Investigation of the Degree of Functionalization and Colloidal Stability of Shell‐by‐Shell Functionalized TiO2 Nanoparticles as a Function of Different Phosphonic Acid Chain Lengths Article Swipe
Lisa M. S. Stiegler
,
Vincent Wedler
,
İdil Büküşoğlu
,
Andreas Hirsch
,
Wolfgang Peukert
,
Johannes Walter
·
YOU?
·
· 2025
· Open Access
·
· DOI: https://doi.org/10.1002/chem.202501008
YOU?
·
· 2025
· Open Access
·
· DOI: https://doi.org/10.1002/chem.202501008
In this work, a series of Shell‐by‐Shell ( SbS )‐functionalized colloidal systems consisting of 6 nm TiO 2 anatase nanoparticles (NPs), one of the phosphonic acids (PAs) propylphosphonic acid (PAC 3 ), hexylphosphonic acid (PAC 6 ), dodecylphosphonic acid (PAC 12 ), tetradecylphosphonic acid (PAC 14 ), hexadecylphosphonic acid (PAC 16 ), octadecylphosphonic acid (PAC 18 ) and the amphiphile sodium dodecylbenzenesulfonate (SDBS) were prepared, resulting in TiO 2 ‐PAC X @SDBS (X = 3, 6, 12, 14, 16, or 18) NPs dispersed in deionized water (DIW). During the whole functionalization process, the NPs were subjected to thermogravimetric analysis (TGA) to gain insights into their degree of functionalization and respective thermal stability. In addition, the colloidal stability of the NPs as a function of PA chain length was analyzed by analytical ultracentrifugation (AUC). By combining both TGA and AUC, it was found that the resulting hierarchical NP architectures form agglomerates, with the degree of agglomeration depending on the length of the PA used for the first‐shell functionalization. This allows conclusions to be drawn about the efficiency of the overlap between the PA and the SDBS carbon chains.
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- Type
- article
- Language
- en
- Landing Page
- https://doi.org/10.1002/chem.202501008
- https://onlinelibrary.wiley.com/doi/pdfdirect/10.1002/chem.202501008
- OA Status
- hybrid
- References
- 62
- Related Works
- 10
- OpenAlex ID
- https://openalex.org/W4410658361
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Raw OpenAlex JSON
- OpenAlex ID
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https://openalex.org/W4410658361Canonical identifier for this work in OpenAlex
- DOI
-
https://doi.org/10.1002/chem.202501008Digital Object Identifier
- Title
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Investigation of the Degree of Functionalization and Colloidal Stability of Shell‐by‐Shell Functionalized TiO2 Nanoparticles as a Function of Different Phosphonic Acid Chain LengthsWork title
- Type
-
articleOpenAlex work type
- Language
-
enPrimary language
- Publication year
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2025Year of publication
- Publication date
-
2025-05-23Full publication date if available
- Authors
-
Lisa M. S. Stiegler, Vincent Wedler, İdil Büküşoğlu, Andreas Hirsch, Wolfgang Peukert, Johannes WalterList of authors in order
- Landing page
-
https://doi.org/10.1002/chem.202501008Publisher landing page
- PDF URL
-
https://onlinelibrary.wiley.com/doi/pdfdirect/10.1002/chem.202501008Direct link to full text PDF
- Open access
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YesWhether a free full text is available
- OA status
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hybridOpen access status per OpenAlex
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https://onlinelibrary.wiley.com/doi/pdfdirect/10.1002/chem.202501008Direct OA link when available
- Concepts
-
Surface modification, Thermogravimetric analysis, Sodium dodecylbenzenesulfonate, Colloid, Anatase, Chemical engineering, Nanoparticle, Thermal stability, Chemistry, Materials science, Polymer chemistry, Nanotechnology, Organic chemistry, Aqueous solution, Catalysis, Engineering, PhotocatalysisTop concepts (fields/topics) attached by OpenAlex
- Cited by
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0Total citation count in OpenAlex
- References (count)
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62Number of works referenced by this work
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10Other works algorithmically related by OpenAlex
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