Scalable Synthesis of MXene Nanoscrolls Article Swipe
Teng Zhang
,
Benjamin Chacon
,
Danzhen Zhang
,
AW Cotton
,
Yihui Zhang
,
Yuan Zhang
,
Stefano Ippolito
,
Francesca Urban
,
Tetiana Parker
,
Lingyi Bi
,
Kateryna Shevchuk
,
Kyle Matthews
,
Eric A. Stach
,
Yury Gogotsi
·
YOU?
·
· 2025
· Open Access
·
· DOI: https://doi.org/10.26434/chemrxiv-2025-z9424
YOU?
·
· 2025
· Open Access
·
· DOI: https://doi.org/10.26434/chemrxiv-2025-z9424
MXenes are a promising class of 2D carbides and nitrides known for their high electrical conductivity, hydrophilicity, mechanical strength, and unique optoelectronic properties, leading to numerous applications. However, their scalable synthesis in a 1D morphology, such as MXene nanotubes or scrolls, has not been demonstrated yet. This work presents a versatile and scalable method for manufacturing MXene scrolls, including Ti2CTx, Ti3C2Tx, Ti3CNTx, V2CTx, Nb2CTx, and Ta4C3Tx. We demonstrate high-yield production of up to 45 wt% of MAX phase precursor and precise control over scrolls’ alignment and morphology. Properties of scrolls differ from 2D flakes; e.g., a freestanding film made of scrolled Nb2CTx presents a transition to superconducting state below 5.2 K. Films of MXene scrolls exhibit 3 times lower density and enhanced mass transport compared to flakes, resulting in an improved performance in supercapacitor electrodes and humidity sensors. The dispersion of the scrolls in water behaves like an electrorheological fluid. Aligning scrolls in an electric field allows for circuit switching between electrically insulating and conductive states. These scrolls can be assembled into vertically aligned MXene forests, fibers, and other architectures. The availability of 1D MXene scroll offers exciting opportunities in many fields.
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Metadata
- Type
- preprint
- Language
- en
- Landing Page
- https://doi.org/10.26434/chemrxiv-2025-z9424
- https://chemrxiv.org/engage/api-gateway/chemrxiv/assets/orp/resource/item/67c884186dde43c9089e5c08/original/scalable-synthesis-of-m-xene-nanoscrolls.pdf
- OA Status
- gold
- Cited By
- 2
- Related Works
- 10
- OpenAlex ID
- https://openalex.org/W4408232182
All OpenAlex metadata
Raw OpenAlex JSON
- OpenAlex ID
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https://openalex.org/W4408232182Canonical identifier for this work in OpenAlex
- DOI
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https://doi.org/10.26434/chemrxiv-2025-z9424Digital Object Identifier
- Title
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Scalable Synthesis of MXene NanoscrollsWork title
- Type
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preprintOpenAlex work type
- Language
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enPrimary language
- Publication year
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2025Year of publication
- Publication date
-
2025-03-07Full publication date if available
- Authors
-
Teng Zhang, Benjamin Chacon, Danzhen Zhang, AW Cotton, Yihui Zhang, Yuan Zhang, Stefano Ippolito, Francesca Urban, Tetiana Parker, Lingyi Bi, Kateryna Shevchuk, Kyle Matthews, Eric A. Stach, Yury GogotsiList of authors in order
- Landing page
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https://doi.org/10.26434/chemrxiv-2025-z9424Publisher landing page
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https://chemrxiv.org/engage/api-gateway/chemrxiv/assets/orp/resource/item/67c884186dde43c9089e5c08/original/scalable-synthesis-of-m-xene-nanoscrolls.pdfDirect link to full text PDF
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YesWhether a free full text is available
- OA status
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goldOpen access status per OpenAlex
- OA URL
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https://chemrxiv.org/engage/api-gateway/chemrxiv/assets/orp/resource/item/67c884186dde43c9089e5c08/original/scalable-synthesis-of-m-xene-nanoscrolls.pdfDirect OA link when available
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Scalability, Computer science, Materials science, Computer architecture, Nanotechnology, DatabaseTop concepts (fields/topics) attached by OpenAlex
- Cited by
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2Total citation count in OpenAlex
- Citations by year (recent)
-
2025: 2Per-year citation counts (last 5 years)
- Related works (count)
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10Other works algorithmically related by OpenAlex
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