One-step synthesis of lead zirconate titanate particles using a solid-state reaction method Article Swipe

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Darmawan Hidayat , Mohammad Taufik , Setianto Setianto ·

YOU? · · 2022 · Open Access · · DOI: https://doi.org/10.1016/j.heliyon.2022.e09125

This study aims to determine the one-step synthesis of lead zirconate titanate (PbZr_(1-x)Ti_xO₃; PZT) particles, using a solid-state reaction method. These particles were synthesized at x of 0.48, using a solid-state reaction (SSR) method at various operating temperatures of 700-1000 °C. Before the reaction in a muffle furnace, the precursor powder was shaker milled for 2 h. The structural analysis of the diffraction patterns showed the formation of the PZT perovskite particles. It also showed the evolution from the tetragonal phase (at 800 and 900 °C) to the coexistence of tetragonal and rhombohedral stages in samples synthesized at 1000 °C. Furthermore, the crystallite particle size synthesized and commercialized at 1000 °C were 36.00 and 47.98 nm, respectively. These showed the formation of monodispersed size distribution, with an average of approximately 4.7 μm. Therefore, the PZT particles were successfully synthesized through a one-step synthesis, using the SSR method with a pre-mixed shaker milling.

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Materials Science

Solid-State Electronics

Concepts

Lead zirconate titanate Lead (geology) Materials science Solid-state Chemical engineering Nanotechnology Process engineering Chemistry Ferroelectricity Engineering Physical chemistry Geology Optoelectronics Geomorphology Dielectric

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Type: article
Language: en
Landing Page: https://doi.org/10.1016/j.heliyon.2022.e09125
PDF: http://www.cell.com/article/S2405844022004133/pdf
OA Status: gold
Cited By: 12
References: 35
Related Works: 10
OpenAlex ID: https://openalex.org/W4220911634

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DOI: https://doi.org/10.1016/j.heliyon.2022.e09125

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Title: One-step synthesis of lead zirconate titanate particles using a solid-state reaction method

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Type: article

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Language: en

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Publication year: 2022

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Publication date: 2022-03-01

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Authors: Darmawan Hidayat, Mohammad Taufik, Setianto Setianto

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Landing page: https://doi.org/10.1016/j.heliyon.2022.e09125

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PDF URL: https://www.cell.com/article/S2405844022004133/pdf

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Concepts: Lead zirconate titanate, Lead (geology), Materials science, Solid-state, Chemical engineering, Nanotechnology, Process engineering, Chemistry, Ferroelectricity, Engineering, Physical chemistry, Geology, Optoelectronics, Geomorphology, Dielectric

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Cited by: 12

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