In situ x-ray diffraction of high density polyethylene during dynamic drive: Polymer chain compression and decomposition Article Swipe
Rachel C. Huber
,
Erik B. Watkins
,
Dana M. Dattelbaum
,
Brian Bartram
,
L. L. Gibson
,
R. L. Gustavsen
·
YOU?
·
· 2021
· Open Access
·
· DOI: https://doi.org/10.1063/5.0057439
YOU?
·
· 2021
· Open Access
·
· DOI: https://doi.org/10.1063/5.0057439
Polymers are widely implemented materials often used for safety and security in our daily lives. However, we do not have a thorough understanding of the phase transformations of these materials when exposed to extreme condition, high strain rate events. To study polymers in these severe environments, we performed plate impact experiments that impart a one-dimensional shockwave, at high pressures and temperatures, to observe the materials response. Generally, velocimetry is the experimental diagnostic used to capture the movement of high velocity interfaces to then calculate the mechanical variables associated with shock compression. However, when a material undergoes a phase transition, such as between two crystalline phases or melting to decomposition during shock compression, velocimetry does not explicitly indicate what structural change occurred. At the Dynamic Compression Sector at the Advanced Photon Source, gas gun driven compression has been paired with x-ray diffraction, providing the ability to study both the shock parameters and structural changes concurrently. We explored high density polyethylene (HDPE) both on its reactants Hugoniot (<10.12 GPa) and within its transition region (24.3 GPa) where HDPE is hypothesized to decompose from reactants to products. With x-ray diffraction, we observed both polymer chain compression and crystal structure reorientation from orthorhombic to monoclinic above 6 GPa as well as either a possible phase change or chemical decomposition at 24.3 GPa. With these experiments, we were able to determine the crystalline and amorphous Hugoniot loci at pressures below the polymer transition region.
Related Topics
Concepts
High-density polyethylene
Materials science
Amorphous solid
Orthorhombic crystal system
Monoclinic crystal system
Diffraction
Polymer
Polyoxymethylene
Phase (matter)
Phase transition
Shock (circulatory)
Compression (physics)
Polyethylene
Composite material
Chemical physics
Thermodynamics
Crystallography
Crystal structure
Chemistry
Optics
Organic chemistry
Physics
Medicine
Internal medicine
Metadata
- Type
- article
- Language
- en
- Landing Page
- https://doi.org/10.1063/5.0057439
- OA Status
- green
- Cited By
- 10
- References
- 54
- Related Works
- 10
- OpenAlex ID
- https://openalex.org/W3210311020
All OpenAlex metadata
Raw OpenAlex JSON
- OpenAlex ID
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https://openalex.org/W3210311020Canonical identifier for this work in OpenAlex
- DOI
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https://doi.org/10.1063/5.0057439Digital Object Identifier
- Title
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In situ x-ray diffraction of high density polyethylene during dynamic drive: Polymer chain compression and decompositionWork title
- Type
-
articleOpenAlex work type
- Language
-
enPrimary language
- Publication year
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2021Year of publication
- Publication date
-
2021-11-03Full publication date if available
- Authors
-
Rachel C. Huber, Erik B. Watkins, Dana M. Dattelbaum, Brian Bartram, L. L. Gibson, R. L. GustavsenList of authors in order
- Landing page
-
https://doi.org/10.1063/5.0057439Publisher landing page
- Open access
-
YesWhether a free full text is available
- OA status
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greenOpen access status per OpenAlex
- OA URL
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https://www.osti.gov/biblio/1829005Direct OA link when available
- Concepts
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High-density polyethylene, Materials science, Amorphous solid, Orthorhombic crystal system, Monoclinic crystal system, Diffraction, Polymer, Polyoxymethylene, Phase (matter), Phase transition, Shock (circulatory), Compression (physics), Polyethylene, Composite material, Chemical physics, Thermodynamics, Crystallography, Crystal structure, Chemistry, Optics, Organic chemistry, Physics, Medicine, Internal medicineTop concepts (fields/topics) attached by OpenAlex
- Cited by
-
10Total citation count in OpenAlex
- Citations by year (recent)
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2025: 2, 2024: 5, 2023: 2, 2022: 1Per-year citation counts (last 5 years)
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54Number of works referenced by this work
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10Other works algorithmically related by OpenAlex
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