Liquid‐Phase Synthesis of Halide Solid Electrolytes for All‐Solid‐State Batteries Using Organic Solvents Article Swipe
Hirotada Gamo
,
Mitsunori Kitta
,
Nobuhiko Takeichi
·
YOU?
·
· 2025
· Open Access
·
· DOI: https://doi.org/10.1002/eem2.70184
YOU?
·
· 2025
· Open Access
·
· DOI: https://doi.org/10.1002/eem2.70184
Halide solid electrolytes (SEs) show high ionic conductivity and good compatibility with cathode active materials, providing long‐life all‐solid‐state lithium‐ion batteries (ASSLIBs). Liquid‐phase synthesis technology is a feasible option for the large‐scale manufacturing of halide SEs. However, no leading liquid‐phase synthesis method for halide SEs has been developed because of a limited understanding of the solvent effect on the formation of halide SEs. Herein, a scalable and universal liquid‐phase synthesis method for halide SEs using organic solvents is reported. The Li 3− x YCl 6− x SEs synthesized via pyridine transform trigonal structure to metastable orthorhombic structure as the Li concentration decreases, forming a highly pure orthorhombic phase with an ionic conductivity of 1.3 × 10 −4 S cm −1 at 25 °C in the composition of x = 1. Spectroscopic analysis indicates that pyridine acts as a reducing ligand, stabilizing the orthorhombic Li 2 YCl 5 by modulating the valence state of yttrium ions. Additionally, the developed synthesis method is extended to the synthesis of bromide SEs with high ionic conductivity. ASSLIBs using LiNi 0.8 Co 0.1 Mn 0.1 O 2 ‐Li 2 YCl 5 cathode composites demonstrate good cycling stability for 100 cycles. The liquid‐phase synthesis technology reported here opens opportunities for the practical manufacturing of halide‐based ASSLIBs.
Related Topics
Concepts
Halide
Orthorhombic crystal system
Ionic conductivity
Inorganic chemistry
Electrolyte
Materials science
Pyridine
Bromide
Cathode
Ionic bonding
Chemical engineering
Fast ion conductor
Solvent
Conductivity
Yttrium
Ionic liquid
Chemistry
Iodide
Trifluoromethanesulfonate
Anode
Tin
Dissociation (chemistry)
Metadata
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- article
- Language
- en
- Landing Page
- https://doi.org/10.1002/eem2.70184
- OA Status
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- References
- 41
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- https://openalex.org/W7105664106
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https://doi.org/10.1002/eem2.70184Digital Object Identifier
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Liquid‐Phase Synthesis of Halide Solid Electrolytes for All‐Solid‐State Batteries Using Organic SolventsWork title
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articleOpenAlex work type
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enPrimary language
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2025Year of publication
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2025-11-14Full publication date if available
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Hirotada Gamo, Mitsunori Kitta, Nobuhiko TakeichiList of authors in order
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https://doi.org/10.1002/eem2.70184Publisher landing page
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YesWhether a free full text is available
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hybridOpen access status per OpenAlex
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https://doi.org/10.1002/eem2.70184Direct OA link when available
- Concepts
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Halide, Orthorhombic crystal system, Ionic conductivity, Inorganic chemistry, Electrolyte, Materials science, Pyridine, Bromide, Cathode, Ionic bonding, Chemical engineering, Fast ion conductor, Solvent, Conductivity, Yttrium, Ionic liquid, Chemistry, Iodide, Trifluoromethanesulfonate, Anode, Tin, Dissociation (chemistry)Top concepts (fields/topics) attached by OpenAlex
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0Total citation count in OpenAlex
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| abstract_inverted_index.1. | 128 |
| abstract_inverted_index.10 | 114 |
| abstract_inverted_index.25 | 120 |
| abstract_inverted_index.Co | 175 |
| abstract_inverted_index.Li | 79, 98, 142 |
| abstract_inverted_index.Mn | 177 |
| abstract_inverted_index.an | 108 |
| abstract_inverted_index.as | 96, 135 |
| abstract_inverted_index.at | 119 |
| abstract_inverted_index.by | 146 |
| abstract_inverted_index.cm | 117 |
| abstract_inverted_index.in | 122 |
| abstract_inverted_index.is | 24, 76, 159 |
| abstract_inverted_index.no | 36 |
| abstract_inverted_index.of | 32, 48, 52, 59, 111, 125, 151, 164, 206 |
| abstract_inverted_index.on | 56 |
| abstract_inverted_index.to | 92, 161 |
| abstract_inverted_index.× | 113 |
| abstract_inverted_index.0.1 | 176, 178 |
| abstract_inverted_index.0.8 | 174 |
| abstract_inverted_index.1.3 | 112 |
| abstract_inverted_index.100 | 192 |
| abstract_inverted_index.SEs | 43, 72, 85, 166 |
| abstract_inverted_index.The | 78, 194 |
| abstract_inverted_index.YCl | 82, 144, 183 |
| abstract_inverted_index.and | 8, 65 |
| abstract_inverted_index.for | 28, 41, 70, 191, 202 |
| abstract_inverted_index.has | 44 |
| abstract_inverted_index.the | 29, 53, 57, 97, 123, 140, 148, 155, 162, 203 |
| abstract_inverted_index.via | 87 |
| abstract_inverted_index.°C | 121 |
| abstract_inverted_index.3− | 80 |
| abstract_inverted_index.6− | 83 |
| abstract_inverted_index.LiNi | 173 |
| abstract_inverted_index.SEs. | 34, 61 |
| abstract_inverted_index.acts | 134 |
| abstract_inverted_index.been | 45 |
| abstract_inverted_index.good | 9, 188 |
| abstract_inverted_index.here | 199 |
| abstract_inverted_index.high | 5, 168 |
| abstract_inverted_index.pure | 104 |
| abstract_inverted_index.show | 4 |
| abstract_inverted_index.that | 132 |
| abstract_inverted_index.with | 11, 107, 167 |
| abstract_inverted_index.−1 | 118 |
| abstract_inverted_index.−4 | 115 |
| abstract_inverted_index.(SEs) | 3 |
| abstract_inverted_index.ionic | 6, 109, 169 |
| abstract_inverted_index.ions. | 153 |
| abstract_inverted_index.opens | 200 |
| abstract_inverted_index.phase | 106 |
| abstract_inverted_index.solid | 1 |
| abstract_inverted_index.state | 150 |
| abstract_inverted_index.using | 73, 172 |
| abstract_inverted_index.‐Li | 181 |
| abstract_inverted_index.Halide | 0 |
| abstract_inverted_index.active | 13 |
| abstract_inverted_index.effect | 55 |
| abstract_inverted_index.halide | 33, 42, 60, 71 |
| abstract_inverted_index.highly | 103 |
| abstract_inverted_index.method | 40, 69, 158 |
| abstract_inverted_index.option | 27 |
| abstract_inverted_index.ASSLIBs | 171 |
| abstract_inverted_index.Herein, | 62 |
| abstract_inverted_index.because | 47 |
| abstract_inverted_index.bromide | 165 |
| abstract_inverted_index.cathode | 12, 185 |
| abstract_inverted_index.cycles. | 193 |
| abstract_inverted_index.cycling | 189 |
| abstract_inverted_index.forming | 101 |
| abstract_inverted_index.leading | 37 |
| abstract_inverted_index.ligand, | 138 |
| abstract_inverted_index.limited | 50 |
| abstract_inverted_index.organic | 74 |
| abstract_inverted_index.solvent | 54 |
| abstract_inverted_index.valence | 149 |
| abstract_inverted_index.yttrium | 152 |
| abstract_inverted_index.ASSLIBs. | 208 |
| abstract_inverted_index.However, | 35 |
| abstract_inverted_index.analysis | 130 |
| abstract_inverted_index.extended | 160 |
| abstract_inverted_index.feasible | 26 |
| abstract_inverted_index.pyridine | 88, 133 |
| abstract_inverted_index.reducing | 137 |
| abstract_inverted_index.reported | 198 |
| abstract_inverted_index.scalable | 64 |
| abstract_inverted_index.solvents | 75 |
| abstract_inverted_index.trigonal | 90 |
| abstract_inverted_index.batteries | 19 |
| abstract_inverted_index.developed | 46, 156 |
| abstract_inverted_index.formation | 58 |
| abstract_inverted_index.indicates | 131 |
| abstract_inverted_index.practical | 204 |
| abstract_inverted_index.providing | 15 |
| abstract_inverted_index.reported. | 77 |
| abstract_inverted_index.stability | 190 |
| abstract_inverted_index.structure | 91, 95 |
| abstract_inverted_index.synthesis | 22, 39, 68, 157, 163, 196 |
| abstract_inverted_index.transform | 89 |
| abstract_inverted_index.universal | 66 |
| abstract_inverted_index.(ASSLIBs). | 20 |
| abstract_inverted_index.composites | 186 |
| abstract_inverted_index.decreases, | 100 |
| abstract_inverted_index.materials, | 14 |
| abstract_inverted_index.metastable | 93 |
| abstract_inverted_index.modulating | 147 |
| abstract_inverted_index.technology | 23, 197 |
| abstract_inverted_index.composition | 124 |
| abstract_inverted_index.demonstrate | 187 |
| abstract_inverted_index.long‐life | 16 |
| abstract_inverted_index.stabilizing | 139 |
| abstract_inverted_index.synthesized | 86 |
| abstract_inverted_index.conductivity | 7, 110 |
| abstract_inverted_index.electrolytes | 2 |
| abstract_inverted_index.orthorhombic | 94, 105, 141 |
| abstract_inverted_index.Additionally, | 154 |
| abstract_inverted_index.Spectroscopic | 129 |
| abstract_inverted_index.compatibility | 10 |
| abstract_inverted_index.concentration | 99 |
| abstract_inverted_index.conductivity. | 170 |
| abstract_inverted_index.large‐scale | 30 |
| abstract_inverted_index.lithium‐ion | 18 |
| abstract_inverted_index.manufacturing | 31, 205 |
| abstract_inverted_index.opportunities | 201 |
| abstract_inverted_index.understanding | 51 |
| abstract_inverted_index.Liquid‐phase | 21 |
| abstract_inverted_index.halide‐based | 207 |
| abstract_inverted_index.liquid‐phase | 38, 67, 195 |
| abstract_inverted_index.all‐solid‐state | 17 |
| cited_by_percentile_year | |
| countries_distinct_count | 1 |
| institutions_distinct_count | 3 |
| citation_normalized_percentile.value | 0.74831919 |
| citation_normalized_percentile.is_in_top_1_percent | False |
| citation_normalized_percentile.is_in_top_10_percent | False |