In situ Study of Au Nanoparticle Growth in a Mechanochemical-Aging-Based Synthesis Article Swipe
Austin J. Richard
,
M.J. Ferguson
,
Blaine G. Fiss
,
Hatem M. Titi
,
Jesús Valdez
,
Nikolas Provatas
,
Tomislav Friščić
,
Audrey Moores
·
YOU?
·
· 2022
· Open Access
·
· DOI: https://doi.org/10.26434/chemrxiv-2022-r3w01-v2
YOU?
·
· 2022
· Open Access
·
· DOI: https://doi.org/10.26434/chemrxiv-2022-r3w01-v2
As we strive to perform chemical transformations in a more sustainable fashion, inducing reactions through the absorption of mechanical energy has emerged as a highly successful approach. Due to the wide-ranging applications of gold nanoparticles (AuNPs), mechanochemical strategies have already been employed for their synthesis. However, we do not yet fully understand the underlying processes surrounding the gold salt reduction, nucleation and growth of AuNPs in the solid state. Herein, we present a mechanically activated aging synthesis of AuNPs, through a solid-state Turkevich reaction. Solid reactants are only briefly exposed to mechanical energy before being aged statically for a period of six weeks at different temperatures. The aging step grants a greater period of time to analyze the initial reduction and subsequent nanoparticle formation processes. During the aging period the reaction was monitored using a combination of X-ray photoelectron spectroscopy (XPS), diffuse reflectance spectroscopy (DRS), powder X-ray diffraction (PXRD) and transmission electron microscopy (TEM) to gain meaningful insights into the solid-state formation of gold nanoparticles.
Related Topics
Concepts
X-ray photoelectron spectroscopy
Nucleation
Nanoparticle
Colloidal gold
Materials science
Powder diffraction
Transmission electron microscopy
Chemical engineering
Nanotechnology
Electron diffraction
Spectroscopy
Diffraction
Chemistry
Crystallography
Organic chemistry
Optics
Physics
Engineering
Quantum mechanics
Metadata
- Type
- preprint
- Language
- en
- Landing Page
- https://doi.org/10.26434/chemrxiv-2022-r3w01-v2
- https://chemrxiv.org/engage/api-gateway/chemrxiv/assets/orp/resource/item/632b7026fee74e4492454476/original/in-situ-study-of-au-nanoparticle-growth-in-a-mechanochemical-aging-based-synthesis.pdf
- OA Status
- gold
- References
- 52
- Related Works
- 10
- OpenAlex ID
- https://openalex.org/W4296634943
All OpenAlex metadata
Raw OpenAlex JSON
- OpenAlex ID
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https://openalex.org/W4296634943Canonical identifier for this work in OpenAlex
- DOI
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https://doi.org/10.26434/chemrxiv-2022-r3w01-v2Digital Object Identifier
- Title
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In situ Study of Au Nanoparticle Growth in a Mechanochemical-Aging-Based SynthesisWork title
- Type
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preprintOpenAlex work type
- Language
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enPrimary language
- Publication year
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2022Year of publication
- Publication date
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2022-09-22Full publication date if available
- Authors
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Austin J. Richard, M.J. Ferguson, Blaine G. Fiss, Hatem M. Titi, Jesús Valdez, Nikolas Provatas, Tomislav Friščić, Audrey MooresList of authors in order
- Landing page
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https://doi.org/10.26434/chemrxiv-2022-r3w01-v2Publisher landing page
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https://chemrxiv.org/engage/api-gateway/chemrxiv/assets/orp/resource/item/632b7026fee74e4492454476/original/in-situ-study-of-au-nanoparticle-growth-in-a-mechanochemical-aging-based-synthesis.pdfDirect link to full text PDF
- Open access
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YesWhether a free full text is available
- OA status
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goldOpen access status per OpenAlex
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https://chemrxiv.org/engage/api-gateway/chemrxiv/assets/orp/resource/item/632b7026fee74e4492454476/original/in-situ-study-of-au-nanoparticle-growth-in-a-mechanochemical-aging-based-synthesis.pdfDirect OA link when available
- Concepts
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X-ray photoelectron spectroscopy, Nucleation, Nanoparticle, Colloidal gold, Materials science, Powder diffraction, Transmission electron microscopy, Chemical engineering, Nanotechnology, Electron diffraction, Spectroscopy, Diffraction, Chemistry, Crystallography, Organic chemistry, Optics, Physics, Engineering, Quantum mechanicsTop concepts (fields/topics) attached by OpenAlex
- Cited by
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0Total citation count in OpenAlex
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52Number of works referenced by this work
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10Other works algorithmically related by OpenAlex
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