article
- Language
- en
- Landing Page
- https://doi.org/10.1002/admi.202300602
- https://onlinelibrary.wiley.com/doi/pdfdirect/10.1002/admi.202300602
- OA Status
- gold
- Cited By
- 11
- References
- 50
- Related Works
- 10
- OpenAlex ID
- https://openalex.org/W4386022589
All OpenAlex metadata
Raw OpenAlex JSON
- OpenAlex ID
-
https://openalex.org/W4386022589Canonical identifier for this work in OpenAlex
- DOI
-
https://doi.org/10.1002/admi.202300602Digital Object Identifier
- Title
-
Hematite α‐Fe2O3(0001) in Top and Side View: Resolving Long‐Standing Controversies about Its Surface StructureWork title
- Type
-
articleOpenAlex work type
- Language
-
enPrimary language
- Publication year
-
2023Year of publication
- Publication date
-
2023-08-18Full publication date if available
- Authors
-
Jesús Redondo, Jan Michalička, Florian Kraushofer, Giada Franceschi, Břetislav Šmíd, Nishant Kumar, Ondřej Man, Matthias Blatnik, Dominik Wrana, Benjamín Mallada, Martin Švec, Gareth S. Parkinson, Martin Setvín, Michele Riva, Ulrike Diebold, Jan ČechalList of authors in order
- Landing page
-
https://doi.org/10.1002/admi.202300602Publisher landing page
- PDF URL
-
https://onlinelibrary.wiley.com/doi/pdfdirect/10.1002/admi.202300602Direct link to full text PDF
- Open access
-
YesWhether a free full text is available
- OA status
-
goldOpen access status per OpenAlex
- OA URL
-
https://onlinelibrary.wiley.com/doi/pdfdirect/10.1002/admi.202300602Direct OA link when available
- Concepts
-
Hematite, Materials science, Oxide, Transmission electron microscopy, Scanning tunneling microscope, Electron energy loss spectroscopy, Nanomaterials, Energy-dispersive X-ray spectroscopy, Spectroscopy, Electron diffraction, Oxidizing agent, Iron oxide, Photoemission electron microscopy, Surface energy, Scanning electron microscope, Impurity, Nanotechnology, Analytical Chemistry (journal), Diffraction, Electron microscope, Optics, Chemistry, Metallurgy, Physics, Composite material, Chromatography, Organic chemistry, Quantum mechanicsTop concepts (fields/topics) attached by OpenAlex
- Cited by
-
11Total citation count in OpenAlex
- Citations by year (recent)
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2025: 4, 2024: 7Per-year citation counts (last 5 years)
- References (count)
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50Number of works referenced by this work
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10Other works algorithmically related by OpenAlex
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| display_name | Hematite α‐Fe2O3(0001) in Top and Side View: Resolving Long‐Standing Controversies about Its Surface Structure |
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| primary_topic.display_name | Iron oxide chemistry and applications |
| related_works | https://openalex.org/W2124496689, https://openalex.org/W2034971043, https://openalex.org/W1995236256, https://openalex.org/W2517456317, https://openalex.org/W2149895428, https://openalex.org/W2575938942, https://openalex.org/W4381618427, https://openalex.org/W2784241602, https://openalex.org/W2999512016, https://openalex.org/W3048620448 |
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