Rapid Scan Electron Paramagnetic Resonance (EPR) and Digital EPR Development Article Swipe
Rapid scan electron paramagnetic resonance (EPR) was developed in the Eaton laboratory at the University of Denver. Applications of rapid scan to wider spectra, such as for immobilized nitroxides, spin-labeled proteins, irradiated tooth and fingernail samples were demonstrated in this dissertation. The scan width has been increased from 55 G to 160 G. The signal to noise (S/N) improvement for slowly tumbling spin-labeled protein samples that is provided by rapid scan EPR will be highly advantageous for biophysical studies. With substantial improvement in S/N by rapid scan, the dose estimation for irradiated tooth enamels became more reliable than the traditional continuous wave (CW) EPR.\nAn alternate approach of rapid scan, called field-stepped direct detection EPR, was developed to reconstruct wider EPR signals. A Mn2+ containing crystal was measured by field-stepped direct detection EPR, which had a spectrum more than 6000 G wide. Since the field-stepped direct detection extends the advantages of rapid scan to much wider scan ranges, this methodology has a great potential to replace the traditional CW EPR.\nWith recent advances in digital electronics, a digital rapid scan spectrometer was built based on an arbitrary waveform generator (AWG), which can excite spins and detect EPR signals with a fully digital system. A near-baseband detection method was used to acquire the in-phase and quadrature signals in one physical channel. The signal was analyzed digitally to generate ideally orthogonal quadrature signals.\nA multiharmonic algorithm was developed that employed harmonics of the modulation frequencies acquired in the spectrometer transient mode. It was applied for signals with complicated lineshapes, and can simplify the selection of modulation amplitude.\nA digital saturation recovery system based on an AWG was built at X-band (9.6 GHz). To demonstrate performance of the system, the spin-lattice relaxation time of a fused quartz rod was measured at room temperature with fully digital excitation and detection.
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- Language
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- Landing Page
- https://digitalcommons.du.edu/etd/1057
- https://digitalcommons.du.edu/etd/1057
- OA Status
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- Related Works
- 20
- OpenAlex ID
- https://openalex.org/W2527646706
All OpenAlex metadata
Raw OpenAlex JSON
- OpenAlex ID
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https://openalex.org/W2527646706Canonical identifier for this work in OpenAlex
- Title
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Rapid Scan Electron Paramagnetic Resonance (EPR) and Digital EPR DevelopmentWork title
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articleOpenAlex work type
- Language
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enPrimary language
- Publication year
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2015Year of publication
- Publication date
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2015-01-01Full publication date if available
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Zhelin YuList of authors in order
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https://digitalcommons.du.edu/etd/1057Publisher landing page
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https://digitalcommons.du.edu/etd/1057Direct link to full text PDF
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- OA status
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greenOpen access status per OpenAlex
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https://digitalcommons.du.edu/etd/1057Direct OA link when available
- Concepts
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Electron paramagnetic resonance, Pulsed EPR, Nuclear magnetic resonance, Resonance (particle physics), Materials science, Physics, Magnetic resonance imaging, Atomic physics, Medicine, Spin echo, RadiologyTop concepts (fields/topics) attached by OpenAlex
- Cited by
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0Total citation count in OpenAlex
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20Other works algorithmically related by OpenAlex
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| countries_distinct_count | 0 |
| institutions_distinct_count | 1 |
| citation_normalized_percentile.value | 0.08004031 |
| citation_normalized_percentile.is_in_top_1_percent | False |
| citation_normalized_percentile.is_in_top_10_percent | False |