Highly Active Oxidation Catalysts through Confining Pd Clusters on CeO₂ Nano‐Islands Article Swipe

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Jan‐Dierk Grunwaldt , Daria Gashnikova , Florian Maurer , Eric Sauter , Sarah Bernart , Jelena Jelic , Paolo Dolcet , Carina B. Maliakkal , Yuemin Wang , Christof Wöll , Felix Studt , Christian Kübel , Maria Casapu ·

YOU? · · 2024 · Open Access · · DOI: https://doi.org/10.1002/ange.202408511

CeO 2 ‐supported noble metal clusters are attractive catalytic materials for several applications. However, their atomic dispersion under oxidizing reaction conditions often leads to catalyst deactivation. In this study, the noble metal cluster formation threshold is rationally adjusted by using a mixed CeO 2 ‐Al 2 O 3 support. The preferential location of Pd on CeO 2 islands leads to a high local surface noble metal concentration and promotes the in situ formation of small Pd clusters at a rather low noble metal loading (0.5 wt %), which are shown to be the active species for CO conversion at low temperatures. As elucidated by complementary in situ/operando techniques, the spatial separation of CeO 2 islands on Al 2 O 3 confines the mobility of Pd, preventing the full redispersion or the formation of larger noble metal particles and maintaining a high CO oxidation activity at low temperatures. In a broader perspective, this approach to more efficiently use the noble metal can be transferred to further systems and reactions in heterogeneous catalysis.

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Noble metal Catalysis Oxidizing agent Metal Heterogeneous catalysis Chemical engineering Cluster (spacecraft) Chemistry Nanoparticle Precious metal Nanotechnology Materials science Inorganic chemistry Organic chemistry Engineering Programming language Computer science

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Type: article
Language: en
Landing Page: https://doi.org/10.1002/ange.202408511
OA Status: hybrid
References: 64
Related Works: 10
OpenAlex ID: https://openalex.org/W4399704240

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DOI: https://doi.org/10.1002/ange.202408511

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Title: Highly Active Oxidation Catalysts through Confining Pd Clusters on CeO₂ Nano‐Islands

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Language: en

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Publication year: 2024

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Publication date: 2024-06-15

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Authors: Jan‐Dierk Grunwaldt, Daria Gashnikova, Florian Maurer, Eric Sauter, Sarah Bernart, Jelena Jelic, Paolo Dolcet, Carina B. Maliakkal, Yuemin Wang, Christof Wöll, Felix Studt, Christian Kübel, Maria Casapu

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Landing page: https://doi.org/10.1002/ange.202408511

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Concepts: Noble metal, Catalysis, Oxidizing agent, Metal, Heterogeneous catalysis, Chemical engineering, Cluster (spacecraft), Chemistry, Nanoparticle, Precious metal, Nanotechnology, Materials science, Inorganic chemistry, Organic chemistry, Engineering, Programming language, Computer science

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Highly Active Oxidation Catalysts through Confining Pd Clusters on CeO₂ Nano‐Islands Article Swipe