Spectroscopic/Microscopic Elucidation for Chemical Changes During Acid Pretreatment on Arundo donax Article Swipe
Bingwei Chen
,
Wang Xinzhou
,
Weiqi Leng
,
Yu’na Kan
,
Changtong Mei
,
Shengcheng Zhai
·
YOU?
·
· 2019
· Open Access
·
· DOI: https://doi.org/10.12162/jbb.v4i3.008
YOU?
·
· 2019
· Open Access
·
· DOI: https://doi.org/10.12162/jbb.v4i3.008
The Arundo donax is a typical fast-growing species from the family Gramineae, which is widely cultivated in China. With a huge yield of A. donax in China, this plant offers great potential for biofuels production. The different types of organization of cell and the tissue in the A. donax could influence the efficiency of enzymatic hydrolysis. In this study, A. donax was subjected to 0.5% (w/w) sulfuric acid (H2SO4) for pretreatment at 140°C for 10 min, 20 min, 40 min, and 60 min, respectively. The changes in microstructure, chemical composition, topochemical properties were comprehensively analyzed. Using a series of spectroscopic and microscopic techniques including Fourier transform infrared spectroscopy (FT-IR), X-Ray diffraction (XRD), polarized light microscopy (PLM), and confocal Raman microscopy (CRM) to obtain the correlative structural and chemical information. Analysis results of chemical composition, FT-IR spectra and XRD indicated that with increasing reaction time, more hemicellulose and lignin would be removed. Correspondingly, there was an obvious increase of the cellulose relative crystallinity via extending reaction time. Results of the PLM observations showed that the birefringence gradually dimmed due to the diminishing of the cellulose component. Furthermore, the CRM mapping images showed the lignin component in compound middle lamellar (CML) was difficult to remove relatively as compared with that in secondary walls. These results indicated that the combination of spectroscopic and microscopic elucidation could give an insightful understanding of chemical changes in cellular level during pretreatment.
Related Topics
Concepts
Arundo donax
Lignin
Cellulose
Crystallinity
Chemical composition
Chemistry
Sulfuric acid
Fourier transform infrared spectroscopy
Hemicellulose
Chemical structure
Lamellar structure
Chemical engineering
Nuclear chemistry
Materials science
Biomass (ecology)
Biochemistry
Organic chemistry
Crystallography
Biology
Agronomy
Engineering
Metadata
- Type
- article
- Language
- en
- Landing Page
- https://doaj.org/article/795ce2f07f57454a93eda4c18b3b85a5
- OA Status
- green
- Cited By
- 27
- References
- 42
- Related Works
- 20
- OpenAlex ID
- https://openalex.org/W2986039006
All OpenAlex metadata
Raw OpenAlex JSON
- OpenAlex ID
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https://openalex.org/W2986039006Canonical identifier for this work in OpenAlex
- DOI
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https://doi.org/10.12162/jbb.v4i3.008Digital Object Identifier
- Title
-
Spectroscopic/Microscopic Elucidation for Chemical Changes During Acid Pretreatment on Arundo donaxWork title
- Type
-
articleOpenAlex work type
- Language
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enPrimary language
- Publication year
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2019Year of publication
- Publication date
-
2019-07-01Full publication date if available
- Authors
-
Bingwei Chen, Wang Xinzhou, Weiqi Leng, Yu’na Kan, Changtong Mei, Shengcheng ZhaiList of authors in order
- Landing page
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https://doaj.org/article/795ce2f07f57454a93eda4c18b3b85a5Publisher landing page
- Open access
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YesWhether a free full text is available
- OA status
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greenOpen access status per OpenAlex
- OA URL
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https://jbb.xml-journal.net/en/article/doi/10.12162/jbb.v4i3.008Direct OA link when available
- Concepts
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Arundo donax, Lignin, Cellulose, Crystallinity, Chemical composition, Chemistry, Sulfuric acid, Fourier transform infrared spectroscopy, Hemicellulose, Chemical structure, Lamellar structure, Chemical engineering, Nuclear chemistry, Materials science, Biomass (ecology), Biochemistry, Organic chemistry, Crystallography, Biology, Agronomy, EngineeringTop concepts (fields/topics) attached by OpenAlex
- Cited by
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27Total citation count in OpenAlex
- Citations by year (recent)
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2025: 1, 2024: 3, 2023: 6, 2022: 2, 2021: 6Per-year citation counts (last 5 years)
- References (count)
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42Number of works referenced by this work
- Related works (count)
-
20Other works algorithmically related by OpenAlex
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