Structure-Function Correlations in Sputter Deposited Gold/Fluorocarbon Multilayers for Tuning Optical Response Article Swipe
Pallavi Pandit
,
Matthias Schwartzkopf
,
André Rothkirch
,
Stephan V. Roth
,
Sigrid Bernstorff
,
Ajay Gupta
·
YOU?
·
· 2019
· Open Access
·
· DOI: https://doi.org/10.20944/preprints201906.0287.v1
YOU?
·
· 2019
· Open Access
·
· DOI: https://doi.org/10.20944/preprints201906.0287.v1
A new strategy to nanoengineer gold/fluorocarbon multilayer (ML) nanostructures is reported. We have investigated the morphological changes occuring at the metal-polymer interface in multilayer structures with varying volume fraction of gold (Au) and the kinetic growth aspect of the microscale properties of nano-sized Au in plasma polymer fluorocarbon (PPFC). Investigations were carried out at various temperatures and annealing time by means of grazing incidence small-angle and wide-angle X-ray scattering (GISAXS and GIWAXS). We have fabricated a series of multilayers with variying volume fraction (0.12, 0.27, 0.38) of Au and bilayer periodicity in ML structure. They show an interesting granular structure consisting of nearly spherical shaped nanoparticles within the polymer layer. The nanoparticle (NP) morphology changes due to the collective effects of NPs diffusion within ensembles in the in-plane vicinity and inter-layer with increasing temperature. The in-plane NPs size distinctly increases (from 1.9 to 4 nm) with increasing temperature. The NPs become more spherical thus reducing the surface energy. Linear growth of NPs with temperature and time shows diffusion-controled growth of NPs in the ML structure. The structural stability of the multilayer is controlled by the volume ratio of the metal in polymer. At room temperature UV-Vis shows a blueshift of the plasmon peak from 560 nm in ML Au/PTFE_1 to 437 nm in Au/PTFE_3. We have identified the fabrication and post-deposition annealing conditions to limit the Local Surface Plasmon resonance (LSPR) shift (from 〖∆λ〗_LSPR=180 nm (Au/PTFE_1) to 〖∆λ〗_LSPR=67 nm (Au/PTFE_3 ML)) and their optical response over a wide visible wavelength range. A variation in the dielectric constant of the polymer in precence of varying Au inclusion is found to be the main factor affecting the LSPR frequency. Our finding may provide insights in Nano engineering ML structure can be useful to systematically control the growth of NPs in polymer matrix.
Related Topics
Concepts
Materials science
Annealing (glass)
Grazing-incidence small-angle scattering
Volume fraction
Surface plasmon resonance
Nanoparticle
Bilayer
Polymer
Colloidal gold
Nanotechnology
Scattering
Analytical Chemistry (journal)
Optics
Composite material
Chemistry
Biochemistry
Small-angle neutron scattering
Chromatography
Neutron scattering
Physics
Membrane
Metadata
- Type
- preprint
- Language
- en
- Landing Page
- https://doi.org/10.20944/preprints201906.0287.v1
- https://www.preprints.org/manuscript/201906.0287/v1/download
- OA Status
- green
- Cited By
- 3
- References
- 62
- Related Works
- 10
- OpenAlex ID
- https://openalex.org/W3125275745
All OpenAlex metadata
Raw OpenAlex JSON
- OpenAlex ID
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https://openalex.org/W3125275745Canonical identifier for this work in OpenAlex
- DOI
-
https://doi.org/10.20944/preprints201906.0287.v1Digital Object Identifier
- Title
-
Structure-Function Correlations in Sputter Deposited Gold/Fluorocarbon Multilayers for Tuning Optical ResponseWork title
- Type
-
preprintOpenAlex work type
- Language
-
enPrimary language
- Publication year
-
2019Year of publication
- Publication date
-
2019-06-27Full publication date if available
- Authors
-
Pallavi Pandit, Matthias Schwartzkopf, André Rothkirch, Stephan V. Roth, Sigrid Bernstorff, Ajay GuptaList of authors in order
- Landing page
-
https://doi.org/10.20944/preprints201906.0287.v1Publisher landing page
- PDF URL
-
https://www.preprints.org/manuscript/201906.0287/v1/downloadDirect link to full text PDF
- Open access
-
YesWhether a free full text is available
- OA status
-
greenOpen access status per OpenAlex
- OA URL
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https://www.preprints.org/manuscript/201906.0287/v1/downloadDirect OA link when available
- Concepts
-
Materials science, Annealing (glass), Grazing-incidence small-angle scattering, Volume fraction, Surface plasmon resonance, Nanoparticle, Bilayer, Polymer, Colloidal gold, Nanotechnology, Scattering, Analytical Chemistry (journal), Optics, Composite material, Chemistry, Biochemistry, Small-angle neutron scattering, Chromatography, Neutron scattering, Physics, MembraneTop concepts (fields/topics) attached by OpenAlex
- Cited by
-
3Total citation count in OpenAlex
- Citations by year (recent)
-
2021: 1, 2020: 1, 2019: 1Per-year citation counts (last 5 years)
- References (count)
-
62Number of works referenced by this work
- Related works (count)
-
10Other works algorithmically related by OpenAlex
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