Lithium recovery in a batch adsorption study: Synthesis, characterization, optimization, regeneration, kinetics, and isotherm studies Article Swipe
Baker Nasser Saleh Al-dhawi
,
S. R. M. Kutty
,
Aawag Mohsen Alawag
,
Najib Mohammed Yahya Almahbashi
,
Wahid Ali Hamood Altowayti
,
Abdullah Saleh Algamili
,
Ahmad Hussaini Jagaba
,
Abdullahi Haruna Birniwa
·
YOU?
·
· 2024
· Open Access
·
· DOI: https://doi.org/10.1016/j.sciaf.2024.e02449
YOU?
·
· 2024
· Open Access
·
· DOI: https://doi.org/10.1016/j.sciaf.2024.e02449
Lithium (Li)recovery is significant due to an increasing need for Li in diverse applications, particularly in the energy storage domain. In this study, a synthesized adsorbent was developed and utilized to efficiently recover Li. Therefore, this research aims to assess the effectiveness of using the synthesized adsorbent LiHMO to recover Li from the aqueous solution. The surface area and characteristics of the synthesized adsorbent were subjected to analysis utilizing different methods and techniques, including scanning electron microscopy (FESEM), X-ray diffraction (XRD), Brunauer-Emmett-Teller (BET) analysis, and Fourier-transform infrared spectroscopy (FTIR). The findings indicated that the synthesized adsorbent demonstrated exceptional adsorption capabilities for Li recovery. Characterization analysis revealed a well-defined porous structure and functional groups on the adsorbent's surface, facilitating adsorption. The surface area of the adsorbent was determined to be 25.54 m²/g, providing a substantial active surface for adsorption processes. The Box-Behnken response surface method (RSM) was utilized to optimize the recovery process for key factors such as pH, adsorbent dose, time, and concentration. The critical operating parameters identified included a pH of 4, initial concentration of 900 mg/L, contact time of 460 min, and adsorbent dosage of 1300 mg/L. The obtained data were analyzed using a quadratic model, yielding an R² value of 0.9538, indicating that the adsorbent is effective in Li adsorption. The optimal conditions for maximizing Li recovery were found to be 95 % and 89 % for maximum and minimum recovery, respectively. The amount of adsorbate adsorbed (qe) was determined to be 6.2 mg g-1. Various kinetic models and isotherms were utilized to conform to these parameters. The Freundlich isotherm and the intraparticle diffusion model showed strong fits, as evidenced by their R² results of 0.9876 and 0.9862, respectively. The kinetic study suggested that the intraparticle-diffusion model best explained the adsorption process, indicating chemisorption as the rate-limiting step. The equilibrium data fitted well with the Freundlich isotherm, suggesting multilayer adsorption with heterogeneous surface energies. Furthermore, the study assessed the adsorbent's regeneration potential, finding that the first cycle of regeneration achieved 91.9 % efficiency, while the fifth cycle maintained a high efficiency of 89.7 %, indicating good reusability of the adsorbent. The study's findings showcase the efficiency of the synthesized adsorbent LiHMO in Li recovery from aqueous solutions, offering valuable information about the best conditions for the adsorption process. As a result of its superior sorption capacity and high recovery of adsorbed Li, the LiHMO adsorbent was selected as the optimal choice for Li recovery from aqueous solutions.
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- Type
- article
- Language
- en
- Landing Page
- https://doi.org/10.1016/j.sciaf.2024.e02449
- OA Status
- gold
- Cited By
- 3
- References
- 66
- Related Works
- 10
- OpenAlex ID
- https://openalex.org/W4403990522
All OpenAlex metadata
Raw OpenAlex JSON
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https://openalex.org/W4403990522Canonical identifier for this work in OpenAlex
- DOI
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https://doi.org/10.1016/j.sciaf.2024.e02449Digital Object Identifier
- Title
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Lithium recovery in a batch adsorption study: Synthesis, characterization, optimization, regeneration, kinetics, and isotherm studiesWork title
- Type
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articleOpenAlex work type
- Language
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enPrimary language
- Publication year
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2024Year of publication
- Publication date
-
2024-11-01Full publication date if available
- Authors
-
Baker Nasser Saleh Al-dhawi, S. R. M. Kutty, Aawag Mohsen Alawag, Najib Mohammed Yahya Almahbashi, Wahid Ali Hamood Altowayti, Abdullah Saleh Algamili, Ahmad Hussaini Jagaba, Abdullahi Haruna BirniwaList of authors in order
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https://doi.org/10.1016/j.sciaf.2024.e02449Publisher landing page
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YesWhether a free full text is available
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goldOpen access status per OpenAlex
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https://doi.org/10.1016/j.sciaf.2024.e02449Direct OA link when available
- Concepts
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Kinetics, Adsorption, Characterization (materials science), Lithium (medication), Chemical engineering, Materials science, Chemistry, Regeneration (biology), Sorption isotherm, Nanotechnology, Physical chemistry, Engineering, Physics, Medicine, Biology, Internal medicine, Quantum mechanics, Cell biologyTop concepts (fields/topics) attached by OpenAlex
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3Total citation count in OpenAlex
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2025: 3Per-year citation counts (last 5 years)
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66Number of works referenced by this work
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10Other works algorithmically related by OpenAlex
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| primary_location.landing_page_url | https://doi.org/10.1016/j.sciaf.2024.e02449 |
| publication_date | 2024-11-01 |
| publication_year | 2024 |
| referenced_works | https://openalex.org/W4283398817, https://openalex.org/W4288069221, https://openalex.org/W6852605536, https://openalex.org/W3191588010, https://openalex.org/W4312208471, https://openalex.org/W3091732986, https://openalex.org/W4286484258, https://openalex.org/W4284892580, https://openalex.org/W2972307200, https://openalex.org/W3138061517, https://openalex.org/W4386498835, https://openalex.org/W4320919972, https://openalex.org/W4399666716, https://openalex.org/W4322762442, https://openalex.org/W4213389581, https://openalex.org/W4366991949, https://openalex.org/W7025188983, https://openalex.org/W3026157797, https://openalex.org/W3010408268, https://openalex.org/W2916252188, https://openalex.org/W2113606704, https://openalex.org/W2930216851, https://openalex.org/W3095091066, https://openalex.org/W4387345622, https://openalex.org/W4388817583, https://openalex.org/W6688024308, https://openalex.org/W2112017750, https://openalex.org/W1986113254, https://openalex.org/W2293657740, https://openalex.org/W2031439198, https://openalex.org/W2567291156, https://openalex.org/W2007517290, https://openalex.org/W6649335225, https://openalex.org/W2155256513, https://openalex.org/W1984030839, https://openalex.org/W2040089921, https://openalex.org/W3088866531, https://openalex.org/W4394779363, https://openalex.org/W4400424364, https://openalex.org/W6810266613, https://openalex.org/W2966693206, https://openalex.org/W3209934957, https://openalex.org/W2019951926, https://openalex.org/W4213316793, https://openalex.org/W4283071725, https://openalex.org/W3094884678, https://openalex.org/W6858240982, https://openalex.org/W3211605142, https://openalex.org/W3034949438, https://openalex.org/W3138113954, https://openalex.org/W4309744811, https://openalex.org/W4200491531, https://openalex.org/W4379931636, https://openalex.org/W4319081413, https://openalex.org/W3087771167, https://openalex.org/W2898912843, https://openalex.org/W2967048849, https://openalex.org/W3115462246, https://openalex.org/W4366286103, https://openalex.org/W3113015791, https://openalex.org/W6839493273, https://openalex.org/W3042204241, https://openalex.org/W4223900617, https://openalex.org/W4283780356, https://openalex.org/W2212997086, https://openalex.org/W1996619669 |
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| abstract_inverted_index.showed | 268 |
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