Ion Pair-Dispersive Liquid-Liquid Microextraction Coupled to Microsample Injection System-Flame Atomic Absorption Spectrometry For Determination of Gold at Trace Level in Real Samples Article Swipe

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Latif Elçı , Ayşen Höl , Aslıhan Arslan Kartal , Abdullah Akdoğan , Aydan Elçi , Taner Arslan ·

YOU? · · 2015 · Open Access · · DOI: https://doi.org/10.17344/acsi.2014.897

A novel ion pair-dispersive liquid-liquid microextraction (IP-DLLME) of gold followed by its determination with microsample injection system-flame atomic absorption spectrometry (MIS-FAAS) detection was developed. The extraction method was based on the reaction of anionic tetrachloro gold(III) complex with the cationic form of Rhodamine B to give a violet ion pair complex, which is extracted from 1.0 mol L(-1) HCl solution of 8.0 mL to fine droplets of chloroform of 500 µL. A Plackett-Burman experimental design of MINITAB statistical program was employed to optimize the influence of main parameters to be controlled in DLLME. After optimizing the extraction conditions, gold was quantitatively recovered by preconcentration factor of 40, limit of detection (LOD) of 1.8 μg L(-1) and relative standard deviation of less than 6.8%. The proposed method was successfully applied to the preconcentration and determination of gold in some samples such as tap water, waste water, copper electrolysis solution and copper wire coated nickel.

Related Topics

Chemistry

Extraction (Chemistry)

Tap Water

Copper

Chromatography

Atomic Absorption Spectroscopy

Chloroform

Response Surface Methodology

Physics

Engineering

Organic Chemistry

Environmental Engineering

Concepts

Detection limit Chemistry Extraction (chemistry) Tap water Copper Chromatography Analytical Chemistry (journal) Trace Amounts Atomic absorption spectroscopy Plackett–Burman design Chloroform Enrichment factor Response surface methodology Physics Engineering Organic chemistry Environmental engineering Medicine Alternative medicine Quantum mechanics Pathology

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Type: article
Language: en
Landing Page: https://doi.org/10.17344/acsi.2014.897
PDF: https://journals.matheo.si/index.php/ACSi/article/download/897/422
OA Status: diamond
Cited By: 15
References: 34
Related Works: 10
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DOI: https://doi.org/10.17344/acsi.2014.897

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Title: Ion Pair-Dispersive Liquid-Liquid Microextraction Coupled to Microsample Injection System-Flame Atomic Absorption Spectrometry For Determination of Gold at Trace Level in Real Samples

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Type: article

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Language: en

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Publication year: 2015

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Publication date: 2015-03-15

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Authors: Latif Elçı, Ayşen Höl, Aslıhan Arslan Kartal, Abdullah Akdoğan, Aydan Elçi, Taner Arslan

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Landing page: https://doi.org/10.17344/acsi.2014.897

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PDF URL: https://journals.matheo.si/index.php/ACSi/article/download/897/422

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Concepts: Detection limit, Chemistry, Extraction (chemistry), Tap water, Copper, Chromatography, Analytical Chemistry (journal), Trace Amounts, Atomic absorption spectroscopy, Plackett–Burman design, Chloroform, Enrichment factor, Response surface methodology, Physics, Engineering, Organic chemistry, Environmental engineering, Medicine, Alternative medicine, Quantum mechanics, Pathology

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Cited by: 15

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Citations by year (recent): 2025: 2, 2024: 1, 2023: 1, 2022: 1, 2020: 3

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