Ordered Mesoporous Carbons via Self-Assembly of Tailored Block Copolyethers for Pore Size-Dependent Applications Article Swipe
Felix Markus
,
Charlotte Vogler
,
Johanna R. Bruckner
,
Stefan Naumann
·
YOU?
·
· 2021
· Open Access
·
· DOI: https://doi.org/10.1021/acsanm.0c03467
YOU?
·
· 2021
· Open Access
·
· DOI: https://doi.org/10.1021/acsanm.0c03467
Using an organocatalytic polymerization method for the preparation of well-defined, amphiphilic block copolyethers of the type PPOn/2-PEOm-PPOn/2 ("Reverse Pluronics", Mn up to 50 000 g/mol, ĐM = 1.01–1.08, >100 examples), it is demonstrated that the application of these polymers as structure-directing agents (SDAs) in a standard soft-templating process delivers ordered mesoporous carbons (OMCs), whereby the resulting pore diameters are monomodal and narrowly distributed. Moreover, by the judicious choice of the SDA properties (total molar mass, ratio of n and m, and PPO block length), pore diameters in the range of 6–18 nm can be selectively addressed, notably within the same arrangement pattern (2D hexagonal, p6mm). This provides a rational, operationally simple method to tailor pore properties of otherwise uniform carbons, also significantly reducing the effort necessary to obtain systematically altered materials. Ready access to such quick screenings is assumed to be immensely useful for pore size-dependent applications from numerous disciplines such as sensing, catalysis, or energy storage and conversion. Surprisingly, it is not only found that a minimum of Mn = 13 000 g/mol is required to deliver ordered (nondistorted) materials under these conditions but also that very high-molar-mass SDAs are best suited to achieve optimum results, potentially providing an explanation for why "Reverse Pluronics" are frequently, and wrongly, thought to be per se unsuitable for the preparation of well-ordered mesoporous carbons.
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- Type
- article
- Language
- en
- Landing Page
- https://doi.org/10.1021/acsanm.0c03467
- OA Status
- hybrid
- Cited By
- 17
- References
- 44
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- OpenAlex ID
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All OpenAlex metadata
Raw OpenAlex JSON
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https://openalex.org/W3135021917Canonical identifier for this work in OpenAlex
- DOI
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https://doi.org/10.1021/acsanm.0c03467Digital Object Identifier
- Title
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Ordered Mesoporous Carbons via Self-Assembly of Tailored Block Copolyethers for Pore Size-Dependent ApplicationsWork title
- Type
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articleOpenAlex work type
- Language
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enPrimary language
- Publication year
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2021Year of publication
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2021-03-10Full publication date if available
- Authors
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Felix Markus, Charlotte Vogler, Johanna R. Bruckner, Stefan NaumannList of authors in order
- Landing page
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https://doi.org/10.1021/acsanm.0c03467Publisher landing page
- Open access
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YesWhether a free full text is available
- OA status
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hybridOpen access status per OpenAlex
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https://doi.org/10.1021/acsanm.0c03467Direct OA link when available
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Mesoporous material, Materials science, Block (permutation group theory), Self-assembly, Nanotechnology, Chemical engineering, Chemistry, Mathematics, Organic chemistry, Combinatorics, Engineering, CatalysisTop concepts (fields/topics) attached by OpenAlex
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17Total citation count in OpenAlex
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2025: 6, 2024: 2, 2023: 6, 2022: 2, 2021: 1Per-year citation counts (last 5 years)
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44Number of works referenced by this work
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10Other works algorithmically related by OpenAlex
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| abstract_inverted_index.these | 37, 182 |
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| abstract_inverted_index.(total | 72 |
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