Optimal processing conditions of a bio-based epoxy synthesized from vanillyl alcohol Article Swipe
Sihem Zaidi
,
Suman Thakur
,
Daniel Sánchez‐Rodríguez
,
Raquel Verdejo
,
Jordi Farjas
,
J. Costa
·
YOU?
·
· 2024
· Open Access
·
· DOI: https://doi.org/10.1016/j.polymdegradstab.2024.110743
YOU?
·
· 2024
· Open Access
·
· DOI: https://doi.org/10.1016/j.polymdegradstab.2024.110743
This work provides a comprehensive thermomechanical and rheological characterization of a high-performance epoxy resin synthesized from a vanillin derivative, vanillyl alcohol. The study includes a complete analysis of the curing and decomposition kinetics that enabled a Time-Temperature-Transformation plot accounting for gelation, vitrification, and resin degradation to be developed. These plots allow one to determine the optimal time and temperature processing conditions that will yield the best mechanical properties. Kinetic predictions and experimental results showed that this resin can be cured at room temperature in just a few hours, forming a solid gelled glass. Enhanced mechanical properties are achieved by post-curing the resin at temperatures above T = 85.4 °C. With a dynamic storage modulus of 2.7 GPa, this bio-based resin proves to be a sustainable alternative to fossil-based resins whose primary source is the ever-prevalent bisphenol A diglycidyl ether. Thermal oxidation is the main cause of the mechanical deterioration at high temperatures, as revealed by FTIR spectroscopy.
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Metadata
- Type
- article
- Language
- en
- Landing Page
- https://doi.org/10.1016/j.polymdegradstab.2024.110743
- OA Status
- hybrid
- Cited By
- 3
- References
- 70
- Related Works
- 10
- OpenAlex ID
- https://openalex.org/W4392699709
All OpenAlex metadata
Raw OpenAlex JSON
- OpenAlex ID
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https://openalex.org/W4392699709Canonical identifier for this work in OpenAlex
- DOI
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https://doi.org/10.1016/j.polymdegradstab.2024.110743Digital Object Identifier
- Title
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Optimal processing conditions of a bio-based epoxy synthesized from vanillyl alcoholWork title
- Type
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articleOpenAlex work type
- Language
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enPrimary language
- Publication year
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2024Year of publication
- Publication date
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2024-03-12Full publication date if available
- Authors
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Sihem Zaidi, Suman Thakur, Daniel Sánchez‐Rodríguez, Raquel Verdejo, Jordi Farjas, J. CostaList of authors in order
- Landing page
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https://doi.org/10.1016/j.polymdegradstab.2024.110743Publisher landing page
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YesWhether a free full text is available
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hybridOpen access status per OpenAlex
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https://doi.org/10.1016/j.polymdegradstab.2024.110743Direct OA link when available
- Concepts
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Epoxy, Diglycidyl ether, Dynamic mechanical analysis, Materials science, Curing (chemistry), Glass transition, Composite material, Fourier transform infrared spectroscopy, Vanillin, Bisphenol A, Thermal decomposition, Chemical engineering, Polymer, Organic chemistry, Chemistry, EngineeringTop concepts (fields/topics) attached by OpenAlex
- Cited by
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3Total citation count in OpenAlex
- Citations by year (recent)
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2025: 2, 2024: 1Per-year citation counts (last 5 years)
- References (count)
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70Number of works referenced by this work
- Related works (count)
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10Other works algorithmically related by OpenAlex
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