Imaging Phase Segregation in Nanoscale LixCoO2 Single Particles Article Swipe
Elliot J. Fuller
,
David S. Ashby
,
C. Polop
,
Elena Salagre
,
Bhuvsmita Bhargava
,
Yueming Song
,
E. Vasco
,
Joshua D. Sugar
,
Paul Albertus
,
Tevfik Onur Menteş
,
Andrea Locatelli
,
P. Segovia
,
M.A. González
,
A. Mascaraque
,
E. G. Michel
,
A. Alec Talin
·
YOU?
·
· 2022
· Open Access
·
· DOI: https://doi.org/10.1021/acsnano.2c05594
YOU?
·
· 2022
· Open Access
·
· DOI: https://doi.org/10.1021/acsnano.2c05594
LixCoO2 (LCO) is a common battery cathode material that has recently emerged as a promising material for other applications including electrocatalysis and as electrochemical random access memory (ECRAM). During charge-discharge cycling LCO exhibits phase transformations that are significantly complicated by electron correlation. While the bulk phase diagram for an ensemble of battery particles has been studied extensively, it remains unclear how these phases scale to nanometer dimensions and the effects of strain and diffusional anisotropy at the single-particle scale. Understanding these effects is critical to modeling battery performance and for predicting the scalability and performance of electrocatalysts and ECRAM. Here we investigate isolated, epitaxial LiCoO2 islands grown by pulsed laser deposition. After electrochemical cycling of the islands, conductive atomic force microscopy (c-AFM) is used to image the spatial distribution of conductive and insulating phases. Above 20 nm island thicknesses, we observe a kinetically arrested state in which the phase boundary is perpendicular to the Li-planes; we propose a model and present image analysis results that show smaller LCO islands have a higher conductive fraction than larger area islands, and the overall conductive fraction is consistent with the lithiation state. Thinner islands (14 nm), with a larger surface to volume ratio, are found to exhibit a striping pattern, which suggests surface energy can dominate below a critical dimension. When increasing force is applied through the AFM tip to strain the LCO islands, significant shifts in current flow are observed, and underlying mechanisms for this behavior are discussed. The c-AFM images are compared with photoemission electron microscopy images, which are used to acquire statistics across hundreds of particles. The results indicate that strain and morphology become more critical to electrochemical performance as particles approach nanometer dimensions.
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Metadata
- Type
- article
- Language
- en
- Landing Page
- https://doi.org/10.1021/acsnano.2c05594
- OA Status
- green
- Cited By
- 14
- References
- 29
- Related Works
- 10
- OpenAlex ID
- https://openalex.org/W4296545203
All OpenAlex metadata
Raw OpenAlex JSON
- OpenAlex ID
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https://openalex.org/W4296545203Canonical identifier for this work in OpenAlex
- DOI
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https://doi.org/10.1021/acsnano.2c05594Digital Object Identifier
- Title
-
Imaging Phase Segregation in Nanoscale LixCoO2 Single ParticlesWork title
- Type
-
articleOpenAlex work type
- Language
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enPrimary language
- Publication year
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2022Year of publication
- Publication date
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2022-09-21Full publication date if available
- Authors
-
Elliot J. Fuller, David S. Ashby, C. Polop, Elena Salagre, Bhuvsmita Bhargava, Yueming Song, E. Vasco, Joshua D. Sugar, Paul Albertus, Tevfik Onur Menteş, Andrea Locatelli, P. Segovia, M.A. González, A. Mascaraque, E. G. Michel, A. Alec TalinList of authors in order
- Landing page
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https://doi.org/10.1021/acsnano.2c05594Publisher landing page
- Open access
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YesWhether a free full text is available
- OA status
-
greenOpen access status per OpenAlex
- OA URL
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https://www.osti.gov/servlets/purl/2008143Direct OA link when available
- Concepts
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Materials science, Nanoscopic scale, Phase (matter), Nanotechnology, Crystallography, Physics, Chemistry, Quantum mechanicsTop concepts (fields/topics) attached by OpenAlex
- Cited by
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14Total citation count in OpenAlex
- Citations by year (recent)
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2025: 8, 2024: 4, 2023: 2Per-year citation counts (last 5 years)
- References (count)
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29Number of works referenced by this work
- Related works (count)
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10Other works algorithmically related by OpenAlex
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| abstract_inverted_index.become | 273 |
| abstract_inverted_index.common | 4 |
| abstract_inverted_index.energy | 210 |
| abstract_inverted_index.higher | 171 |
| abstract_inverted_index.images | 248 |
| abstract_inverted_index.island | 137 |
| abstract_inverted_index.larger | 175, 195 |
| abstract_inverted_index.memory | 26 |
| abstract_inverted_index.phases | 62 |
| abstract_inverted_index.pulsed | 108 |
| abstract_inverted_index.random | 24 |
| abstract_inverted_index.ratio, | 199 |
| abstract_inverted_index.scale. | 78 |
| abstract_inverted_index.shifts | 232 |
| abstract_inverted_index.state. | 188 |
| abstract_inverted_index.strain | 71, 227, 270 |
| abstract_inverted_index.volume | 198 |
| abstract_inverted_index.(c-AFM) | 121 |
| abstract_inverted_index.Thinner | 189 |
| abstract_inverted_index.acquire | 260 |
| abstract_inverted_index.applied | 221 |
| abstract_inverted_index.battery | 5, 51, 86 |
| abstract_inverted_index.cathode | 6 |
| abstract_inverted_index.current | 234 |
| abstract_inverted_index.cycling | 30, 113 |
| abstract_inverted_index.diagram | 46 |
| abstract_inverted_index.effects | 69, 81 |
| abstract_inverted_index.emerged | 11 |
| abstract_inverted_index.exhibit | 203 |
| abstract_inverted_index.images, | 255 |
| abstract_inverted_index.islands | 105, 168, 190 |
| abstract_inverted_index.observe | 140 |
| abstract_inverted_index.overall | 180 |
| abstract_inverted_index.phases. | 133 |
| abstract_inverted_index.present | 160 |
| abstract_inverted_index.propose | 156 |
| abstract_inverted_index.remains | 58 |
| abstract_inverted_index.results | 163, 267 |
| abstract_inverted_index.smaller | 166 |
| abstract_inverted_index.spatial | 127 |
| abstract_inverted_index.studied | 55 |
| abstract_inverted_index.surface | 196, 209 |
| abstract_inverted_index.through | 222 |
| abstract_inverted_index.unclear | 59 |
| abstract_inverted_index.(ECRAM). | 27 |
| abstract_inverted_index.analysis | 162 |
| abstract_inverted_index.approach | 281 |
| abstract_inverted_index.arrested | 143 |
| abstract_inverted_index.behavior | 243 |
| abstract_inverted_index.boundary | 149 |
| abstract_inverted_index.compared | 250 |
| abstract_inverted_index.critical | 83, 215, 275 |
| abstract_inverted_index.dominate | 212 |
| abstract_inverted_index.electron | 40, 253 |
| abstract_inverted_index.ensemble | 49 |
| abstract_inverted_index.exhibits | 32 |
| abstract_inverted_index.fraction | 173, 182 |
| abstract_inverted_index.hundreds | 263 |
| abstract_inverted_index.indicate | 268 |
| abstract_inverted_index.islands, | 116, 177, 230 |
| abstract_inverted_index.material | 7, 15 |
| abstract_inverted_index.modeling | 85 |
| abstract_inverted_index.pattern, | 206 |
| abstract_inverted_index.recently | 10 |
| abstract_inverted_index.striping | 205 |
| abstract_inverted_index.suggests | 208 |
| abstract_inverted_index.epitaxial | 103 |
| abstract_inverted_index.including | 19 |
| abstract_inverted_index.isolated, | 102 |
| abstract_inverted_index.nanometer | 65, 282 |
| abstract_inverted_index.observed, | 237 |
| abstract_inverted_index.particles | 52, 280 |
| abstract_inverted_index.promising | 14 |
| abstract_inverted_index.Li-planes; | 154 |
| abstract_inverted_index.anisotropy | 74 |
| abstract_inverted_index.conductive | 117, 130, 172, 181 |
| abstract_inverted_index.consistent | 184 |
| abstract_inverted_index.dimension. | 216 |
| abstract_inverted_index.dimensions | 66 |
| abstract_inverted_index.discussed. | 245 |
| abstract_inverted_index.increasing | 218 |
| abstract_inverted_index.insulating | 132 |
| abstract_inverted_index.lithiation | 187 |
| abstract_inverted_index.mechanisms | 240 |
| abstract_inverted_index.microscopy | 120, 254 |
| abstract_inverted_index.morphology | 272 |
| abstract_inverted_index.particles. | 265 |
| abstract_inverted_index.predicting | 90 |
| abstract_inverted_index.statistics | 261 |
| abstract_inverted_index.underlying | 239 |
| abstract_inverted_index.complicated | 38 |
| abstract_inverted_index.deposition. | 110 |
| abstract_inverted_index.diffusional | 73 |
| abstract_inverted_index.dimensions. | 283 |
| abstract_inverted_index.investigate | 101 |
| abstract_inverted_index.kinetically | 142 |
| abstract_inverted_index.performance | 87, 94, 278 |
| abstract_inverted_index.scalability | 92 |
| abstract_inverted_index.significant | 231 |
| abstract_inverted_index.applications | 18 |
| abstract_inverted_index.correlation. | 41 |
| abstract_inverted_index.distribution | 128 |
| abstract_inverted_index.extensively, | 56 |
| abstract_inverted_index.thicknesses, | 138 |
| abstract_inverted_index.Understanding | 79 |
| abstract_inverted_index.perpendicular | 151 |
| abstract_inverted_index.photoemission | 252 |
| abstract_inverted_index.significantly | 37 |
| abstract_inverted_index.electrochemical | 23, 112, 277 |
| abstract_inverted_index.single-particle | 77 |
| abstract_inverted_index.transformations | 34 |
| abstract_inverted_index.charge-discharge | 29 |
| abstract_inverted_index.electrocatalysis | 20 |
| abstract_inverted_index.electrocatalysts | 96 |
| abstract_inverted_index.LiCoO<sub>2</sub> | 104 |
| abstract_inverted_index.Li<sub><i>x</i></sub>CoO<sub>2</sub> | 0 |
| cited_by_percentile_year.max | 99 |
| cited_by_percentile_year.min | 94 |
| corresponding_author_ids | https://openalex.org/A5012085818, https://openalex.org/A5033155792 |
| countries_distinct_count | 3 |
| institutions_distinct_count | 16 |
| corresponding_institution_ids | https://openalex.org/I192454743 |
| sustainable_development_goals[0].id | https://metadata.un.org/sdg/14 |
| sustainable_development_goals[0].score | 0.75 |
| sustainable_development_goals[0].display_name | Life below water |
| citation_normalized_percentile.value | 0.80906568 |
| citation_normalized_percentile.is_in_top_1_percent | False |
| citation_normalized_percentile.is_in_top_10_percent | False |