Mobility Selective Ion Soft-Landing and Characterization Enabled Using Structures for Lossless Ion Manipulation Article Swipe

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Jung Yun Lee , Ailin Li , Venkateshkumar Prabhakaran , Xin Zhang , Christopher Harrilal , Libor Kovařík , Yehia Ibrahim , Richard Smith , Sandilya Garimella ·

YOU? · · 2024 · Open Access · · DOI: https://doi.org/10.1021/acs.analchem.3c04328

While conventional ion-soft landing uses the mass-to-charge (m/z) ratio to achieve molecular selection for deposition, here we demonstrate the use of Structures for Lossless Ion Manipulation (SLIM) for mobility-based ion selection and deposition. The dynamic rerouting capabilities of SLIM were leveraged to enable the rerouting of a selected range of mobilities to a different SLIM path (rather than MS) that terminated at a deposition surface. A selected mobility range from a phosphazene ion mixture was rerouted and deposited with a current pulse (∼150 pA) resembling its mobility peak. In addition, from a mixture of tetra-alkyl ammonium (TAA) ions containing chain lengths of C5-C8, selected chains (C6, C7) were collected on a surface, reconstituted into solution-phase, and subsequently analyzed with a SLIM-qToF to obtain an IMS/MS spectrum, confirming the identity of the selected species. Further, this method was used to characterize triply charged tungsten-polyoxometalate anions, PW₁₂O₄₀^3- (WPOM). The arrival time distribution of the IMS/MS showed multiple peaks associated with the triply charged anion (PW₁₂O₄₀^3-), of which a selected ATD was deposited and imaged using TEM. Additionally, the identity of the deposited WPOM was ascertained using energy-dispersive (EDS) spectroscopy. Further, we present theory and computations that reveal ion landing energies, the ability to modulate the energies, and deposition spot sizes.

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Chemistry Ion Ion-mobility spectrometry Deposition (geology) Analytical Chemistry (journal) Characterization (materials science) Polyoxometalate Range (aeronautics) Chemical physics Nanotechnology Materials science Organic chemistry Sediment Biology Paleontology Catalysis Composite material

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Type: article
Language: en
Landing Page: https://doi.org/10.1021/acs.analchem.3c04328
OA Status: green
Cited By: 3
References: 52
Related Works: 10
OpenAlex ID: https://openalex.org/W4391743547

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DOI: https://doi.org/10.1021/acs.analchem.3c04328

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Title: Mobility Selective Ion Soft-Landing and Characterization Enabled Using Structures for Lossless Ion Manipulation

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Language: en

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Publication year: 2024

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Publication date: 2024-02-12

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Authors: Jung Yun Lee, Ailin Li, Venkateshkumar Prabhakaran, Xin Zhang, Christopher Harrilal, Libor Kovařík, Yehia Ibrahim, Richard Smith, Sandilya Garimella

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Landing page: https://doi.org/10.1021/acs.analchem.3c04328

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OA URL: https://www.osti.gov/biblio/2441344

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Concepts: Chemistry, Ion, Ion-mobility spectrometry, Deposition (geology), Analytical Chemistry (journal), Characterization (materials science), Polyoxometalate, Range (aeronautics), Chemical physics, Nanotechnology, Materials science, Organic chemistry, Sediment, Biology, Paleontology, Catalysis, Composite material

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Cited by: 3

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Citations by year (recent): 2025: 1, 2024: 2

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