Nanostructure-induced performance degradation of WO₃·nH₂O for energy conversion and storage devices Article Swipe

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Zhenyin Hai , Mohammad Karbalaei Akbari , Zihan Wei , Danfeng Cui , Chenyang Xue , Hongyan Xu , Philippe M. Heynderickx , Francis Verpoort , Serge Zhuiykov ·

YOU? · · 2018 · Open Access · · DOI: https://doi.org/10.3762/bjnano.9.265

Although 2D layered nanomaterials have been intensively investigated towards their application in energy conversion and storage devices, their disadvantages have rarely been explored so far especially compared to their 3D counterparts. Herein, WO 3 · n H 2 O ( n = 0, 1, 2), as the most common and important electrochemical and electrochromic active nanomaterial, is synthesized in 3D and 2D structures through a facile hydrothermal method, and the disadvantages of the corresponding 2D structures are examined. The weakness of 2D WO 3 · n H 2 O originates from its layered structure. X-ray diffraction and scanning electron microscopy analyses of as-grown WO 3 · n H 2 O samples suggest a structural transition from 2D to 3D upon temperature increase. 2D WO 3 · n H 2 O easily generates structural instabilities by 2D intercalation, resulting in a faster performance degradation, due to its weak interlayer van der Waals forces, even though it outranks the 3D network structure in terms of improved electronic properties. The structural transformation of 2D layered WO 3 · n H 2 O into 3D nanostructures is observed via ex situ Raman measurements under electrochemical cycling experiments. The proposed degradation mechanism is confirmed by the morphology changes. The work provides strong evidence for and in-depth understanding of the weakness of 2D layered nanomaterials and paves the way for further interlayer reinforcement, especially for 2D layered transition metal oxides.

Related Topics

Materials Science

Nanomaterials

Nanotechnology

Intercalation (Chemistry)

Van Der Waals Force

Electrochemistry

Transition Metal

Scanning Electron Microscope

Concepts

Electrochromism Materials science Nanomaterials Nanostructure Raman spectroscopy Nanotechnology Intercalation (chemistry) van der Waals force Electrochemistry Transition metal Degradation (telecommunications) Hydrothermal circulation Scanning electron microscope Chemical engineering Electrode Molecule Inorganic chemistry Catalysis Chemistry Composite material Physical chemistry Optics Organic chemistry Telecommunications Physics Engineering Computer science Biochemistry

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Type: article
Language: en
Landing Page: https://doi.org/10.3762/bjnano.9.265
PDF: https://www.beilstein-journals.org/bjnano/content/pdf/2190-4286-9-265.pdf
OA Status: diamond
Cited By: 2
References: 54
Related Works: 10
OpenAlex ID: https://openalex.org/W2900819572

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DOI: https://doi.org/10.3762/bjnano.9.265

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Title: Nanostructure-induced performance degradation of WO₃·nH₂O for energy conversion and storage devices

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Language: en

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Publication year: 2018

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Publication date: 2018-11-12

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Authors: Zhenyin Hai, Mohammad Karbalaei Akbari, Zihan Wei, Danfeng Cui, Chenyang Xue, Hongyan Xu, Philippe M. Heynderickx, Francis Verpoort, Serge Zhuiykov

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Landing page: https://doi.org/10.3762/bjnano.9.265

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Concepts: Electrochromism, Materials science, Nanomaterials, Nanostructure, Raman spectroscopy, Nanotechnology, Intercalation (chemistry), van der Waals force, Electrochemistry, Transition metal, Degradation (telecommunications), Hydrothermal circulation, Scanning electron microscope, Chemical engineering, Electrode, Molecule, Inorganic chemistry, Catalysis, Chemistry, Composite material, Physical chemistry, Optics, Organic chemistry, Telecommunications, Physics, Engineering, Computer science, Biochemistry

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Cited by: 2

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Nanostructure-induced performance degradation of WO₃·nH₂O for energy conversion and storage devices Article Swipe