Oxidation of TiC–SiC nanocomposite Article Swipe
Hélène Aréna
,
Moustapha Coulibaly
,
Nicolas Pradeilles
,
Adel Mesbah
,
Alban Jonchère
,
Guilhem Arrachart
,
Marion Vandenhende
,
Alexandre Maı̂tre
,
Samuel Bernard
,
Xavier Deschanels
·
YOU?
·
· 2025
· Open Access
·
· DOI: https://doi.org/10.1111/jace.20336
YOU?
·
· 2025
· Open Access
·
· DOI: https://doi.org/10.1111/jace.20336
This work aims at understanding the oxidation mechanism of a TiC–SiC nanocomposite ceramic material. Samples were subjected to heat treatments up to 1400°C under air, varying the relative density of the composite, the heating rate, and the dwell time. The weight variations were followed by thermogravimetric analyses coupled with mass spectrometry. The oxidized samples were then characterized by scanning electron microscopy on cross‐sections (SEM‐EDX) and their microstructure and composition were studied by transmission electron microscopy (TEM‐EDX). The oxidation process was also followed by in situ high‐temperature X‐ray diffraction and high‐temperature environmental scanning electron microscopy. Until 1000°C, the formation of a multilayer alteration scale was observed, with a dense and protective SiO 2 layer. Above 1200°C, this layer showed cracks, and the oxidation was increased. Based on the results, a three‐step mechanism was proposed for the temperature‐dependent conversion of TiC and SiC to the subsequent oxides.
Related Topics
Concepts
Scanning electron microscope
Microstructure
Materials science
Thermogravimetric analysis
Transmission electron microscopy
Nanocomposite
Ceramic
Composite number
Layer (electronics)
Chemical engineering
Composite material
Analytical Chemistry (journal)
Chemistry
Nanotechnology
Chromatography
Engineering
Metadata
- Type
- article
- Language
- en
- Landing Page
- https://doi.org/10.1111/jace.20336
- OA Status
- green
- References
- 42
- Related Works
- 10
- OpenAlex ID
- https://openalex.org/W4406134191
All OpenAlex metadata
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https://openalex.org/W4406134191Canonical identifier for this work in OpenAlex
- DOI
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https://doi.org/10.1111/jace.20336Digital Object Identifier
- Title
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Oxidation of TiC–SiC nanocompositeWork title
- Type
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articleOpenAlex work type
- Language
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enPrimary language
- Publication year
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2025Year of publication
- Publication date
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2025-01-07Full publication date if available
- Authors
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Hélène Aréna, Moustapha Coulibaly, Nicolas Pradeilles, Adel Mesbah, Alban Jonchère, Guilhem Arrachart, Marion Vandenhende, Alexandre Maı̂tre, Samuel Bernard, Xavier DeschanelsList of authors in order
- Landing page
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https://doi.org/10.1111/jace.20336Publisher landing page
- Open access
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YesWhether a free full text is available
- OA status
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greenOpen access status per OpenAlex
- OA URL
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https://hal.science/hal-04878586Direct OA link when available
- Concepts
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Scanning electron microscope, Microstructure, Materials science, Thermogravimetric analysis, Transmission electron microscopy, Nanocomposite, Ceramic, Composite number, Layer (electronics), Chemical engineering, Composite material, Analytical Chemistry (journal), Chemistry, Nanotechnology, Chromatography, EngineeringTop concepts (fields/topics) attached by OpenAlex
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