H2[Pt(C2O4)2] as a Tailor‐made Halide‐free Precursor for the Preparation of Diesel Oxidation Catalysts: Nanoparticles Formation, Thermal Stability and Catalytic Performance Article Swipe
Federico Spolaore
,
Christoph Hengst
,
F. Dornhaus
,
Martin Votsmeier
,
Silvia Gross
·
YOU?
·
· 2023
· Open Access
·
· DOI: https://doi.org/10.1002/cctc.202301015
YOU?
·
· 2023
· Open Access
·
· DOI: https://doi.org/10.1002/cctc.202301015
The aim of this study was to investigate a tailor‐made metal precursor and its chemical properties to tune the properties of supported metal nanoparticles (NPs) and their catalytic performance when used as Diesel Oxidation Catalyst (DOC). The formation of extremely small Pt NPs from a new halide‐free Pt complex was investigated, namely bis(oxalato)platinate, H 2 [Pt(C 2 O 4 ) 2 ]. The size evolution of the supported NPs, from the formation upon the Pt precursor decomposition on γ‐alumina to the sintering of the NPs at high temperatures, was followed by thermogravimetric analysis coupled with mass spectrometry (TG‐MS) and differential scanning calorimetry (DSC), transmission electron microscopy (TEM) and diffuse reflectance infrared Fourier transform (DRIFT) spectroscopy. A correlation between the NPs’ size of the catalyst and the performance for the CO, C 3 H 6 , C 3 H 8 and NO oxidation reactions pointed out a retained activity during test cycles, showing low sensitivity to the test conditions applied (i. e., temperature and gas composition). The overall catalytic performance was better in the fresh catalysts compared to the reference catalyst prepared from platinum nitrate, Pt(NO 3 ) 4 . In particular, the different dispersion of the Pt NPs over the support obtained from the two precursors was identified as the reason for the different catalytic performance, retaining small NPs size after the tests cycles.
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- Type
- article
- Language
- en
- Landing Page
- https://doi.org/10.1002/cctc.202301015
- OA Status
- green
- References
- 67
- Related Works
- 10
- OpenAlex ID
- https://openalex.org/W4388451068
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Raw OpenAlex JSON
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https://openalex.org/W4388451068Canonical identifier for this work in OpenAlex
- DOI
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https://doi.org/10.1002/cctc.202301015Digital Object Identifier
- Title
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H2[Pt(C2O4)2] as a Tailor‐made Halide‐free Precursor for the Preparation of Diesel Oxidation Catalysts: Nanoparticles Formation, Thermal Stability and Catalytic PerformanceWork title
- Type
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articleOpenAlex work type
- Language
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enPrimary language
- Publication year
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2023Year of publication
- Publication date
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2023-11-07Full publication date if available
- Authors
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Federico Spolaore, Christoph Hengst, F. Dornhaus, Martin Votsmeier, Silvia GrossList of authors in order
- Landing page
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https://doi.org/10.1002/cctc.202301015Publisher landing page
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YesWhether a free full text is available
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greenOpen access status per OpenAlex
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https://hdl.handle.net/11577/3510129Direct OA link when available
- Concepts
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Catalysis, Thermogravimetric analysis, Platinum, Differential scanning calorimetry, Halide, Inorganic chemistry, Nanoparticle, Chemistry, Platinum nanoparticles, Fourier transform infrared spectroscopy, Materials science, Chemical engineering, Organic chemistry, Nanotechnology, Engineering, Thermodynamics, PhysicsTop concepts (fields/topics) attached by OpenAlex
- Cited by
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0Total citation count in OpenAlex
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10Other works algorithmically related by OpenAlex
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