Microstructural Stability of IN625 Reinforced by the Addition of TiC Produced by Laser Powder Bed Fusion after Prolonged Thermal Exposure Article Swipe
Serena Lerda
,
Giulio Marchese
,
Emilio Bassini
,
Mariangela Lombardi
,
Daniele Ugues
,
Paolo Fino
,
Sara Biamino
·
YOU?
·
· 2024
· Open Access
·
· DOI: https://doi.org/10.3390/ma17184532
YOU?
·
· 2024
· Open Access
·
· DOI: https://doi.org/10.3390/ma17184532
This paper deals with the development and characterization of an Inconel 625 (IN625) reinforced with 2 wt.% of sub-micrometrical TiC particles produced by the laser powder bed fusion (LPBF) process. IN625 and IN625 2 wt.% TiC microstructural evolution was evaluated in the as-built, solution-annealed (2 h at 1150 °C), and prolonged heat-treated (2 h at 1150 °C + 100 h at 1000 °C) conditions. The IN625 and IN625 + TiC samples were successfully produced with low residual porosity (<0.15%). In the as-built conditions, both materials developed mainly columnar grains elongated to the building direction with melt pools, fine dendric structures, and small fractions of recrystallized grains. Some TiC segregations were observed in the composite, preferentially located at the melt pool boundaries. The heat treatments led to a different microstructural evolution between the base alloy and the composite. After solution annealing, the IN625 alloy was subjected to full recrystallization with a drastic reduction in hardness. Afterward, the prolonged thermal exposures for 100 h at 1000 °C provoked the formation of carbides, increasing the hardness. On the contrary, the composite retained the as-built microstructure with columnar grains in the solution-annealed and prolonged heat-treated conditions, revealing a limited formation and growth of carbides, thus resulting in a reduced hardness variation. The addition of TiC inside the IN625 enhanced the microstructural stability of the composite, preventing the recrystallization and the growth of phases occurring under prolonged thermal exposures. The current study therefore reported the effect of TiC particles on the microstructural stabilization of LPBFed IN625, with a peculiar focus on the prolonged thermal exposure at 1000 °C.
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- Type
- article
- Language
- en
- Landing Page
- http://doi.org/10.3390/ma17184532
- OA Status
- gold
- References
- 38
- Related Works
- 10
- OpenAlex ID
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Raw OpenAlex JSON
- OpenAlex ID
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https://openalex.org/W4402793440Canonical identifier for this work in OpenAlex
- DOI
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https://doi.org/10.3390/ma17184532Digital Object Identifier
- Title
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Microstructural Stability of IN625 Reinforced by the Addition of TiC Produced by Laser Powder Bed Fusion after Prolonged Thermal ExposureWork title
- Type
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articleOpenAlex work type
- Language
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enPrimary language
- Publication year
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2024Year of publication
- Publication date
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2024-09-14Full publication date if available
- Authors
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Serena Lerda, Giulio Marchese, Emilio Bassini, Mariangela Lombardi, Daniele Ugues, Paolo Fino, Sara BiaminoList of authors in order
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https://doi.org/10.3390/ma17184532Publisher landing page
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YesWhether a free full text is available
- OA status
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goldOpen access status per OpenAlex
- OA URL
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https://doi.org/10.3390/ma17184532Direct OA link when available
- Concepts
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Materials science, Fusion, Thermal stability, Composite material, Thermal, Metallurgy, Laser, Microstructure, Chemical engineering, Thermodynamics, Optics, Physics, Linguistics, Philosophy, EngineeringTop concepts (fields/topics) attached by OpenAlex
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0Total citation count in OpenAlex
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38Number of works referenced by this work
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10Other works algorithmically related by OpenAlex
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