Modification and Patterning of Self‐Assembled Monolayers Using Electrogenerated Etchants and Homogeneous Scavenging Reactions in a Scanning Electrochemical Microscope Article Swipe
Britta Vaske
,
Maximilian Schaube
,
Frank Meiners
,
Jan Henning Ross
,
Jens Christoffers
,
Günther Wittstock
·
YOU?
·
· 2021
· Open Access
·
· DOI: https://doi.org/10.1002/celc.202100718
YOU?
·
· 2021
· Open Access
·
· DOI: https://doi.org/10.1002/celc.202100718
Self‐assembled monolayers (SAMs) of oligoethylene glycol (OEG)‐terminated alkanethiolates on gold, which are used to control protein adsorption and cell adhesion, were patterned by reaction with Br 2 /HOBr electrogenerated at a microelectrode of a scanning electrochemical microscope (SECM). The spreading of the Br 2 diffusion layers was limited by a homogeneous reaction with cystamine or L‐cystine as scavengers. The influence of process parameters on the patterning process was explored by simulation and combinatorial experiments. The experimental determination of pattern sizes from SECM feedback images was verified by scanning force microscopy. The simulation considered the local Br 2 formation as well as Br 2 consumption in the reaction with the OEG SAM, by reduction at the gold substrate, and by the homogeneous scavenging reaction. It used experimentally determined diffusion coefficients and rate constants of the scavenging reaction. and Experiments and simulation confirmed the existence of regions in the parameter space, in which the patterning process is robust against small variation of the parameters working distance, pulse time and scavenger excess.
Related Topics
Concepts
Scanning electrochemical microscopy
Monolayer
Chemistry
Electrochemistry
Substrate (aquarium)
Diffusion
Microelectrode
Self-assembled monolayer
Scanning electron microscope
Chemical engineering
Analytical Chemistry (journal)
Materials science
Nanotechnology
Physical chemistry
Organic chemistry
Electrode
Thermodynamics
Oceanography
Composite material
Physics
Engineering
Geology
Metadata
- Type
- article
- Language
- en
- Landing Page
- https://doi.org/10.1002/celc.202100718
- OA Status
- hybrid
- Cited By
- 7
- References
- 82
- Related Works
- 10
- OpenAlex ID
- https://openalex.org/W3187332186
All OpenAlex metadata
Raw OpenAlex JSON
- OpenAlex ID
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https://openalex.org/W3187332186Canonical identifier for this work in OpenAlex
- DOI
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https://doi.org/10.1002/celc.202100718Digital Object Identifier
- Title
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Modification and Patterning of Self‐Assembled Monolayers Using Electrogenerated Etchants and Homogeneous Scavenging Reactions in a Scanning Electrochemical MicroscopeWork title
- Type
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articleOpenAlex work type
- Language
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enPrimary language
- Publication year
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2021Year of publication
- Publication date
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2021-08-05Full publication date if available
- Authors
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Britta Vaske, Maximilian Schaube, Frank Meiners, Jan Henning Ross, Jens Christoffers, Günther WittstockList of authors in order
- Landing page
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https://doi.org/10.1002/celc.202100718Publisher landing page
- Open access
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YesWhether a free full text is available
- OA status
-
hybridOpen access status per OpenAlex
- OA URL
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https://doi.org/10.1002/celc.202100718Direct OA link when available
- Concepts
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Scanning electrochemical microscopy, Monolayer, Chemistry, Electrochemistry, Substrate (aquarium), Diffusion, Microelectrode, Self-assembled monolayer, Scanning electron microscope, Chemical engineering, Analytical Chemistry (journal), Materials science, Nanotechnology, Physical chemistry, Organic chemistry, Electrode, Thermodynamics, Oceanography, Composite material, Physics, Engineering, GeologyTop concepts (fields/topics) attached by OpenAlex
- Cited by
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7Total citation count in OpenAlex
- Citations by year (recent)
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2025: 2, 2022: 5Per-year citation counts (last 5 years)
- References (count)
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82Number of works referenced by this work
- Related works (count)
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10Other works algorithmically related by OpenAlex
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