Rationalization of Hydrothermal Synthesis of NaNbO3 by Rapid in Situ Time-Resolved Synchrotron X-ray Diffraction Article Swipe
Susanne Linn Skjærvø
,
Kristin Høydalsvik Wells
,
Sanna Sommer
,
T. Dan Vu
,
Julian R. Tolchard
,
Wouter van Beek
,
Tor Grande
,
Bo B. Iversen
,
Mari‐Ann Einarsrud
·
YOU?
·
· 2018
· Open Access
·
· DOI: https://doi.org/10.1021/acs.cgd.7b01192
YOU?
·
· 2018
· Open Access
·
· DOI: https://doi.org/10.1021/acs.cgd.7b01192
In situ monitoring of the formation of crystalline phases during conventional hydrothermal synthesis is experimentally challenging. Here, we report an in situ time-resolved synchrotron X-ray diffraction study during hydrothermal synthesis of NaNbO3 using a high-pressure custom-made capillary cell penetrable to X-rays. The high time resolution (0.1 s) revealed a sequence of transient intermediate phases, including several unknown phases, before the final perovskite NaNbO3 was formed. These new findings highlight the complexity of the hydrothermal synthesis of NaNbO3 and demonstrate the potential for obtaining in-depth knowledge of the reactions taking place by time-resolved in situ X-ray diffraction.
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Metadata
- Type
- article
- Language
- en
- Landing Page
- https://doi.org/10.1021/acs.cgd.7b01192
- OA Status
- green
- Cited By
- 21
- References
- 23
- Related Works
- 10
- OpenAlex ID
- https://openalex.org/W2783427290
All OpenAlex metadata
Raw OpenAlex JSON
- OpenAlex ID
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https://openalex.org/W2783427290Canonical identifier for this work in OpenAlex
- DOI
-
https://doi.org/10.1021/acs.cgd.7b01192Digital Object Identifier
- Title
-
Rationalization of Hydrothermal Synthesis of NaNbO3 by Rapid in Situ Time-Resolved Synchrotron X-ray DiffractionWork title
- Type
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articleOpenAlex work type
- Language
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enPrimary language
- Publication year
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2018Year of publication
- Publication date
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2018-01-10Full publication date if available
- Authors
-
Susanne Linn Skjærvø, Kristin Høydalsvik Wells, Sanna Sommer, T. Dan Vu, Julian R. Tolchard, Wouter van Beek, Tor Grande, Bo B. Iversen, Mari‐Ann EinarsrudList of authors in order
- Landing page
-
https://doi.org/10.1021/acs.cgd.7b01192Publisher landing page
- Open access
-
YesWhether a free full text is available
- OA status
-
greenOpen access status per OpenAlex
- OA URL
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https://hdl.handle.net/11250/2580868Direct OA link when available
- Concepts
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Hydrothermal circulation, Synchrotron, Hydrothermal synthesis, In situ, Diffraction, Materials science, X-ray crystallography, Crystallography, Synchrotron radiation, Nanotechnology, Chemistry, Chemical engineering, Optics, Physics, Organic chemistry, EngineeringTop concepts (fields/topics) attached by OpenAlex
- Cited by
-
21Total citation count in OpenAlex
- Citations by year (recent)
-
2024: 2, 2023: 1, 2022: 2, 2021: 3, 2020: 6Per-year citation counts (last 5 years)
- References (count)
-
23Number of works referenced by this work
- Related works (count)
-
10Other works algorithmically related by OpenAlex
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