Solar photoelectro-Fenton-like process with anodically-generated HClO in a flow reactor: Norfloxacin as a pollutant with a particular structure Article Swipe
María F. Murrieta
,
Enric Brillas
,
José L. Nava
,
Ignasi Sirés
·
YOU?
·
· 2022
· Open Access
·
· DOI: https://doi.org/10.1016/j.seppur.2022.122893
YOU?
·
· 2022
· Open Access
·
· DOI: https://doi.org/10.1016/j.seppur.2022.122893
The degradation and mineralization of the drug norfloxacin (NFX) has been assessed in a model solution, containing 15 mM NaCl +45 mM Na2SO4 at pH 3.0, using a flow plant with an FM01-LC filter-press reactor equipped with a Ti|Ir-Sn-Ru oxides anode to electrogenerate HClO from Cl− oxidation and a stainless-steel cathode. Unexpectedly, anodic oxidation with active chlorine (AO-HClO) outperformed electro-Fenton (EF-HClO), photoelectro-Fenton (PEF-HClO) and solar photoelectro-Fenton (SPEF-HClO) due to: (i) the formation of refractory complexes between iron ions and carboxyl group of NFX, and (ii) the conversion of HClO into less effective •OH upon its Fenton-like reaction with added Fe2+ catalyst. SPEF-HClO was superior among Fenton-based treatments because the •OH concentration was largely increased by the photolysis of Fe(III) species. At an initial NFX concentration in the range 0.103–0.146 mM, the optimum conditions for SPEF-HClO were 0.40 mM Fe2+ and 15 mA cm−2. A BDD anode allowed a higher production of •OH, accelerating the degradation and mineralization, with similar energy requirements as compared to trials with Ti|Ir-Sn-Ru oxides anode. The SPEF-HClO process in urban wastewater was less powerful because of the parallel oxidation of natural organic matter. HClO, Fe2+ and Fetotal were quantified in both water matrices. The initial degradation sequence for NFX, proposed from 10 primary by-products identified by LC-MS/MS, revealed the occurrence of hydroxylation, chlorination and defluorination steps. Additionally, 5 stable by-products were detected by GC–MS.
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- https://ars.els-cdn.com/content/image/1-s2.0-S1383586622024509-ga1_lrg.jpg
- OA Status
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All OpenAlex metadata
Raw OpenAlex JSON
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https://openalex.org/W4313214960Canonical identifier for this work in OpenAlex
- DOI
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https://doi.org/10.1016/j.seppur.2022.122893Digital Object Identifier
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Solar photoelectro-Fenton-like process with anodically-generated HClO in a flow reactor: Norfloxacin as a pollutant with a particular structureWork title
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articleOpenAlex work type
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enPrimary language
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2022Year of publication
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2022-12-13Full publication date if available
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María F. Murrieta, Enric Brillas, José L. Nava, Ignasi SirésList of authors in order
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https://doi.org/10.1016/j.seppur.2022.122893Publisher landing page
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https://ars.els-cdn.com/content/image/1-s2.0-S1383586622024509-ga1_lrg.jpgDirect link to full text PDF
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YesWhether a free full text is available
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hybridOpen access status per OpenAlex
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https://ars.els-cdn.com/content/image/1-s2.0-S1383586622024509-ga1_lrg.jpgDirect OA link when available
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Chemistry, Mineralization (soil science), Chlorine, Hydroxylation, Anode, Inorganic chemistry, Nuclear chemistry, Organic chemistry, Electrode, Nitrogen, Enzyme, Physical chemistryTop concepts (fields/topics) attached by OpenAlex
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20Total citation count in OpenAlex
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2025: 6, 2024: 7, 2023: 7Per-year citation counts (last 5 years)
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60Number of works referenced by this work
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10Other works algorithmically related by OpenAlex
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| publication_date | 2022-12-13 |
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