Nanofibrillated Bacterial Cellulose Modified with (3-Aminopropyl)trimethoxysilane under Aqueous Conditions: Applications to Poly(methyl methacrylate) Fiber-Reinforced Nanocomposites Article Swipe
Hiroyuki Kono
,
Taiki Uno
,
Haruto Tsujisaki
,
Tokuo Matsushima
,
Kenji Tajima
·
YOU?
·
· 2020
· Open Access
·
· DOI: https://doi.org/10.1021/acsomega.0c04533
YOU?
·
· 2020
· Open Access
·
· DOI: https://doi.org/10.1021/acsomega.0c04533
The development of eco-friendly fiber-reinforced composite resins is an important objective from an environmental perspective, and nanofibrillated bacterial cellulose (NFBC), with extremely long high-aspect-ratio fibers, is a filler material with high potential for use in such composite resins. In this study, we investigated chemical modification of the surfaces of NFBC fibers by coupling with (3-aminopropyl)trimethoxysilane and fabricated nanocomposite materials using the prepared surface-modified NFBC. The product prepared by the one-pot reaction of (3-aminopropyl)trimethoxysilane with NFBC microfibrils dispersed in aqueous acid retained the same nanofibril structure as the intact NFBC. The degree of molar substitution and the silicon states on the surface of the product depended on the NFBC/(3-aminopropyl)trimethoxysilane ratio. The thermal analysis revealed that the thermal degradation temperature of the products increases with an increase of degree of molar substitution. Highly transparent (78-89% at 600 nm) poly(methyl methacrylate)-based nanocomposites were prepared by solvent casting; the nanocomposite containing 1.0 wt % (3-aminopropyl)trimethoxysilylated NFBC was only 8% less transparent than neat poly(methyl methacrylate) at 600 nm. In addition, the tensile strength of the nanocomposite was more than twice that of neat poly(methyl methacrylate) when 1 wt % of the surface-modified NFBC was added. The surface-modified NFBC is expected to be a reinforcing nanofiber material that imparts excellent physical properties to fiber-reinforced resins.
Related Topics
Concepts
Materials science
Nanocomposite
Methacrylate
Surface modification
Ultimate tensile strength
Nanofiber
Thermal stability
Composite material
Methyl methacrylate
Fiber
Composite number
Aqueous solution
Cellulose
Chemical engineering
Polymer chemistry
Polymer
Polymerization
Organic chemistry
Chemistry
Engineering
Metadata
- Type
- article
- Language
- en
- Landing Page
- https://doi.org/10.1021/acsomega.0c04533
- https://pubs.acs.org/doi/pdf/10.1021/acsomega.0c04533
- OA Status
- gold
- Cited By
- 29
- References
- 36
- Related Works
- 10
- OpenAlex ID
- https://openalex.org/W3096489270
All OpenAlex metadata
Raw OpenAlex JSON
- OpenAlex ID
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https://openalex.org/W3096489270Canonical identifier for this work in OpenAlex
- DOI
-
https://doi.org/10.1021/acsomega.0c04533Digital Object Identifier
- Title
-
Nanofibrillated Bacterial Cellulose Modified with (3-Aminopropyl)trimethoxysilane under Aqueous Conditions: Applications to Poly(methyl methacrylate) Fiber-Reinforced NanocompositesWork title
- Type
-
articleOpenAlex work type
- Language
-
enPrimary language
- Publication year
-
2020Year of publication
- Publication date
-
2020-11-02Full publication date if available
- Authors
-
Hiroyuki Kono, Taiki Uno, Haruto Tsujisaki, Tokuo Matsushima, Kenji TajimaList of authors in order
- Landing page
-
https://doi.org/10.1021/acsomega.0c04533Publisher landing page
- PDF URL
-
https://pubs.acs.org/doi/pdf/10.1021/acsomega.0c04533Direct link to full text PDF
- Open access
-
YesWhether a free full text is available
- OA status
-
goldOpen access status per OpenAlex
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https://pubs.acs.org/doi/pdf/10.1021/acsomega.0c04533Direct OA link when available
- Concepts
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Materials science, Nanocomposite, Methacrylate, Surface modification, Ultimate tensile strength, Nanofiber, Thermal stability, Composite material, Methyl methacrylate, Fiber, Composite number, Aqueous solution, Cellulose, Chemical engineering, Polymer chemistry, Polymer, Polymerization, Organic chemistry, Chemistry, EngineeringTop concepts (fields/topics) attached by OpenAlex
- Cited by
-
29Total citation count in OpenAlex
- Citations by year (recent)
-
2025: 9, 2024: 5, 2023: 6, 2022: 7, 2021: 2Per-year citation counts (last 5 years)
- References (count)
-
36Number of works referenced by this work
- Related works (count)
-
10Other works algorithmically related by OpenAlex
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