Speciation Of Iron (Iii) Oxide Nanoparticles And Other Paramagnetic Intermediates During High-Temperature Oxidative Pyrolysis Of 1-Methylnaphthalene Article Swipe

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Michael P. Herring , Lavrent Khachatryan , Barry Dellinger ·

YOU? · · 2015 · Open Access · · DOI: https://doi.org/10.5281/zenodo.1108403

Low Temperature Matrix Isolation - Electron Paramagnetic Resonance (LTMI-EPR) Spectroscopy was utilized to identify the species of iron oxide nanoparticles generated during the oxidative pyrolysis of 1-methylnaphthalene (1-MN). The otherwise gas-phase reactions of 1--MN were impacted by a polypropylenimine tetra-hexacontaamine dendrimer complexed with iron (III) nitrate nonahydrate diluted in air under atmospheric conditions. The EPR fine structure of Fe (III)2O3 nanoparticles clusters, characterized by gfactors of 2.00, 2.28, 3.76 and 4.37 were detected on a cold finger maintained at 77 K after accumulation over a multitude of experiments. Additionally, a high valence Fe (IV) paramagnetic intermediate and superoxide anion-radicals, O2•- adsorbed on nanoparticle surfaces in the form of Fe (IV) --- O2•- were detected from the quenching area of Zone 1 in the gas-phase.

Related Topics

Electron Paramagnetic Resonance

Infrared Spectroscopy

Organic Chemistry

Nuclear Magnetic Resonance

Nanotechnology

Physics

Quantum Mechanics

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Electron paramagnetic resonance Nanoparticle Chemistry Radical Paramagnetism Matrix isolation Adsorption Oxide Pyrolysis Valence (chemistry) Inorganic chemistry Iron oxide nanoparticles Photochemistry Iron oxide Materials science Physical chemistry Infrared spectroscopy Organic chemistry Nuclear magnetic resonance Nanotechnology Physics Quantum mechanics

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Type: article
Language: en
Landing Page: https://www.ncbi.nlm.nih.gov/pmc/articles/4581597
OA Status: green
Cited By: 7
References: 24
Related Works: 10
OpenAlex ID: https://openalex.org/W2299463370

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DOI: https://doi.org/10.5281/zenodo.1108403

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Title: Speciation Of Iron (Iii) Oxide Nanoparticles And Other Paramagnetic Intermediates During High-Temperature Oxidative Pyrolysis Of 1-Methylnaphthalene

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Language: en

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Publication year: 2015

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Publication date: 2015-08-03

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Authors: Michael P. Herring, Lavrent Khachatryan, Barry Dellinger

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Concepts: Electron paramagnetic resonance, Nanoparticle, Chemistry, Radical, Paramagnetism, Matrix isolation, Adsorption, Oxide, Pyrolysis, Valence (chemistry), Inorganic chemistry, Iron oxide nanoparticles, Photochemistry, Iron oxide, Materials science, Physical chemistry, Infrared spectroscopy, Organic chemistry, Nuclear magnetic resonance, Nanotechnology, Physics, Quantum mechanics

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Cited by: 7

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referenced_works	https://openalex.org/W2066311520, https://openalex.org/W2094789389, https://openalex.org/W2334883700, https://openalex.org/W2105067416, https://openalex.org/W2068185427, https://openalex.org/W1558593020, https://openalex.org/W2312787852, https://openalex.org/W2003437825, https://openalex.org/W1542999932, https://openalex.org/W2040038309, https://openalex.org/W1845242231, https://openalex.org/W1971835748, https://openalex.org/W1966881345, https://openalex.org/W1994410863, https://openalex.org/W2024195093, https://openalex.org/W1985068361, https://openalex.org/W1990310429, https://openalex.org/W1979778685, https://openalex.org/W2084938182, https://openalex.org/W2129652151, https://openalex.org/W1980699588, https://openalex.org/W1986980888, https://openalex.org/W2329090926, https://openalex.org/W1992368545
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