Ionic Liquid‐Mediated Oxidative Degradation of Polycaprolactone into Adipic Acids over Pt/TiO2 in Water Article Swipe
Yusi Wang
,
Hui Zhang
,
Wei Zeng
,
Yanfei Zhao
,
Rongxiang Li
,
Minhao Tang
,
Buxing Han
,
Zhimin Liu
·
YOU?
·
· 2025
· Open Access
·
· DOI: https://doi.org/10.1002/anie.202424236
YOU?
·
· 2025
· Open Access
·
· DOI: https://doi.org/10.1002/anie.202424236
Upgrading polyester waste into high value‐added chemicals can achieve carbon recycling, which is of great significance for sustainable development. Herein, we report a one‐pot protocol to oxidatively degrade polycaprolactone (PCL) with air into adipic acid (AA) mediated by ionic liquid (IL, e.g., 1‐butyl‐3‐methylimidazolium bis(trifluoromethylsulfonyl)imide, [BMIm][NTf 2 ]) in water. In this protocol, IL catalyzes the hydrolysis of PCL into 6‐hydroxyhexanoic acid (6‐HHA) and further mediates the oxidation of 6‐HHA into AA over TiO 2 ‐supported Pt nanocatalysts, reaching the highest AA yield of 85.6% under relatively mild conditions (140 °C, 1.5 MPa). Mechanism investigation indicates that both O 2 •– and •OH derived from oxygen and water are involved in the oxidation of 6‐HHA to form 6‐oxohexanoic acid via two pathways, which further convert into AA. The IL inhibits the overoxidation of AA, thus leading to a high selectivity toward AA. This protocol provides a green and feasible way to degrade PCL and also to access AA.
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- Type
- article
- Language
- en
- Landing Page
- https://doi.org/10.1002/anie.202424236
- https://onlinelibrary.wiley.com/doi/pdfdirect/10.1002/anie.202424236
- OA Status
- bronze
- Cited By
- 1
- References
- 57
- Related Works
- 10
- OpenAlex ID
- https://openalex.org/W4408070501
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- DOI
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https://doi.org/10.1002/anie.202424236Digital Object Identifier
- Title
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Ionic Liquid‐Mediated Oxidative Degradation of Polycaprolactone into Adipic Acids over Pt/TiO2 in WaterWork title
- Type
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articleOpenAlex work type
- Language
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enPrimary language
- Publication year
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2025Year of publication
- Publication date
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2025-03-10Full publication date if available
- Authors
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Yusi Wang, Hui Zhang, Wei Zeng, Yanfei Zhao, Rongxiang Li, Minhao Tang, Buxing Han, Zhimin LiuList of authors in order
- Landing page
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https://doi.org/10.1002/anie.202424236Publisher landing page
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https://onlinelibrary.wiley.com/doi/pdfdirect/10.1002/anie.202424236Direct link to full text PDF
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bronzeOpen access status per OpenAlex
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https://onlinelibrary.wiley.com/doi/pdfdirect/10.1002/anie.202424236Direct OA link when available
- Concepts
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Ionic liquid, Degradation (telecommunications), Polycaprolactone, Oxidative phosphorylation, Adipic acid, Ionic bonding, Chemistry, Chemical engineering, Polymer chemistry, Organic chemistry, Materials science, Catalysis, Biochemistry, Ion, Computer science, Polymer, Engineering, TelecommunicationsTop concepts (fields/topics) attached by OpenAlex
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1Total citation count in OpenAlex
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2025: 1Per-year citation counts (last 5 years)
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10Other works algorithmically related by OpenAlex
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| abstract_inverted_index.overoxidation | 131 |
| abstract_inverted_index.value‐added | 6 |
| abstract_inverted_index.nanocatalysts, | 77 |
| abstract_inverted_index.6‐oxohexanoic | 117 |
| abstract_inverted_index.polycaprolactone | 29 |
| abstract_inverted_index.6‐hydroxyhexanoic | 60 |
| abstract_inverted_index.1‐butyl‐3‐methylimidazolium | 43 |
| abstract_inverted_index.bis(trifluoromethylsulfonyl)imide, | 44 |
| cited_by_percentile_year.max | 95 |
| cited_by_percentile_year.min | 91 |
| countries_distinct_count | 1 |
| institutions_distinct_count | 8 |
| citation_normalized_percentile.value | 0.60827436 |
| citation_normalized_percentile.is_in_top_1_percent | False |
| citation_normalized_percentile.is_in_top_10_percent | False |